Experimental device and method for testing foam fluid properties and defoaming separation effects

Patent metadata

Field	Value
Publication number	US-12146818-B2
Application number	US-202017774037-A
Country	US
Kind code	B2
Filing date	Nov 3, 2020
Priority date	Nov 4, 2019
Publication date	Nov 19, 2024
Grant date	Nov 19, 2024

Abstract

An experimental device and method for testing foam fluid properties and defoaming separation effects, the experimental device including a foam generation module configured to generate a foam fluid, an experimental loop configured to transport the foam fluid and enable the foam fluid to sufficiently develop in a loop, a foam property test module configured to test foam fluid properties, a foam separation processing module configured to separate foam from fluid and gas, and a defoaming result evaluation module configured to test and evaluate defoaming results. In the method, different foam fluids are generated in the foam generation module and are transported to the foam property test module and different foam separation processing modules through the experimental loop, and the foam properties of the foam fluids and defoaming separation effects are measured by the foam property test module and the defoaming result evaluation module connected to the foam separation processing module.

First claim

What is claimed is:

1. An experimental device for testing foam fluid properties and defoaming separation effects, comprising a foam generation module, an experimental loop, a foam property test module, a foam separation processing module and a defoaming result evaluation module, wherein
a tail end of the foam generation module is connected to the experimental loop, different ratios of oil-water and CO 2 gas are mixed in the foam generation module to form a foam fluid, and the foam fluid is transported into the experimental loop;
the foam fluid is developed inside the experimental loop and is respectively transported to the foam property test module and the foam separation processing module at a tail end of the experimental loop;
the foam property test module receives the foam fluid that is sufficiently developed in the experimental loop, and analyzes a foam volume, a half foam life period and a foam quality of the foam fluid that is sufficiently developed;
the foam separation processing module receives the foam fluid that is sufficiently developed in the experimental loop, and separates the foam fluid that is sufficiently developed into gas and liquid; and
the foam separation processing module is provided with the defoaming result evaluation module, and the defoaming result evaluation module analyzes the gas separated by the foam separation processing module to obtain a liquid content in the gas, a droplet size in the gas and an oil content in the gas;
the foam generation module comprises an oil-water mixing kettle, a CO 2 gas cylinder and a foam generation device, and the foam generation device is respectively connected to the oil-water mixing kettle and the CO 2 gas cylinder through two connecting pipelines; and
the connecting pipeline from the oil-water mixing kettle to the foam generation device is sequentially provided with a second centrifugal pump and a first flow meter according to a liquid flow direction, the connecting pipeline from the CO 2 gas cylinder to the foam generation device is sequentially provided with a gas storage tank and a first gas-phase flow meter according to a gas flow direction, and the oil-water mixed liquid in the oil-water mixing kettle and the CO 2 gas in the CO 2 gas cylinder enter the inside of the foam generation device through a liquid-phase pipeline inlet at a bottom of the foam generation device and a gas-phase pipeline inlet on a side wall of the foam generation device;
the tail end of the experimental loop is sequentially provided with a first bypass pipeline and a second bypass pipeline according to a flow direction of the foam fluid, and a main pipeline at the tail end of the experimental loop is connected to the foam separation processing module;
the foam property test module comprises an analysis tank, a lower end of the analysis tank is provided with a liquid-phase outlet, a side wall of the analysis tank is provided with a gas outlet, a first absorption box and a first sampling valve are sequentially installed outward from the gas outlet, a water-absorbing and oil-absorbing material is placed in the first absorption box, and the first sampling valve is connected to a gas collection bag through a pipeline;
the foam separation processing module comprises a horizontal separator, the horizontal separator is a visualized tank body, and a side wall of the tank body is provided with standard scales;
a lower end of the horizontal separator is provided with a liquid-phase outlet, the periphery of the lower end of the horizontal separator is coated with a second heating jacket, an upper end of the horizontal separator is provided with a gas-phase outlet, and the gas-phase outlet on the horizontal separator is connected to the defoaming result evaluation module;
the upper end of the horizontal separator is also provided with a pipe column type cyclone separator, a lower end of the pipe column type cyclone separator is communicated to the horizontal separator, the main pipeline at the tail end of the experimental loop is also provided with a third bypass pipeline, the third bypass pipeline is connected to the pipe column type cyclone separator, and the foam fluid that is sufficiently developed enters the pipe column type cyclone separator through the third bypass pipeline of the experimental loop, and then flows into the horizontal separator from the pipe column type cyclone separator;
a foam fluid inlet of the pipe column type cyclone separator is provided with a gas-phase outlet, and the gas-phase outlet of the pipe column type cyclone separator is communicated to the gas-phase outlet of the horizontal separator through a gas pipe; and

