Method and arrangement for feedback based control in chemical refining of wood

Patent metadata

Field	Value
Publication number	US-12508736-B2
Application number	US-202017426586-A
Country	US
Kind code	B2
Filing date	Jan 27, 2020
Priority date	Jan 29, 2019
Publication date	Dec 30, 2025
Grant date	Dec 30, 2025

Abstract

Method and control system are provided for controlling values of process parameters of a pretreatment process of wood particles. A sampler is used to obtain a sample of a product flow of said pretreatment process after said wood particles have undergone steam explosion in a hemihydrolysis reactor. A particle measurement device is used to measure one or more characteristics of particles in said sample and to produce one or more pieces of measurement information indicative of the measured characteristics. Said one or more pieces of measurement information are used to select one or more values of one or more of said process parameters.

First claim

The invention claimed is:

1 . A method for controlling values of process parameters of a pretreatment process of wood particles, the method comprising:
sampling a product flow of said pretreatment process after said wood particles have undergone steam explosion in a hemihydrolysis reactor to obtain a sample; measuring one or more characteristics of particles in said sample to produce one or more pieces of measurement information indicative of the measured characteristics; and selecting, using said one or more pieces of measurement information, to select one or more values of one or more of said process parameters, wherein said measuring comprises using a particle measurement device to measure shive content in the sample, and wherein said selecting comprises selecting at least a value of a second residence time of said product flow in an impregnating vessel that precedes said hemihydrolysis reactor in said pretreatment and selecting at least one of the process parameters selected from: a third residence time of said product flow in a first soaking silo that precedes said impregnating vessel in said pretreatment, or a fifth residence time of said product flow in a second soaking silo that is between said impregnating vessel and said hemihydrolysis reactor in said pretreatment, and wherein said particle measurement device is configured to measure shive content in said sample as one of said one or more characteristics of particles, the measured shive content is compared to a default shive content to produce at least a second piece of said one or more pieces of measurement information, and value for at least one of said third residence time or said fifth residence time is selected to intensify impregnation of wood particles in said first or second soaking silo respectively in response to said second piece of measurement information indicating larger than default shive content.

2 . A method according to claim 1 , wherein said one or more of said process parameters comprise at least one of:
a temperature in said hemihydrolysis reactor, a pressure difference between an input and output of said hemihydrolysis reactor, a first residence time of said product flow in said hemihydrolysis reactor.

3 . A method according to claim 2 , wherein:
said particle measurement device is configured to measure particle size or particle size distribution in said sample as one of said one or more characteristics of particles, the measured particle size or particle size distribution is compared to a default size or a default size distribution respectively to produce at least a first piece of said one or more pieces of measurement information, and value for at least one of said temperature, said pressure difference, or said first residence time is increased to increase reaction severity in said hemihydrolysis reactor in response to said first piece of measurement information indicating larger than default particles in said sample.

4 . A method according to claim 2 , wherein:
said particle measurement device is configured to measure particle size or particle size distribution in said sample as one of said one or more characteristics of particles, the measured particle size or particle size distribution is compared to a default size or a default size distribution respectively to produce at least a first piece of said one or more pieces of measurement information, and value for at least one of said temperature, said pressure difference, or said first residence time is decreased to decrease reaction severity in said hemihydrolysis reactor in response to said first piece of measurement information indicating smaller than default particles in said sample.

5 . A method according to claim 1 , wherein:
said particle measurement device is configured to measure shive content in said sample as one of said one or more characteristics of particles, the measured shive content is compared to a default shive content to produce at least a second piece of said one or more pieces of measurement information, and value for at least one of said second residence time or said acid content is selected to intensify impregnation of wood particles in said impregnating vessel in response to said second piece of measurement information indicating larger than default shive content.

6 . A method according to claim 1 , wherein said one or more of said process parameters comprise at least one of:
rotation rate of a mixer that succeeds said hemihydrolysis reactor in said pretreatment, or a sixth residence time of said product flow in said mixer.

7 . A method according to claim 6 , wherein:
said particle measurement device is configured to measure homogeneity in said sample as one of said one or more characteristics of particles, the measured homogeneity is compared to a default homogeneity to produce at least a third piece of said one or more pieces of measurement information, and value for at least one of said rotation rate or said sixth residence time is increased to intensify homogenizing of said product flow in said mixer in response to said third piece of measurement information indicating lower than default homogeneity.

8 . A method according to claim 1 , wherein said particle measurement device is configured to directly measure presence and size of particles in said sample with an optical measurement method.

9 . A method according to claim 1 , wherein said particle measurement device is configured to measure one or more characteristics of particles in said sample through an indirect measurement method not measuring directly the presence and size of particles in the sample.

10 . A method according to claim 9 , wherein said particle measurement device is configured to measure drainability of said sample.

11 . A method according to claim 1 , comprising:
measuring content of one or more chemical constituents in said product flow after wood particles in said product flow have undergone said steam explosion, and to produce one or more pieces of chemical constituent information indicative of the measured content, and selecting one or more values of said one or more process parameters using said one or more pieces of chemical constituent information.

12 . A method according to claim 11 , wherein said chemical constituents comprise at least one of: furfural, lactic acid.

13 . A control system for controlling values of process parameters of a pretreatment process of wood particles, the control system comprising:
a sampler; one or more measurement information inputs coupled to said sampler for receiving measurement information indicative of measured characteristics of samples taken by said sampler of a product flow in said pretreatment process; one or more control information outputs for setting values for said one or more process parameters of said pretreatment process, and a processing engine coupled to said measurement information inputs and said control information outputs; wherein said processing engine is programmed to
obtain a sample of said product flow of said pretreatment process using said sampler after said wood particles have undergone steam explosion in a hemihydrolysis reactor,
measure one or more characteristics of particles in said sample using a particle measurement device, wherein said one or more characteristics of particles include at least shive content in the sample, and to produce one or more pieces of measurement information indicative of the measured characteristics; and
select one or more values of one or more of said process parameters using said one or more pieces of measurement information,
wherein said using of said one

Assignees

• Upm Kymmene Corp

Inventors

• Turunen Sami
• Laitila Mika
• Tamper Juha

Classifications

• D21B1/04

  by dividing raw materials into small particles, e.g. fibres (breaking-up or cutting wood or the like by dry methods B27L; mechanical separation of fibres from plant material D01B1/00; hackling or heckling machines D01B5/00) · CPC title

• D21B1/36

  Explosive disintegration by sudden pressure reduction · CPC title

• G01N2015/0042

  Investigating dispersion of solids · CPC title

• G01N2001/105

  from high-pressure reactors or lines · CPC title

• G01N33/0098

  Plants or trees (wood G01N33/46) · CPC title