Silicon carbide powder production method

Patent metadata

Field	Value
Publication number	US-9399583-B2
Application number	US-201214368452-A
Country	US
Kind code	B2
Filing date	Dec 28, 2012
Priority date	Dec 28, 2011
Publication date	Jul 26, 2016
Grant date	Jul 26, 2016

Abstract

A method for preparing silicon carbide powder according to an embodiment of the present disclosure includes the steps of: mixing a silicon (Si) source with a carbon (C) source including a solid carbon source or an organic carbon compound, and a silicon dioxide (SiO2) source, to form a mixture; and allowing the mixture to react, wherein the molar ratio of silicon dioxide in the silicon dioxide source to the sum of silicon in the silicon source and carbon in the carbon source is 0.01:1 to 0.3:1.

First claim

What is clamed is:

1. A method for preparing silicon carbide powder, the method comprising the steps of:
mixing a silicon source, a carbon source, and a silicon dioxide source to form a mixture; and
allowing the mixture to react to form the silicon carbide powder,
wherein the molar ratio of silicon dioxide (SiO 2 ) in the silicon dioxide source to the sum of silicon (Si) in the metal silicon source and carbon (C) in the carbon source is 0.01:1 to 0.3:1.

2. The method of claim 1 , wherein the molar ratio of silicon dioxide in the silicon dioxide source to the sum of silicon in the silicon source and carbon in the carbon source is 0.1:1 to 0.2:1.

3. The method of claim 1 , wherein the mixture is heated at a temperature between 1400° C. and 1700° C.

4. The method of claim 1 , wherein the carbon source includes a solid carbon source, wherein the solid carbon source is selected from the group consisting of carbon black, carbon nanotubes and fullerene.

5. The method of claim 1 , wherein the carbon source includes an organic carbon compound, wherein the organic carbon compound is selected from the group consisting of phenol resin, franc resin, xylene resin, polyimide, polyurethane, polyacrylonitrile, polyvinyl alcohol, cellulose, pitch, tar and sugar.

6. The method of claim 1 , wherein the silicon dioxide source is selected from the group consisting of silica sol, silicon dioxide, fine silica and quartz powder.

7. The method of claim 1 , wherein the molar ratio of metal silicon in the silicon source to carbon in the carbon source is 1:0.8 to 1:1.2.

8. The method of claim 1 , wherein the molar ratio of metal silicon in the silicon source to carbon in the carbon source is 1:0.9 to 1:1.1.

Assignees

• Lg Innotek Co Ltd

Inventors

• Kim Byung Sook

Classifications

• C01B32/984 Primary

  Preparation from elemental silicon · CPC title

• C01P2004/62

  Submicrometer sized, i.e. from 0.1-1 micrometer · CPC title

• Y10T428/2982

  Particulate matter [e.g., sphere, flake, etc.] · CPC title

• C01B32/97

  Preparation from SiO or SiO2 · CPC title

• C01B33/113

  Silicon oxides; Hydrates thereof {(preparing monoxide by reduction of siliceous material C01B33/182)} · CPC title