Apparatus and methods for determining surface wetting of material under subterranean wellbore conditions
US-9829421-B2 · Nov 28, 2017 · US
US9518907B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9518907-B2 |
| Application number | US-201414157211-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 16, 2014 |
| Priority date | Jan 16, 2014 |
| Publication date | Dec 13, 2016 |
| Grant date | Dec 13, 2016 |
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Apparatus and methods to determine structural integrity of composites are described herein. One described example method for determining sufficiency of structural integration of a composite structure for an aircraft includes applying a fluid droplet to a surface of the composite structure, determining a three-dimensional contact angle between the surface and a portion of the droplet, comparing the three-dimensional contact angle to a threshold angle, and determining whether the structural integration of the composite structure is sufficient based on the comparison.
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What is claimed is: 1. A method for determining a bond strength of a composite structure for an aircraft, the method comprising: applying a fluid droplet to a surface of the composite structure; determining a three-dimensional contact angle between the surface and a portion of the droplet; comparing the three-dimensional contact angle to a threshold angle; and determining whether the bond strength is sufficient based on the comparison, wherein a value of the three-dimensional contact angle of less than a predetermined threshold angle of about 10 degrees between the surface of the composite structure and the portion of the fluid droplet is indicative of the composite structure having sufficient bond strength to provide a pre-predetermined load bearing capacity. 2. The method as defined in claim 1 , further comprising selecting the composite structure for integration into an assembly when the bond strength is sufficient. 3. The method as defined in claim 1 , further comprising approving the composite structure when the bond strength is sufficient after integration of the composite structure into an assembly. 4. The method as defined in claim 1 , wherein the three-dimensional contact angle being less than the threshold angle indicates sufficient bond strength of the composite structure. 5. The method as defined in claim 1 , wherein the three-dimensional contact angle being greater than the threshold angle indicates insufficient bond strength of the composite structure. 6. The method as defined in claim 1 , wherein determining the three-dimensional contact angle further comprises measuring a diameter and volume of the droplet. 7. The method as defined in claim 1 , wherein the portion of the droplet comprises a head or a tail of the droplet. 8. The method as defined claim 7 , wherein the composite structure comprises bismaleimide, epoxy, polyamide, or thermoplastic. 9. The method as defined in claim 1 , wherein the threshold angle is calculated based on a pre-determined load bearing capacity. 10. The method as defined in claim 9 , wherein the threshold angle calculation is calculated using an equation including a component of the surface tension of the surface due to vapor gaseous phase of the droplet in equilibrium. 11. The method as defined in claim 1 , wherein applying the fluid droplet comprises use of a pipette or ballistic deposition. 12. An aircraft component that requires fewer fasteners, comprising: an external skin having a bonded composite structure, defining a skin surface area of an aircraft; a support frame; and an adhesive applied to the composite structure to attach the external skin to the support frame, wherein the composite structure has sufficient bond strength to enable adhesive attachment of the external skin to the support frame with less than 0.50 fasteners to couple the skin and the support frame per square-foot of the skin surface area, where a three-dimensional contact angle between the composite structure and a portion of a fluid droplet applied to the surface of the composite structure is less than a pre-determined threshold angle of about 10 degrees is indicative of sufficient bond strength. 13. The apparatus as defined in claim 12 , wherein the composite structure is outboard of an aircraft. 14. The apparatus as defined in claim 12 , wherein the portion of the fluid droplet defining the three-dimensional contact angle from the composite structure comprises one or more of a head, a tail, or a mid-section of a loft of the droplet. 15. A tangible machine readable medium having instructions stored thereon, which when executed, cause a machine to: determine a three-dimensional contact angle of a droplet placed onto a surface of a composite structure based on a measured diameter and volume of the droplet; compare the three-dimensional contact angle to a threshold angle of about 10 degrees, wherein the three-dimensional contact angle being less than the threshold angle indicates sufficient bond strength of the composite structure, and wherein the three-dimensional contact angle being greater than the threshold angle indicates insufficient bond strength of the composite structure; and output whether the composite structure has sufficient bond strength. 16. The machine readable medium as defined in claim 15 , which when executed, further cause a machine to measure the volume and the diameter of the droplet. 17. The machine readable medium as defined in claim 15 , which when executed, further cause a machine to calculate an intermolecular surface tension of the composite structure. 18. The machine readable medium as defined in claim 17 , wherein the calculated intermolecular surface tension is determined using an equation including a component of the surface tension of the surface due to vapor gaseous phase of the droplet in equilibrium. 19. The machine readable medium as defined in claim 17 , which when executed, further cause a machine to output one or more of the intermolecular surface tension and a factor of safety based on the intermolecular surface tension. 20. The machine readable medium as defined in claim 15 , which when executed, further cause a machine to generate structural specifications for approval when the three-dimensional contact angle indicates sufficient bond strength.
Construction, shape, or attachment of separate skins, e.g. panels · CPC title
by measuring contact angle · CPC title
of aircraft wings or blades · CPC title
Investigating surface tension of liquids · CPC title
Construction or attachment of skin panels · CPC title
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