the gas-phase outlet of the horizontal separator is connected to the defoaming result evaluation module;
the defoaming result evaluation module comprises a droplet size observation window and a second absorption box at a tail end of the droplet size observation window;
a water-absorbing and oil-absorbing material is placed in the second absorption box.

2. The experimental device for testing foam fluid properties and defoaming separation effects according to claim 1 , wherein a stainless steel wire mesh with mesh holes is arranged inside the foam generation device; and
the gas-phase pipeline inlet and the liquid-phase pipeline inlet of the foam generation device are arranged at 90° in space.

3. The experimental device for testing foam fluid properties and defoaming separation effects according to claim 1 , wherein the first bypass pipeline is connected to the atmosphere, and configured to discharge the foam fluid that is insufficiently developed in the experimental loop; and
the second bypass pipeline is connected to the foam property test module, and configured to discharge the foam fluid that is sufficiently developed in the experimental loop into the foam property test module.

4. The experimental device for testing foam fluid properties and defoaming separation effects according to claim 1 , wherein the analysis tank is a visualized tank body, and a side wall of the tank body is provided with standard scales.

5. The experimental device for testing foam fluid properties and defoaming separation effects according to claim 1 , wherein the gas separated by the foam separation processing module sequentially passes through the droplet size observation window and the second absorption box, an outlet of the second absorption box is provided with two pipelines, the first pipeline is communicated to the atmosphere, the first pipeline is provided with a second gas-phase flow meter, the second pipeline is provided with a second sampling valve, and the second sampling valve is connected to the gas collection bag through a gas pipe.

6. The experimental device for testing foam fluid properties and defoaming separation effects according to claim 1 , wherein a kettle cover of the oil-water mixing kettle is provided with a liquid-phase backflow inlet, and the remaining liquid in the foam property test module and the foam separation processing module circularly flows back into the oil-water mixing kettle.

7. An experimental method using the experimental device for testing foam fluid properties and defoaming separation effects according to claim 5 , comprising:
step 1: preparation stage: introducing CO 2 gas into the entire experimental device to remove impurities in the pipe;
step 2: foam fluid generation stage: introducing the CO 2 gas with a required gas flow rate into the foam generation device, transporting the oil-water mixed liquid with a required liquid flow rate into the foam generation device at the same time, and mixing the CO 2 gas and the oil-water mixed liquid in the foam generation device to generate a foam fluid;
step 3: foam fluid transportation stage: transporting the foam fluid into

Assignees

• Univ China Petroleum East China

Inventors

• Li Yuxing
• Hu Qihui
• Liu cuiwei
• Wang Wuchang
• Meng Lingya
• Wang Jinghan
• Ma Hongtao

Classifications

• G01N2013/0241

  bubble, pendant drop, sessile drop methods · CPC title

• B01D19/0063

  Regulation, control including valves and floats (for construction and details of valves F16K) · CPC title

• B01D19/0057

  the centrifugal movement being caused by a vortex, e.g. using a cyclone, or by a tangential inlet · CPC title

• B01F23/235

  for making foam · CPC title

• G01N2015/0046

  in gas, e.g. smoke · CPC title