Oil compositions

Patent metadata

Field	Value
Publication number	US-12349693-B2
Application number	US-201816196040-A
Country	US
Kind code	B2
Filing date	Nov 20, 2018
Priority date	Feb 10, 2011
Publication date	Jul 8, 2025
Grant date	Jul 8, 2025

Abstract

A refined oil composition having a reduced 3-MCPD ester and/or glycidyl ester content and methods of preparation thereof.

First claim

The invention claimed is:

1. A process for the production of a refined oil having a reduced 3-MCPD ester and glycidyl ester content, the process comprising:
subjecting an oil to bleaching and deodorization consisting of:
(a) bleaching the oil with activated bleaching clay to form a first bleached oil,
(b) deodorizing the first bleached oil at a temperature in a range of 200° C. to 280° C. to form a first deodorized oil,
(c) bleaching the first deodorized oil with activated bleaching clay to form a second bleached oil, and
(d) deodorizing the second bleached oil at a temperature of 130° C. to 160° C.;

wherein:
the bleaching and deodorization reduce the combined 3-MCPD ester and glycidyl ester content of the refined oil to no more than 5 ppm and reduce free fatty acid (FFA) content of the refined oil to less than 0.1% by weight; and
the oil is palm oil containing 3-MCPD ester and glycidyl ester.

2. The process according to claim 1 wherein the bleaching (c) is carried out at a temperature below 80° C.

3. The process according to claim 1 further comprising one or more alkali treatment steps.

4. The process according to claim 1 , wherein the combined 3-MCPD ester and glycidyl ester content is no more than 3 ppm.

5. The process according to claim 1 , wherein the combined 3-MCPD ester and glycidyl ester content is no more than 2 ppm.

6. The process according to claim 1 further comprising a degumming step prior to subjecting the oil to bleaching and deodorization steps.

7. The process according to claim 1 further comprising one or more of the following additional steps selected from neutralization, dewaxing, fractionation, hydrogenation, interesterification, blending with two or more different refined oils, or combinations thereof.

8. The process according to claim 1 , wherein the refined oil has a combined 3-MCPD ester and glycidyl ester content that is at least 50% lower than that of an oil obtained by standard physical refining, wherein standard physical refining comprises degumming, bleaching, and deodorization.

9. The process according to claim 1 , wherein the refined oil has a combined 3-MCPD ester and glycidyl ester content that is at least 90% lower than that of an oil obtained by standard physical refining, wherein standard physical refining comprises degumming, bleaching, and deodorization.

10. The process according to claim 1 , wherein the combined 3-MCPD ester and glycidyl ester content of the refined oil is no more than 1 ppm.

11. The process according to claim 1 , wherein the combined 3-MCPD ester and glycidyl ester content of the refined oil is from 0.3 ppm to 1 ppm.

Assignees

• Cargill Inc

Inventors

• Brùse Falk
• Kruidenberg Marcus Bernardus

Classifications

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title

• C11B3/12

  by distillation · CPC title

• C11B3/10

  by adsorption · CPC title

• C11B3/001 Primary

  by a combination of two or more of the means hereafter · CPC title

• A23L2/52 Primary

  Adding ingredients (adding preservatives A23B70/10) · CPC title