Tungsten pentachloride conditioning and crystalline phase manipulation
US-11066310-B2 · Jul 20, 2021 · US
US11577967B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11577967-B2 |
| Application number | US-202017123445-A |
| Country | US |
| Kind code | B2 |
| Filing date | Dec 16, 2020 |
| Priority date | Apr 30, 2018 |
| Publication date | Feb 14, 2023 |
| Grant date | Feb 14, 2023 |
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A process of conditioning tungsten pentachloride to form specific crystalline phases are disclosed. The specific crystalline phases permit stable vapor pressures over extended periods of time during vapor deposition and etching processes.
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We claim: 1. A WCl 5 -containing composition comprising a crystalline phase having approximately 10% weight to approximately 40% weight of phase 1 WCl 5 as determined by X-ray diffraction. 2. The WCl 5 -containing composition of claim 1 , the crystalline phase having approximately 10% weight to approximately 35% weight of Phase 1 WCl 5 . 3. The WCl 5 -containing composition of claim 1 , the crystalline phase having approximately 10% weight to approximately 30% weight of Phase 1 WCl 5 . 4. The WCl 5 -containing composition of claim 1 , the crystalline phase having approximately 10% weight to approximately 25% weight of Phase 1 WCl 5 .
by d-values or two theta-values, e.g. as X-ray diagram · CPC title
Halides · CPC title
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