Methods for preparing alkali cellulose and cellulose ether

Patent metadata

Field	Value
Publication number	US-9617350-B2
Application number	US-61458706-A
Country	US
Kind code	B2
Filing date	Dec 21, 2006
Priority date	Dec 27, 2005
Publication date	Apr 11, 2017
Grant date	Apr 11, 2017

Abstract

The invention is a method for efficiently preparing alkali cellulose having a uniform alkali distribution therein. More specifically, the invention is a method for preparing alkali cellulose comprising steps of bringing pulp into continuous contact with an alkali metal hydroxide solution in a bucket conveyor type contactor to generate a contact mixture, and draining the contact mixture; a method for preparing a cellulose ether comprising use of the alkali cellulose thus prepared; and an apparatus for preparing alkali cellulose comprising a bucket conveyor contactor comprising at least one inlet port for introducing pulp and an alkali metal hydroxide solution at one end and at least one outlet port for discharging a contact mixture wherein the pulp and the alkali metal hydroxide solution can be moved from one end to the other end while bringing them into contact with each other to generate the contact mixture; and a drainer for separating a cake from the contact mixture discharged from the outlet port.

First claim

The invention claimed is:

1. A method for preparing cellulose ether, comprising the steps of:
bringing pulp into continuous contact with an alkali metal hydroxide solution in a bucket conveyor type contactor to generate a contact mixture;
draining the contact mixture; and
etherifying the alkali cellulose prepared in the draining step with an etherifying agent to produce cellulose ether, and wherein a weight ratio of the alkali metal hydroxide contained by a cake obtained in the draining step to a solid portion contained by the pulp is 0.3 to 1.5.

2. The method for preparing cellulose ether according to claim 1 , wherein a weight ratio of the alkali metal hydroxide contained by a cake obtained in the draining step to a solid portion contained by the pulp is controlled by changing a moving rate or a moving distance of a bucket conveyor of the bucket conveyor type contactor.

3. The method for preparing a cellulose ether according to claim 1 , wherein the pulp is in the form of chips.

4. The method for preparing a cellulose ether according to claim 1 , wherein the bucket conveyor type contactor comprises a bucket conveyor having a moving speed from 0.005 to 5 m/s.

5. The method for preparing a cellulose ether according to claim 1 , wherein the bucket conveyor type contactor comprises a bucket conveyor having a moving distance from 0.5 to 100 m.

6. The method for preparing a cellulose ether according to claim 1 , wherein the pulp and the alkali metal hydroxide solution are introduced successively in the bucket conveyor type contactor.

Assignees

• Narita Mitsuo
• Tabata Masaki
• Yoshida Atsushi
• Umezawa Hiroshi
• Shinetsu Chemical Co

Inventors

• Narita Mitsuo
• Tabata Masaki
• Yoshida Atsushi
• Umezawa Hiroshi

Classifications

• C08B1/10

  Apparatus for the preparation of alkali cellulose · CPC title

• C08B1/08 Primary

  Alkali cellulose · CPC title

• C08B11/193

  Mixed ethers, i.e. ethers with two or more different etherifying groups · CPC title

• C08B11/00 Primary

  Preparation of cellulose ethers {(rendering cellulose suitable for etherification C08B1/06)} · CPC title

• C08B11/16

  Aryl or aralkyl ethers · CPC title