Agricultural sampling system and related methods

Patent metadata

Field	Value
Publication number	US-12104988-B2
Application number	US-202117144116-A
Country	US
Kind code	B2
Filing date	Jan 7, 2021
Priority date	Jul 10, 2018
Publication date	Oct 1, 2024
Grant date	Oct 1, 2024

Abstract

An automated computer-controlled sampling system and related methods for collecting, processing, and analyzing agricultural samples for various chemical properties such as plant available nutrients. The sampling system allows multiple samples to be processed and analyzed for different analytes or chemical properties in a simultaneous concurrent or semi-concurrent manner. Advantageously, the system can process soil samples in the “as collected” condition without drying or grinding. The system generally includes a sample preparation sub-system which receives soil samples collected by a probe collection sub-system and produces a slurry (i.e. mixture of soil, vegetation, and/or manure and water), and a chemical analysis sub-system which processes the prepared slurry samples for quantifying multiple analytes and/or chemical properties of the sample. The sample preparation and chemical analysis sub-systems can be used to analyze soil, vegetation, and/or manure samples.

First claim

The invention claimed is:

1. An automated inline processing system for collecting, preparing, and analyzing an agricultural sample, the system comprising:
a portable vehicle configured to travel through an agricultural field for collecting the sample;
a sample collector first sub-system comprising a sample collection probe configured and operable to collect a sample from the agricultural field, the sample collection probe being mounted on the portable vehicle;
a water source;
a sample preparation second sub-system comprising a mixer fluidly coupled to the water source and including a cavity which receives the sample from the sample collection probe, the mixer comprising a rotatable mixing element configured and operable to prepare a slurry from mixing the sample and water from the water source;
the mixer being configured and operable to discharge the slurry through a discharge flow conduit;
an extractant source;
the sample preparation second sub-system further comprising an extractant pump fluidly coupled to the extractant source, the extractant pump being configured and operable to pump the extractant into the discharge flow conduit at an injection point to mix the extractant with the slurry to extract a test material from the slurry via a chemical reaction;
an analysis third sub-system comprising an analysis cell fluidly coupled to the discharge flow conduit downstream of the injection point, the analysis cell being configured and operable to analyze the test material and measure an analyte present therein;
a programmable controller operably and communicably linked to the sample collection probe, mixer, extractant pump, and analysis cell via wired or wireless communication links;
wherein the controller is configured to collect and process the sample in sequence in real time from collection by the sample collection probe to analysis by the analysis cell.

2. The system according to claim 1 , wherein the mixer, extractant pump, and analysis cell are mounted on the portable vehicle.

3. The system according to claim 1 , wherein the second sub-system comprises a weighing device which is configured and operable to receive and weigh the slurry.

4. The system according to claim 2 , wherein the second sub-system comprises a weighing device which is configured and operable to receive and weigh the slurry.

5. The system according to claim 3 , wherein the weighing device comprises a helically-shaped weigh coil which receives the slurry.

6. The system according to claim 5 , further comprising a support structure and wherein the weigh coil is supported in a cantilevered manner from the support structure.

7. An automated inline processing system for collecting, preparing, and analyzing an agricultural sample comprising solid particles, the system comprising:
a portable vehicle configured to travel through an agricultural field for collecting the sample;
a sample collection probe mounted on the portable vehicle, the sample collection probe being configured and operable to collect a sample from the agricultural field;
a source of water mounted on the portable vehicle;
a mixer mounted on the portable vehicle, the mixer fluidly coupled to the source of water via a flow conduit and fluidly coupled to the sample collection probe via process tubing, the sample collection probe being configured and operable to transfer the sample to the mixer;
the mixer comprising a vessel including a cavity configured to receive the sample from the sample collection probe and water from the source of water, the mixer comprising a rotatable mixing element configured and operable to mix the water and sample which forms a sample slurry;
the mixer being configured and operable to discharge the slurry through a discharge flow conduit;
an extractant system comprising a source of extractant and an extractant pump fluidly coupled to the source of extractant, the extractant pump being configured and operable to pump the extractant into the slurry in the discharge flow conduit at an injection point forming an extractant slurry mixture, the extractant having a chemical composition operable to extract a test material from the slurry via a chemical reaction;
an analysis cell fluidly coupled to the discharge flow conduit downstream of the injection point, the analysis cell being configured and operable to analyze the test material and measure an analyte present therein;
a programmable controller operably and communicably linked to the sample collection probe, mixer, extractant pump, and analysis cell via wired or wireless communication links;
wherein the controller is configured to collect and process the sample in sequence in real time from collection by the sample collection probe to analysis by the analysis cell.

8. The system according to claim 7 , further comprising a centrifuge fluidly coupled between fluidly coupled to the discharge flow conduit and arranged to receive the extractant slurry mixture, the centrifuge being configured and operable to centrifugate the extractant slurry mixture to separate the solid particles of the sample from the extractant slurry mixture thereby forming a clear supernatant.

9. The system according to claim 8 , wherein the centrifuge comprises a plurality of pivotably movable centrifuge tubes coupled to a rotary tube hub, at least one of the centrifuge tubes being fluidly coupled to the discharge flow conduit to receive the extractant slurry mixture.

10. The system according to claim 9 , wherein the centrifuge tubes are movable from a vertical position when the rotary tube hub is stationary, to a horizontal position when the rotary tube hub is rotating.

11. The system according to claim 8 , further comprising a supernatant pump configured and operable to extract and pump the supernatant from the centrifuge to the analysis cell.

Assignees

• Prec Planting Llc

Inventors

• Swanson Todd
• Koch Dale
• Levy Kent
• O'Neall Matthew
• Harman Reid
• Schaefer Timothy
• Vaccari Adam

Classifications

• G01N35/1072

  with provision for selective pipetting of individual channels · CPC title

• G01N35/08

  using a stream of discrete samples flowing along a tube system, e.g. flow injection analysis · CPC title

• G01N2001/4061

  Solvent extraction · CPC title

• G01N1/4055

  by solubility techniques · CPC title

• G01N1/04

  in the solid state, e.g. by cutting · CPC title