Device and method for generating a vapor for a CVD or PVD device from multiple liquid or solid source materials

Patent metadata

Field	Value
Publication number	US-10060022-B2
Application number	US-201515318917-A
Country	US
Kind code	B2
Filing date	Jun 16, 2015
Priority date	Jul 1, 2014
Publication date	Aug 28, 2018
Grant date	Aug 28, 2018

Abstract

In a method and a device for generating vapor for a CVD or PVD device, liquid or solid particles of a first source material are fed into a first heat transfer body via a first feed line. The first heat transfer body vaporizes the particles into a first vapor, which is transported by a carrier gas from the first heat transfer body into a second heat transfer body arranged after the first heat transfer body. The first heat transfer body is heated to a first temperature, and the second heat transfer body is heated to a second temperature. Liquid or solid particles of a second source material are fed into a second heat transfer body via a second feed line. The second heat transfer body vaporizes the particles into a second vapor, which is transported along with the first vapor out of the second heat transfer body by the carrier gas.

First claim

The invention claimed is:

1. An apparatus for generating a vapor for a chemical vapor deposition (CVD) or physical vapor deposition (PVD) device, the apparatus comprising:
a first aerosol source ( 15 ) configured to generate a first aerosol flow of particles of a first source material, wherein said particles of the first source material comprise either of liquid particles and solid articles;
a first feed line ( 5 ) configured to feed the first aerosol flow of particles of the first source material from the first aerosol source ( 15 ) into a first heat transfer body ( 1 );
the first heat transfer body ( 1 ) having heat transfer surfaces that are configured to, when heated to a first temperature, vaporize the particles of the first source material into a first vapor, wherein the first vapor is transported out of the first heat transfer body ( 1 ) by a carrier gas in a direction of a flow of the carrier gas;
a second aerosol source ( 16 ) configured to generate a second aerosol flow of particles of a second source material, wherein said particles of the second source material comprise either of liquid particles and solid particles;
a second feed line ( 6 ) configured to feed the second aerosol flow of the particles of the second source material from the second aerosol source ( 16 ) into a second heat transfer body ( 2 ); and
the second heat transfer body ( 2 ) arranged downstream of the first heat transfer body ( 1 ) in the direction of the carrier gas flow, the second heat transfer body ( 2 ) configured to receive the first vapor from the first heat transfer body ( 1 ) and having heat transfer surfaces that are configured to, when heated to a second temperature, vaporize the particles of the second source material into a second vapor, wherein the second vapor along with the first vapor are transported out of the second heat transfer body ( 2 ) by the carrier gas.

2. The apparatus of claim 1 , wherein the heat transfer surfaces of the first heat transfer body ( 1 ) and the second heat transfer body ( 2 ) are formed by surfaces of porous cells of a foam body,
wherein the foam body comprises an electrically conductive material that is heated by passing an electrical current through the foam body,
wherein the foam body has a porosity of 50 to 500 pores per inch, and/or
wherein a proportion of porous areas on a surface of the foam body is greater than 90 percent.

3. The apparatus of claim 1 , further comprising a third heat transfer body ( 3 ) located downstream from the second heat transfer body ( 2 ) in the direction of the carrier gas flow, wherein a clearance space ( 12 ) is situated between the second heat transfer body ( 2 ) and the third heat transfer body ( 3 ).

4. The apparatus of claim 3 , further comprising a preheating body ( 4 ) with which the carrier gas is heated, the preheating body ( 4 ) located upstream from the first heat transfer body ( 1 ) in the direction of the carrier gas flow.

5. The apparatus of claim 4 , wherein the first heat transfer body ( 1 ), the second heat transfer body ( 2 ), and the third heat transfer body ( 3 ), as well as the preheating body ( 4 ) comprise foam bodies with porous cells, the foam bodies being formed from an electrically conductive material that is heated when an electrical current is flowed through the foam bodies.

6. The apparatus of claim 5 ,
wherein the first feed line ( 5 ) opens into an intermediate space ( 10 ) located between the preheating body ( 4 ) and the first heat transfer body ( 1 ), and
wherein the second feed line ( 6 ) opens into an intermediate space ( 11 ) located between the first heat transfer body ( 1 ) and the second heat transfer body ( 2 ).

7. The apparatus of claim 1 , further comprising:
a gas inlet unit ( 14 ) and a susceptor ( 19 ), wherein the first and second vapors are transported by the carrier gas through the gas inlet unit ( 14 ) toward a substrate ( 20 ) resting on the susceptor ( 19 ), on which the first and second vapors condense in response to a chemical reaction or temperature drop; and
a vacuum pump ( 21 ) configured to evacuate an interior of the CVD or PVD device.

8. The apparatus of claim 1 , wherein the first source material and the second source material differ from one another.

9. The apparatus of claim 3 , wherein a gas outlet surface of the third heat transfer body ( 3 ) lies directly opposite a susceptor ( 19 ) carrying a substrate, and comprises a ceiling of a process chamber.

Assignees

• Aixtron Se

Inventors

• Long Michael

Classifications

• C23C14/12

  Organic material · CPC title

• C23C16/45565

  Shower nozzles · CPC title

• C23C16/4483 Primary

  using a porous body · CPC title

• C23C14/26

  by resistance or inductive heating of the source · CPC title

• C23C16/45512 Primary

  Premixing before introduction in the reaction chamber · CPC title