Apparatus and method for production of untwinned YBCO films

Patent metadata

Field	Value
Publication number	US-9450165-B1
Application number	US-201414557147-A
Country	US
Kind code	B1
Filing date	Dec 1, 2014
Priority date	May 23, 2013
Publication date	Sep 20, 2016
Grant date	Sep 20, 2016

Abstract

A method for manufacturing untwinned YBCO film can include the initial the step of depositing YBCO film on a substrate having a first end and second end. A temperature gradient can be established from the first end to the second end, which can establish an oxygen gradient in the YBCO film. A uniaxial pressure can further be established the film, in the same direction as the temperature gradient, form the first end to the second end. When the uniaxial pressure is established simultaneously with the temperature gradient, the result can be an untwinned YBCO film.

First claim

What is claimed is:

1. A method for manufacturing untwinned YBCO film, said method comprising the steps of:
A) depositing a YBCO film having an initial uniform oxygen content on a substrate so that said YBCO film has a first end and a second end;
B) exerting a uniaxial pressure on said film from said first end to said second end;
C) supplying a desired oxygen partial pressure on said YBCO film; and,
D) establishing a first temperature at said first end and a second temperature at said second end, said first temperature being lower than said second temperature to establish an oxygen gradient in said film, said step D) being accomplished simultaneously with said step B) and step C) so that said YBCO film remains untwinned at the completion of said step D).

2. The method of claim 1 , wherein said step D) is accomplished by placing said first end in contact with a first heat source at said first temperature, and by placing said second end in contact with a second heat source at said second temperature.

3. The method of claim 2 , wherein first temperature is less than 350 degrees Centigrade.

4. The method of claim 2 , wherein said second temperature is greater than 375 degrees Centigrade.

5. The method of claim 1 , wherein said step B) is accomplished by urging said first heat source towards said second heat source.

6. The method of claim 1 , wherein said step A), said step B), said step C) and said step D) are accomplished inside a pressure controlled atmospheric chamber.

7. The method of claim 1 , further comprising the steps of:
E) raising said first temperature to substantially equal said second temperature to establish a uniform film temperature for said YBCO film, said step E) being accomplished after the establishment of said oxygen gradient and during the accomplishment of said step D);
F) reducing said first temperature to ambient; and,
G) removing said pressure.

8. The method of claim 1 , wherein said uniaxial pressure is at least 4.5 MPa.

Assignees

• Taylor Benjamin J
• Us Navy

Inventors

• Taylor Benjamin J

Classifications

• H01L39/2464

  Electricity · mapped topic

• H01L39/2496 Primary

  Electricity · mapped topic

• H01L39/126

  Electricity · mapped topic

• H01L39/2454

  Electricity · mapped topic

• H01L39/225

  Electricity · mapped topic