System to continuously produce carbon fiber via microwave assisted plasma processing

Patent metadata

Field	Value
Publication number	US-9427720-B2
Application number	US-201414222827-A
Country	US
Kind code	B2
Filing date	Mar 24, 2014
Priority date	Nov 9, 2005
Publication date	Aug 30, 2016
Grant date	Aug 30, 2016

Abstract

A method for continuously processing carbon fiber including establishing a microwave plasma in a selected atmosphere contained in an elongated chamber having a microwave power gradient along its length defined by a lower microwave power at one end and a higher microwave power at the opposite end of the elongated chamber. The elongated chamber having an opening in each of the ends of the chamber that are adapted to allow the passage of the fiber tow while limiting incidental gas flow into or out of said chamber. A continuous fiber tow is introduced into the end of the chamber having the lower microwave power. The fiber tow is withdrawn from the opposite end of the chamber having the higher microwave power. The fiber to is subjected to progressively higher microwave energy as the fiber is being traversed through the elongated chamber.

First claim

The invention claimed is:

1. An apparatus for continuously processing at least one carbon fiber tow comprising: a chamber having a first end with a first opening to allow said at least one carbon fiber tow to enter said chamber and a second end with a second opening to allow said carbon fiber tow to exit said chamber, said first and said second openings adapted to limit incidental gas flow into or out of said chamber;
a system comprising at least one of pumps or ducts to supply process gas into said chamber; and
a source of microwave power for introducing microwave power into said chamber, said source of microwave power configured to provide a microwave power gradient within said chamber that is sufficient to support a plasma over at least a portion of a length of said chamber, said source of microwave power comprising a microwave generator and a mitered waveguide oriented at an angle with respect to said carbon fiber tow, wherein said microwave power gradient is established in counterflow relationship to the direction of travel of said carbon fiber tow.

2. An apparatus in accordance with claim 1 wherein said chamber comprises a generally cylindrical tube of microwave transparent material disposed within a metal enclosure.

3. An apparatus in accordance with claim 1 wherein each of said first and second openings comprises two eyelets separated by a differential pumping chamber.

4. An apparatus in accordance with claim 1 wherein each of said first and second openings comprises a pair of rollers in mating arrangement, at least one of said rollers having at least one circumferential groove adapted to contain said at least one carbon fiber tow as said at least one carbon fiber tow passes between said rollers.

Assignees

• Ut Battelle Llc
• Ut-Batelle Llc

Inventors

• White Terry L
• Paulauskas Felix L
• Bigelow Timothy S

Classifications

• D01F9/32 Primary

  Apparatus therefor · CPC title

• H01J37/32229

  Waveguides · CPC title

• D06M10/025

  Corona discharge or low temperature plasma · CPC title

• H01J37/32192

  Microwave generated discharge (H01J37/32357, H01J37/32366, H01J37/32394, H01J37/32403 take precedence) · CPC title

• B01J19/126 Primary

  Microwaves · CPC title