Method for recovering hydrolysate

Patent metadata

Field	Value
Publication number	US-9663896-B2
Application number	US-201514930701-A
Country	US
Kind code	B2
Filing date	Nov 3, 2015
Priority date	Nov 7, 2014
Publication date	May 30, 2017
Grant date	May 30, 2017

Abstract

The method is for producing pulp. More particularly, a displacement batch cooking process comprises recovery of a first treatment liquid by draining of the digester, preferably not using a displacement liquid. The method may preferably be used in a prehydrolysis step, wherein the recovery of the by-products is improved. In the recovery step, after the target P-factor in the prehydrolysis stage is reached, the hydrolysate is withdrawn by draining in at least one phase obtaining a strong first liquid and thereafter any residual hydrolysate may be displaced.

First claim

We claim:

1. A method for recovering a first treatment liquid in a displacement batch pulping process in a digester filled with comminuted cellulosic material and equipped with a bottom, a top and a middle liquid exchange position, said method comprising:
filling the digester with a first treatment liquid during or after a steam prehydrolyzina step wherein the process continues by,
after filling the digester with the first treatment liquid during or after the prehydrolyzing step, subjecting the first treatment liquid contained in the digester to circulation within the digester by withdrawing the first treatment liquid from the middle liquid exchange position and reintroducing the withdrawn first treatment liquid to a top and a bottom of the digester, passing the first treatment liquid through the comminuted cellulosic material disposed in the digester at least once, and washing out the carbohydrates dissolved in the hydrolysate;
in a first draining phase, draining the first treatment liquid from the digester via one of the middle or bottom liquid exchange positions to obtain a strong first liquid; and
sending at least a part of the strong first liquid to a dedicated processing position either for use in a different phase of the batch pulping process or for further processing wherein at least a part the strong first liquid is used for recovering by-products
wherein the first treatment liquid is used during prehydrolysis of the comminuted cellulosic material to produce an acidic hydrolysate containing the carbohydrates dissolved in the hydrolysate during the prehydrolysis and wherein after the first draining phase at least a part of the strong first liquid is sent to further processing in a sugar recovery process by using the carbohydrates dissolved in the hydrolysate, and
wherein the first draining phase is assisted by displacing steam or gases through the digester, the steam or gases being added via the top liquid exchange position and wherein a pressure and a temperature of the strong first liquid is maintained.

2. The method for recovering a first treatment liquid according to claim 1 , wherein the first draining phase comprises the step of withdrawing the strong first liquid through the middle liquid exchange position and in final phases displacing a residual strong first liquid kept in the digester below the middle liquid exchange position via a displacement by using water added to the bottom liquid exchange position to displace the residual strong first liquid out through the middle liquid exchange position.

3. The method for recovering a first treatment liquid according to claim 1 , wherein the strong first liquid is kept at a prehydrolysis temperature and stored in a dedicated accumulator tank before processing the strong first liquid in a sugar recovery process by using the carbohydrates dissolved in the hydrolysate.

4. A method for recovering a first treatment liquid in a displacement batch pulping process in a digester filled with comminuted cellulosic material and equipped with a bottom, a top and a middle liquid exchange position, said method comprising:
filling the digester with a first treatment liquid during or after a steam prehydrolyzing step wherein the process continues by,
after filling the digester with the first treatment liquid during or after the prehydrolyzing step, subjecting the first treatment liquid contained in the digester to circulation within the digester by withdrawing the first treatment liquid from the middle liquid exchange position and reintroducing the withdrawn first treatment liquid to a top and a bottom of the digester, passing the first treatment liquid through the comminuted cellulosic material disposed in the digester at least once, and washing out the carbohydrates dissolved in the hydrolysate;
in a first draining phase, draining the first treatment liquid from the digester via one of the middle or bottom liquid exchange positions to obtain a strong first liquid; and
sending at least a part of the strong first liquid to a dedicated processing position either for use in a different phase of the batch pulping process or for further processing wherein at least a part the strong first liquid is used for recovering by-products;
wherein the first treatment liquid is used during prehydrolysis of the comminuted cellulosic material to produce an acidic hydrolysate containing the carbohydrates dissolved in the hydrolysate during the prehydrolysis and wherein after the first draining phase at least a part of the strong first liquid is sent to further processing in a sugar recovery process by using the carbohydrates dissolved in the hydrolysate; and
wherein after the first draining phase, the digester is filled with water until the comminuted cellulosic material is submerged in the water, the water is subjected to circulation,
in a second draining phase, the water is drained from the digester via one of the middle or bottom liquid exchange positions to obtain a weak first liquid and
at least a part of the weak first liquid is sent to a dedicated second accumulator to be used as being part of the first treatment liquid ahead of prehydrolysis in a subsequent batch cycle.

Assignees

• Valmet Oy

Inventors

• Rosengren Ismo
• Kuusisto Petteri
• Lammi Lari

Classifications

• D21C11/00

  Regeneration of pulp liquors {or effluent waste waters} · CPC title

• D21C11/0007

  Recovery of by-products, i.e. compounds other than those necessary for pulping, for multiple uses or not otherwise provided for (volatile compounds obtained by decomposition of spent liquors in order to regenerate them D21C11/125; compounds obtained by fractionating the liquors in order to regenerate them D21C11/0042) · CPC title

• D21C7/12

  Devices for regulating or controlling · CPC title

• D21C1/02 Primary

  with water or steam · CPC title

• D21C1/00

  Pretreatment of the finely-divided materials before digesting (of waste paper D21C5/02) · CPC title