Flame-resistant heat treatment furnace

Patent metadata

Field	Value
Publication number	US-9834869-B2
Application number	US-201514853138-A
Country	US
Kind code	B2
Filing date	Sep 14, 2015
Priority date	Jul 28, 2011
Publication date	Dec 5, 2017
Grant date	Dec 5, 2017

Abstract

To perform a flame-resistant treatment on a precursor fiber strand by sending hot air to a heat treatment chamber ( 2 ) through a hot air blowing nozzle ( 4 ) in a direction parallel to a running direction of a precursor fiber strand ( 10 ). The hot air blowing from the hot air blowing nozzle ( 4 ) passes through a porous plate and a rectifying member that satisfy the following conditions (1) to (4), wherein the conditions are set as follows: (1) A/B≧4.0; (2) 0.15≦α≦0.35; (3) 0≦B−d≦20; and (4) 80% or more of an area of one opening of the porous plate when causing facing surfaces of the porous plate and the rectifying member to overlap each other is included in one opening of the rectifying member, A indicating a hot air passage distance (mm) of the rectifying member, B indicating a horizontal maximum distance (mm) of one opening of the rectifying member, α indicating a rate of hole area of the porous plate, and d indicating an equivalent diameter (mm) of the porous plate. Accordingly, it is possible to provide a parallel stream type flame-resistant heat treatment furnace having exhibiting the uniform heat transfer performance throughout the inside of the heat treatment chamber by preventing the blockage of the nozzle caused by a silicone compound generated inside the heat treatment chamber even in the hot air blowing nozzle having a simple structure.

First claim

The invention claimed is:

1. A flame-resistant heat treatment furnace comprising:
a heat treatment chamber configured to cause hot air to flow in the same direction as a running direction of a precursor fiber strand, the direction opposite to the running direction of the precursor fiber strand, or both, and heats the precursor fiber strand;
a hot air blowing nozzle configured to introduce the hot air into the heat treatment chamber; and
a hot air suctioning nozzle that is installed at a position away from the hot air blowing nozzle and suctions the hot air,
wherein the hot air blowing nozzle comprises a porous plate and a rectifying member that satisfy conditions (1) to (3):
(1) A/B ≧4.0;
(2) 0.15 ≧α0.35; and
(3) 0≦B-d ≦20;

where
A is a hot air passage distance (mm) of the rectifying member,
B is a horizontal maximum distance (mm) of one opening of the rectifying member,
α is a rate of hole area of the porous plate, and
d is an equivalent diameter (mm) of the porous plate.

2. The flame-resistant heat treatment furnace according to claim 1 , wherein the equivalent diameter d (mm) of the porous plate satisfies a condition (5) of 10≦d ≦20.

3. The flame-resistant heat treatment furnace according to claim 1 ,
wherein an opening pitch P 1 (mm) of openings of the porous plate and an opening pitch P 2 (mm) of openings of the rectifying member satisfy a condition (6) of 0.995×P 2 ≦P 1 ≦1.005×P 2 .

4. The flame-resistant heat treatment furnace according to claim 1 ,
wherein a distance y (mm) between the facing opening surfaces of the porous plate and the rectifying member satisfies a condition (7) of 0≦y ≦7.

5. The flame-resistant heat treatment furnace according to claim 1 ,
wherein a cross-sectional shape of the rectifying member in the hot air passage direction is a lattice shape or a honeycomb shape.

6. The flame-resistant heat treatment furnace according to claim 1 ,
wherein the porous plate and the rectifying member are connected to each other by a positioning member.

7. The flame-resistant heat treatment furnace according to claim 1 ,
wherein the porous plate and the rectifying member are detachable from each other.

8. The flame-resistant heat treatment furnace according to claim 1 ,
wherein the hot air blowing nozzle comprises a direction changing plate that changes a hot air flow direction, and satisfies a condition (8) of (x/L)<0.030 and a condition (9) of (w/L)<0.50,
where x is a distance (mm) between the porous plate at a nozzle tip and the direction changing plate at the nozzle tip, L is an entire length (mm) of the hot air blowing nozzle in the depth direction, and w is an inlet width (mm) of the hot air blowing nozzle.

9. The flame-resistant heat treatment furnace according to claim 1 ,
wherein an installation position of the porous plate is adjustable.

10. A method of manufacturing a carbon fiber comprising:
heating a carbon fiber precursor strand within a flame-resistant heat treatment furnace according to claim 1 .

11. The flame-resistant heat treatment furnace according to claim 1 , wherein the hot air blowing nozzle comprises a porous plate and a rectifying member that further satisfy condition (4):
(4) 80% or more of an area of one opening of the porous plate when causing facing surfaces of the porous plate and the rectifying member to overlap each other is included in one opening of the rectifying member.

12. The flame-resistant heat treatment furnace according to claim 1 , wherein
10≧ A/B 4.0.  (1)

13. The flame-resistant heat treatment furnace according to claim 1 , wherein
7≧ A/B 4.0.  (1)

14. The flame-resistant heat treatment furnace according to claim 1 , wherein
5≧ A/B 4.0.  (1)

15. The flame-resistant heat treatment furnace according to claim 1 , wherein
0.15≦α≦0.30.  (2)

16. The flame-resistant heat treatment furnace according to claim 1 , wherein
0.15≦α≦0.25.  (2)

17. The flame-resistant heat treatment furnace according to claim 1 , wherein
0.17≦α≦0.35.  (2)

18. The flame-resistant heat treatment furnace according to claim 1 , wherein
0.17≦α≦0.30.  (2)

19. The flame-resistant heat treatment furnace according to claim 1 , wherein
0.17≦α≦0.25.  (2)

20. The flame-resistant heat treatment furnace according to claim 1 , wherein the heat treatment chamber causes the hot air to flow in the same direction as the running direction of the precursor fiber strand and in the direction opposite to the running direction of the precursor fiber strand.

Assignees

• Mitsubishi Chem Corp

Inventors

• Kaji Satoshi
• Yamamoto Nobuyuki
• Kawamura Atsushi
• Tomobe Hitoshi

Classifications

• D01F9/14

  by decomposition of organic filaments · CPC title

• D06B5/06

  through yarns, threads or filaments · CPC title

• D01F9/32 Primary

  Apparatus therefor · CPC title

• F26B13/001

  Drying and oxidising yarns, ribbons or the like · CPC title

• D02J13/001

  in a tube or vessel · CPC title