Agricultural sampling system and related methods

Patent metadata

Field	Value
Publication number	US-12140509-B2
Application number	US-202117144081-A
Country	US
Kind code	B2
Filing date	Jan 7, 2021
Priority date	Jul 10, 2018
Publication date	Nov 12, 2024
Grant date	Nov 12, 2024

Abstract

An automated computer-controlled sampling system and related methods for collecting, processing, and analyzing agricultural samples for various chemical properties such as plant available nutrients. The sampling system allows multiple samples to be processed and analyzed for different analytes or chemical properties in a simultaneous concurrent or semi-concurrent manner. Advantageously, the system can process soil samples in the “as collected” condition without drying or grinding. The system generally includes a sample preparation sub-system which receives soil samples collected by a probe collection sub-system and produces a slurry (i.e. mixture of soil, vegetation, and/or manure and water), and a chemical analysis sub-system which processes the prepared slurry samples for quantifying multiple analytes and/or chemical properties of the sample. The sample preparation and chemical analysis sub-systems can be used to analyze soil, vegetation, and/or manure samples.

First claim

The invention claimed is:

1. A separation device for extracting a test material from an agricultural slurry, the device comprising:
a support housing;
a fluid exchange dock fixedly mounted to the housing, the fluid exchange dock comprising a top surface, a bottom surface, and a plurality of flow passages extending between the top surface and bottom surface;
a motor drive mechanism;
a rotary tube hub coupled to the motor drive mechanism, the tube hub rotatable via operation of the motor drive mechanism;
a plurality of centrifuge tubes pivotably mounted to the tube hub, each of the centrifuge tubes comprising a plurality of fluid conduits each having a respective port arranged on a top surface of the centrifuge tube;
an upper cover and a lower cover coupled to the tube hub, each of the covers comprising a plurality of cutouts each configured to receive a corresponding centrifuge tube when in the horizontal orientation;
wherein the centrifuge tubes are in a vertical orientation when the tube hub is not rotated, and a horizontal orientation when the tube hub is rotated via pivotable movement of each centrifuge tube;
wherein the centrifuge tubes are cleanable and reusable.

2. The separation device according to claim 1 , wherein the fluid exchange dock, the rotary tube hub, or both the fluid exchange dock and rotary tube hub is movable between a docked position such that the fluid exchange dock and rotary tube hub are adjacent and an undocked position such that the fluid exchange dock and rotary tube hub are not adjacent, and wherein when the tube hub is in the docked position, a fluid passageway is formed between each of the flow passages of the fluid exchange dock and a corresponding one of the fluid conduits in the centrifuge tubes.

3. The separation device according to claim 2 , wherein the fluid conduits of each centrifuge tube are arranged to receive slurry via the fluid exchange dock, and wherein the fluid conduits are configured to separate a test material from the slurry when the rotatory hub is rotated in the undocked position.

4. The separation device according to claim 2 , wherein the centrifuge tubes are in a vertical orientation when the tube hub is not rotated, and a horizontal orientation when the tube hub is rotated via pivotable movement of each centrifuge tube.

5. The separation device according to claim 4 , further comprising an upper cover and a lower cover coupled to the tube hub, each of the covers comprising a plurality of cutouts each configured to receive a corresponding centrifuge tube when in the horizontal orientation.

6. The separation device according to claim 1 , wherein the ports on the top surface of each centrifuge tube are arranged in cluster pattern which coincides with a corresponding cluster pattern of fluid passageways formed in the bottom surface of the fluid exchange dock.

7. The separation device according to claim 6 , wherein the fluid conduits of each centrifuge tube are arranged to receive slurry via the fluid exchange dock, and wherein the fluid conduits are configured to separate a test material from the slurry when the rotatory hub is rotated in the undocked position.

8. The separation device according to claim 6 , wherein the centrifuge tubes are in a vertical orientation when the tube hub is not rotated, and a horizontal orientation when the tube hub is rotated via pivotable movement of each centrifuge tube.

9. The separation device according to claim 8 , further comprising an upper cover and a lower cover coupled to the tube hub, each of the covers comprising a plurality of cutouts each configured to receive a corresponding centrifuge tube when in the horizontal orientation.

10. The separation device according to claim 1 , wherein the fluid conduits of each centrifuge tube are arranged to receive slurry via the fluid exchange dock, and wherein the fluid conduits are configured to separate a test material from the slurry when the rotatory hub is rotated in the undocked position.

11. The separation device according to claim 10 , wherein the centrifuge tubes are in a vertical orientation when the tube hub is not rotated, and a horizontal orientation when the tube hub is rotated via pivotable movement of each centrifuge tube.

12. The separation device according to claim 11 , further comprising an upper cover and a lower cover coupled to the tube hub, each of the covers comprising a plurality of cutouts each configured to receive a corresponding centrifuge tube when in the horizontal orientation.

13. A separation device for extracting a test material from an agricultural slurry, the device comprising:
a support housing;
a fluid exchange dock fixedly mounted to the housing, the fluid exchange dock comprising a top surface, a bottom surface, and a plurality of flow passages extending between the top surface and bottom surface;
a motor drive mechanism;
a rotary tube hub coupled to the motor drive mechanism, the tube hub rotatable via operation of the motor drive mechanism;
a plurality of centrifuge tubes pivotably mounted to the tube hub, each of the centrifuge tubes comprising a plurality of fluid conduits each having a respective port arranged on a top surface of the centrifuge tube,
wherein the centrifuge tubes are cleanable and reusable;
wherein the drive mechanism comprises a larger main motor configured to rotate the rotatory hub at high speed for centrifugating the slurry, and a smaller indexing motor to incrementally rotate the tube hub at a low speed to align the centrifuge tubes with the flow passages of the fluid exchange dock.

14. The separation device according to claim 13 , wherein the drive mechanism further comprises a gear train coupling each of the main and indexing motors to a drive shaft coupled to the tube hub.

Assignees

• Prec Planting Llc

Inventors

• Swanson Todd
• Koch Dale
• Harman Reid

Classifications

• G01N35/1072

  with provision for selective pipetting of individual channels · CPC title

• G01N35/08

  using a stream of discrete samples flowing along a tube system, e.g. flow injection analysis · CPC title

• G01N2001/4061

  Solvent extraction · CPC title

• G01N1/4055

  by solubility techniques · CPC title

• G01N1/04

  in the solid state, e.g. by cutting · CPC title