Sample droplet generation from segmented fluid flow and related devices and methods
US-9543137-B2 · Jan 10, 2017 · US
US9810636B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9810636-B2 |
| Application number | US-201615172886-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 3, 2016 |
| Priority date | Dec 12, 2002 |
| Publication date | Nov 7, 2017 |
| Grant date | Nov 7, 2017 |
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A device for sustaining a plasma in a torch is provided. In certain examples, the device comprises a first electrode configured to couple to a power source and constructed and arranged to provide a loop current along a radial plane of the torch. In some examples, the radial plane of the torch is substantially perpendicular to a longitudinal axis of the torch.
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What is claimed is: 1. A method of detecting an analyte species comprising: introducing an analyte species into a torch having a longitudinal axis along which a flow of gas is introduced during operation of the torch and having a radial plane substantially perpendicular to the longitudinal axis of the torch; providing a loop current along the radial plane of the torch using a device configured to generate an inductively coupled plasma in the torch, the device comprising a first plate electrode configured to couple to a power source; and detecting an optical emission from the analyte species introduced into the plasma generated in the torch. 2. The method of claim 1 , further comprising configuring the device to comprise a second plate electrode configured to couple to a power source, wherein the second plate electrode is constructed and arranged to provide a loop current along the radial plane of the torch. 3. The method of claim 2 , further comprising configuring each of the first and second plate electrodes to comprise a symmetrical inner cross-section. 4. The method of claim 3 , further comprising configuring the symmetrical inner cross-section to be circular. 5. The method of claim 2 , further comprising configuring the device with at least one spacer separating the first plate electrode and the second plate electrode. 6. The method of claim 2 , further comprising configuring the first plate electrode to sustain a substantially symmetrical plasma in the torch. 7. The method of claim 1 , further comprising configuring the device to comprise a radio frequency source in electrical communication with the first plate electrode. 8. The method of claim 7 , further comprising configuring the radio frequency source to provide radio frequencies of about 1 MHz to about 1000 MHz at a power of about 10 Watts to about 10,000 Watts. 9. The method of claim 7 , further comprising configuring the device with a second radio frequency source in electrical communication with the second plate electrode. 10. The method of claim 2 , further comprising configuring the device to comprise a single radio frequency source in electrical communication with the first plate electrode and the second plate electrode. 11. The method of claim 10 , further comprising configuring the single radio frequency source to provide radio frequency energy of about 1 MHz to about 1,000 MHz at a power of about 10 Watts to about 10,000 Watts. 12. The method of claim 2 , further comprising configuring the device with a grounding plate in electrical communication with the first plate electrode and the second plate electrode. 13. The method of claim 1 , further comprising axially detecting the optical emission from the analyte species. 14. The method of claim 1 , further comprising using collection optics to provide the optical emission from the analyte species to a detector. 15. The method of claim 14 , further comprising configuring the detector to spectrally resolve the optical emission from the analyte species. 16. The method of claim 1 , further comprising radially detecting the optical emission from the analyte species. 17. The method of claim 1 , further comprising introducing the analyte species from a sample introduction device fluidically coupled to the torch.
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