Systems and methods for electroplating sources for alpha spectroscopy

Patent metadata

Field	Value
Publication number	US-10801120-B2
Application number	US-201815881241-A
Country	US
Kind code	B2
Filing date	Jan 26, 2018
Priority date	Jan 26, 2017
Publication date	Oct 13, 2020
Grant date	Oct 13, 2020

Abstract

Disclosed herein are a system and method for electroplating an alpha emitting radionuclide, such as an actinide, for use in alpha spectroscopy. The electrodeposition system for electroplating an alpha emitting radionuclide can include an electroplating cell containing a solution of an electrolyte and the alpha emitting radionuclide, a metal target within the electroplating cell, and a metal anode at a distance from the metal target. The system also includes a platform for supporting the electroplating cell, coupling mechanism connected to the platform, an electric motor on the elastic cushion, and a flywheel with an uneven weight distribution operatively connected to the electric motor. Rotation of the unevenly distributed flywheel generates a vibration in the electroplating cell which dislodges gas bubbles that have formed between the metal target and the metal anode.

First claim

What is claimed is:

1. An electrodeposition system for electroplating an alpha emitting radionuclide comprising:
at least three electroplating cells, each comprising:
a solution comprising an electrolyte and the alpha emitting radionuclide;
a metal target, wherein the metal target is a cathode; and
a metal anode at a distance from the metal target;

a platform operable to support the electroplating cell, the platform comprising a motor recess;
a coupling mechanism coupled to the platform;
a motor housing comprising:
an electric motor; and
a flywheel with an uneven weight distribution coupled to the electric motor, wherein the motor housing is received within the motor recess of the platform, and

a clip bar supported above the platform using at least two shafts, wherein the clip bar comprises at least three clips such that the metal anode is suspended by a wire from a clip on the clip bar above each electroplating cell and placed in the solution within the electroplating cell,
wherein the alpha emitting radionuclide is electroplated on the metal target.

2. The electrodeposition system of claim 1 , further comprising a current source to generate a current between the metal target and the metal anode.

3. The electrodeposition system of claim 1 , wherein the alpha emitting radionuclide is an actinide.

4. The electrodeposition system of claim 1 , wherein the flywheel rotates to generate a vibration of the platform and the at least one electroplating cell through the coupling mechanism.

5. The electrodeposition system of claim 4 , wherein the vibration of the at least one electroplating cell dislodges gas bubbles that have formed between the metal target and the metal anode.

6. The electrodeposition system of claim 1 , wherein the metal target comprises a stainless steel disk.

7. The electrodeposition system of claim 1 , wherein the metal anode comprises platinum.

8. An electrodeposition system for electroplating an alpha emitting radionuclide comprising:
a platform operable to support at least three electroplating cells, the platform comprising a motor recess;
a coupling mechanism coupled to the platform;
an electric motor proximate to the platform;
a flywheel with an uneven weight distribution coupled to the electric motor, wherein the electric motor and flywheel are received within the motor recess; and
a clip bar supported above the platform using at least two shafts, wherein the clip bar comprises at least three clips.

9. The electrodeposition system of claim 8 , wherein the electroplating cell further comprises:
a solution comprising an electrolyte and the alpha emitting radionuclide;
a metal target, wherein the metal target is a cathode; and
a metal anode at a distance from the metal target.

10. The electrodeposition system of claim 9 , wherein the clip bar comprises at least one clip such that the metal anode is suspended by a wire from a clip on the clip bar above each electroplating cell and placed in the solution within the electroplating cell.

Assignees

• Curium Us Llc

Inventors

• Uhland William Claude
• Booij Arend
• Gerritsen Marjolijn

Classifications

• C25D5/20 Primary

  Electroplating using ultrasonic waves · CPC title

• C25D3/54

  of metals not provided for in groups C25D3/04 - C25D3/50 · CPC title

• C25D17/10

  Electrodes {, e.g. composition, counter electrode} · CPC title

• C25D21/10

  Agitating of electrolytes; Moving of racks · CPC title