Method for producing aluminum nitride powder, aluminum nitride powder, and package

Patent metadata

Field	Value
Publication number	US-12486171-B2
Application number	US-202117797741-A
Country	US
Kind code	B2
Filing date	Jan 22, 2021
Priority date	Feb 6, 2020
Publication date	Dec 2, 2025
Grant date	Dec 2, 2025

Abstract

To produce aluminum nitride in the form of a lump that can easily be broken down by light pulverization, which could not be obtained by a conventional combustion synthesis method. A method for producing aluminum nitride powder by a combustion synthesis method using a metallic aluminum powder, characterized in that a powder mixture in which an aluminum nitride powder having an average primary particle diameter of 3 μm or less as a diluent is mixed with a metallic aluminum powder in a ratio of 150 to 400 parts by mass of the aluminum nitride powder relative to 100 parts by mass of the metallic aluminum powder, is ignited to combust in a nitrogen atmosphere.

First claim

The invention claimed is:

1 . A method for producing an aluminum nitride powder by a combustion synthesis method, the method comprising:
mixing an aluminum nitride powder having an average primary particle diameter of 3 μm or less as a diluent with a metallic aluminum powder in a ratio of 150 to 400 parts by mass of the aluminum nitride powder relative to 100 parts by mass of the metallic aluminum powder to form a powder mixture, igniting the powder mixture to combust in a nitrogen atmosphere to obtain an aluminum nitride lump, disaggregating the aluminum nitride lump to form the aluminum nitride powder, wherein the aluminum nitride powder comprises aggregated particles of aluminum nitride primary particles having an average primary particle diameter of 3 μm or less, wherein the aggregated particles have an average particle diameter that exceeds the average primary particle diameter but is 4 μm to 20 μm, wherein a part of the aluminum nitride powder obtained after disaggregating is used as the diluent when the process is repeated.

2 . The method for producing an aluminum nitride powder according to claim 1 , wherein the metallic aluminum powder has an average particle diameter of 1 μm or greater and less than 10 μm.

3 . The method for producing an aluminum nitride powder according to claim 1 , wherein the powder mixture has a bulk density in a range of 0.6 to 0.9 g/cm 3 .

4 . The method for producing an aluminum nitride powder according to claim 1 , wherein the powder mixture is charged in a layered state into a reactor in a shape of a box, wherein the reactor is made of a heat resistant material and has a bottom area of 0.3 m 2 or greater, and the powder mixture is ignited to combust the metallic aluminum powder.

5 . The method for producing an aluminum nitride powder according to claim 4 , wherein a heat-insulating layer is formed on a bottom face of the reactor.

Assignees

• Tokuyama Corp

Inventors

• Yamamoto Yasuyuki
• Satou Hideki

Classifications

• C01P2006/80

  Compositional purity · CPC title

• C01P2004/61

  Micrometer sized, i.e. from 1-100 micrometer · CPC title

• C01B21/0722 Primary

  Preparation by direct nitridation of aluminium · CPC title