Polycrystalline diamond compacts

Patent metadata

Field	Value
Publication number	US-12297153-B2
Application number	US-202016880131-A
Country	US
Kind code	B2
Filing date	May 21, 2020
Priority date	Oct 3, 2008
Publication date	May 13, 2025
Grant date	May 13, 2025

Abstract

Embodiments of the invention relate to polycrystalline diamond (“PCD”) exhibiting enhanced diamond-to-diamond bonding. In an embodiment, PCD includes a plurality of diamond grains defining a plurality of interstitial regions. A metal-solvent catalyst occupies at least a portion of the plurality of interstitial regions. The plurality of diamond grains and the metal-solvent catalyst collectively exhibit a coercivity of about 115 Oersteds (“Oe”) or more and a specific magnetic saturation of about 15 Gauss·cm 3 /grams (“G·cm 3 /g”) or less. Other embodiments are directed to polycrystalline diamond compacts (“PDCs”) employing such PCD, methods of forming PCD and PDCs, and various applications for such PCD and PDCs in rotary drill bits, bearing apparatuses, and wire-drawing dies.

First claim

The invention claimed is:

1. A polycrystalline diamond compact, comprising:
a polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween and defining a plurality of interstitial regions, wherein the plurality of diamond grains exhibit an average grain size of about 5 μm to about 50 μm;
wherein the polycrystalline diamond table includes an unleached portion including:
a metal-solvent catalyst occupying at least a portion of the plurality of interstitial regions, the metal-solvent catalyst present in the unleached portion in an amount of about 3 weight % to about 7.5 weight %;
a portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a coercivity of about 115 Oersteds (“Oe”) to about 250 Oe; and
the portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a specific magnetic saturation of about 5 Gauss·cm 3 /grams (“G·cm 3 /g”) to about 15 G·cm 3 /g;
wherein the polycrystalline diamond table exhibits a G ratio of at least about 4.0×106, and
a substrate bonded to the polycrystalline diamond table.

2. The polycrystalline diamond compact of claim 1 , wherein the plurality of diamond grains exhibit an average grain size of about 10 μm to about 18 μm.

3. The polycrystalline diamond compact of claim 1 , wherein the coercivity of the portion of the plurality of diamond grains and the metal-solvent catalyst collectively is about 115 Oe to about 175 Oe.

4. The polycrystalline diamond compact of claim 1 , wherein the coercivity of the portion of the plurality of diamond grains and the metal-solvent catalyst collectively is about 155 Oe to about 175 Oe.

5. The polycrystalline diamond compact of claim 1 , wherein the magnetic saturation of the portion of the plurality of diamond grains and the metal-solvent catalyst collectively is about 10 G·cm 3 /g to about 15 G·cm 3 /g.

6. The polycrystalline diamond compact of claim 1 , wherein the portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a specific permeability of about 0.10 G·cm 3 /g·Oe or less.

7. The polycrystalline diamond compact of claim 1 , wherein the specific permeability of the portion of the plurality of diamond grains and the metal-solvent catalyst collectively is about 0.06 G·cm 3 /g·Oe to about 0.09 G·cm 3 /g·Oe.

8. The polycrystalline diamond compact of claim 1 , wherein the polycrystalline diamond table includes an unleached volume exhibiting a G ratio of at least about 15.0×10 6 .

9. The polycrystalline diamond compact of claim 1 , wherein the polycrystalline diamond table is formed in a high-pressure/high-temperature process at a cell pressure of at least 7.5 GPa.

10. The polycrystalline diamond compact of claim 1 , wherein the polycrystalline diamond table, when unleached, exhibits a thermal stability, as determined by a distance cut, prior to failure, in a vertical lathe test of at least about 1300 m.

11. The polycrystalline diamond compact of claim 1 , wherein the polycrystalline diamond table is formed from only a single layer of polycrystalline diamond extending from the upper exterior surface to the substrate.

12. A polycrystalline diamond compact, comprising:
a polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween and defining a plurality of interstitial regions, wherein the plurality of diamond grains exhibit an average grain size of about 5 μm to about 30 μm;
wherein the polycrystalline diamond table is formed in a high-pressure/high-temperature process at a cell pressure of at least 7.5 Gpa
wherein the polycrystalline diamond table includes an unleached volume exhibiting a G ratio of at least about 4.0×10 6 ;
wherein the polycrystalline diamond table includes an unleached portion including:
a metal-solvent catalyst occupying at least a portion of the plurality of interstitial regions, the metal-solvent catalyst present in the unleached portion in an amount of about 3 weight % to about 7.5 weight %;
a portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a coercivity of about 115 Oersteds (“Oe”) to 250 Oe;
the portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a specific magnetic saturation of about 5 Gauss·cm 3 /grams (“G·cm 3 /g”) to 15 G·cm 3 /g; and
a substrate bonded to the polycrystalline diamond table.

13. A polycrystalline diamond compact, comprising:
a polycrystalline diamond table including a plurality of diamond grains exhibiting diamond-to-diamond bonding therebetween and defining a plurality of interstitial regions, wherein the plurality of diamond grains exhibit an average grain size of about 5 μm to about 20 μm; and
a substrate bonded to the polycrystalline diamond table
wherein the polycrystalline diamond table includes an unleached volume, the unleached volume exhibiting a G ratio of at least about 8.0×10 6 ;
wherein the polycrystalline diamond table includes an unleached portion includes:
a metal-solvent catalyst occupying at least a portion of the plurality of interstitial regions, the metal-solvent catalyst present in the unleached portion in an amount of about 3 weight % to about 7.5 weight %;
a portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a coercivity of about 115 Oersteds (“Oe”) to 250 Oe;
the portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a specific magnetic saturation of about 10 Gauss·cm 3 /grams (“G·cm 3 /g”) to 15 G·cm 3 /g; and
the portion of the plurality of diamond grains and the metal-solvent catalyst collectively exhibiting a specific permeability of about 0.060 G·cm 3 /g·Oe to about 0.090 G·cm 3 /g·Oe.

Assignees

• Us Synthetic Corp

Inventors

• Bertagnolli Kenneth E
• Qian Jiang
• Wiggins Jason
• Vail Michael
• Mukhopadhyay Debkumar

Classifications

• E21B10/567

  with preformed cutting elements mounted on a distinct support, e.g. polycrystalline inserts · CPC title

• C04B2237/363

  Carbon · CPC title

• C04B2237/36

  Non-oxidic · CPC title

• B24D18/0009

  using moulds or presses · CPC title

• G01N27/72

  by investigating magnetic variables · CPC title