Method of removing work-affected layer

Patent metadata

Field	Value
Publication number	US-9481934-B2
Application number	US-201313796150-A
Country	US
Kind code	B2
Filing date	Mar 12, 2013
Priority date	May 9, 2012
Publication date	Nov 1, 2016
Grant date	Nov 1, 2016

Abstract

A method of removing a work-affected layer formed on the worked surface of a TiAl-based alloy (base material) by machining work, without exerting any adverse effect on the base material. The method of removing the work-affected layer includes a step of dipping a TiAl-based alloy, having a work-affected layer formed on the surface thereof by machining, in an etchant containing predetermined concentrations of hydrofluoric acid and nitric acid. Within the etchant, the concentration of the hydrofluoric acid is not less than 5 g/L and not more than 56 g/L, and the concentration of the nitric acid is selected from within a range from not less than 50 g/L to not more than 260 g/L in accordance with a combination of the concentration of the hydrofluoric acid within the etchant and the etching treatment temperature.

First claim

The invention claimed is:

1. A method of removing a work-affected layer, the method comprising:
a step of dipping a TiAl-based alloy, having the work-affected layer having a thickness of 5 μm to 20 μm formed on a surface thereof by machining, in an etchant consisting of predetermined concentrations of hydrofluoric acid and nitric acid, wherein
the dipping is performed under conditions in which an etching temperature is within a range of 20 to 40° C., an etching time is within a range of 10 to 30 minutes, and an etching rate is within a range of 1 to 15 μm/min, and wherein
within the etchant,
the concentration of the hydrofluoric acid is not less than 5 g/L and not more than 56 g/L, and
the concentration of the nitric acid is selected from within a range from not less than 50 g/L to not more than 260 g/L in accordance with a combination of a concentration of the hydrofluoric acid within the etchant and an etching treatment temperature.

2. The method of removing the work-affected layer according to claim 1 , wherein the TiAl-based alloy has a full lamellar structure.

Assignees

• Mitsubishi Heavy Ind Ltd
• Mitsubishi Heavy Ind Aero Engines Ltd

Inventors

• Kamioka Taisuke

Classifications

• C23F1/20 Primary

  for etching aluminium or alloys thereof · CPC title

• C23G1/106

  refractory metals · CPC title

• C23F1/16 Primary

  Acidic compositions (C23F1/42 takes precedence) · CPC title

• C23F1/26

  for etching refractory metals · CPC title

• C23F3/06

  with acidic solutions · CPC title