Method of manufacturing spray-dried powders

Patent metadata

Field	Value
Publication number	US-12433307-B2
Application number	US-202318108576-A
Country	US
Kind code	B2
Filing date	Feb 10, 2023
Priority date	Apr 27, 2018
Publication date	Oct 7, 2025
Grant date	Oct 7, 2025

Abstract

Methods and industrial scale set-ups for manufacturing spray-dried powders are provided. During the process, a solvent is used. The process is done batchwise such that the emulsification mass ratio is low when removal of the solvent is started. Preferred solvents are isopropyl acetate and ethyl acetate.

First claim

The invention claimed is:

1. A composition comprising water and particles, wherein
the particles have a core and a shell, wherein the shell comprises at least one emulsifier, and the core comprises at least one fat-soluble compound and at least one solvent, and wherein
the composition has a bimodal particle-solvent-distribution of the particles in the composition.

2. The composition according to claim 1 , wherein the at least one solvent has a boiling point of less than 120° C. at 1013.25 hPa.

3. The composition according to claim 1 , wherein the at least one solvent has a boiling point of less than 100° C. at 1013.25 hPa.

4. The composition according to claim 1 , wherein
the at least one solvent is at least one water immiscible organic solvent selected from the group consisting of dichloromethane, ethyl acetate and isopropyl acetate, and/or wherein
the fat-soluble compound is an edible colorant selected from the group consisting of beta-carotene and lycopene.

5. The composition according to claim 1 , wherein the core of the particles further comprises at least one edible oil.

6. The composition according to claim 5 , wherein the at least one edible oil is a vegetable oil.

7. The composition according to claim 6 , wherein the vegetable oil is corn oil.

8. The composition according to claim 1 , wherein the composition has an emulsification mass ratio which is from 5% to 60%.

9. The composition according to claim 8 , wherein the emulsification mass ratio is 5% to 40%.

10. The composition according to claim 8 , wherein the emulsification mass ratio is 5% to 20%.

11. A method of providing a composition which can be spray-dried, which comprises heating the composition of claim 1 under a pressure of less than 1500 mbar to remove solvent completely or at least partially from the composition.

12. The method according to claim 11 , wherein the solvent removal is accomplished with an evaporator.

13. The method according to claim 12 , wherein the evaporator is a wiped film evaporator.

14. A method of manufacturing a water-dispersible powder comprising the steps of:
(i) providing the composition of claim 1 ;
(ii) removing the solvent completely or at least partially from the composition, and thereafter
(iii) spray-drying the resulting composition obtained in step ii).

15. A powder obtained by the method of claim 14 , wherein the powder comprises, based on the total weight of the powder:
(a) at least one modified starch and at least 10 weight-% of beta-carotene; or
(b) at least one gelatin and at least 15 weight % of beta-carotene; or
(c) at least one modified starch and at least 15 weight-% of lycopene; or
(d) at least one gelatin and at least 15 weight-% of lycopene.

16. A product comprising the powder of claim 15 , wherein the product is selected from the group consisting of a food product, a beverage product, a nutraceutical product, a cosmetic product and a pharmaceutical product.

17. The product according to claim 16 , wherein the product comprises less than 500 ppm of the powder, based on the total weight of the powder.

18. The product according to claim 16 , wherein the product comprises less than 200 ppm of the powder, based on the total weight of the powder.

19. The product according to claim 16 , wherein the product comprises less than 100 ppm of the powder, based on the total weight of the powder.

Assignees

• Dsm Ip Assets Bv

Inventors

• Hunziker André
• Lang Renè
• Schaffner David
• Zwick Thomas

Classifications

• A23B2/93

  Spray drying · CPC title

• B01F2101/06

  Mixing of food ingredients · CPC title

• B01F35/7176

  using pumps · CPC title

• B01F27/27

  Mixers with stator-rotor systems, e.g. with intermeshing teeth or cylinders or having orifices (the stirrers having a central axial inflow and a substantially radial outflow B01F27/81) · CPC title

• B01F23/41

  Emulsifying · CPC title