Method for extracting coenzyme q10 and phospholipid from coenzyme q10 fermentation bacterial powder
US-2020399667-A1 · Dec 24, 2020 · US
US11820786B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11820786-B2 |
| Application number | US-202217664980-A |
| Country | US |
| Kind code | B2 |
| Filing date | May 25, 2022 |
| Priority date | May 20, 2015 |
| Publication date | Nov 21, 2023 |
| Grant date | Nov 21, 2023 |
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Embodiments of the present invention provide a method, comprising obtaining a lecithin-containing material, in some aspects derived from a crude refining stream, comprising 20-80 wt % acetone insoluble matter, 1-30 wt % free fatty acid, and less than 10 wt % water, adding a fatty acid or carboxylic source to the lecithin-containing material to obtain a lecithin fatty acid blend or lecithin carboxylic acid blend and incorporating the blend into asphalt or oil field applications.
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We claim: 1. A method, comprising: (a) obtaining a lecithin-containing material, comprising 20-80 wt % acetone insoluble matter, 1-30 wt % free fatty acid, and less than 10 wt % water; (b) adding a fatty acid source to the lecithin-containing material to obtain a lecithin fatty acid blend; and (c) incorporating the lecithin fatty acid blend into asphalt or oil field applications. 2. The method of claim 1 , wherein the lecithin-containing material comprises less than 5 wt % water. 3. The method of claim 1 , wherein the lecithin-containing material comprises less than 2 wt % water. 4. The method of claim 1 , wherein the lecithin-containing material comprises less than 1 wt % water. 5. The method of claim 1 , wherein the lecithin-containing material comprises 10-20 wt % free fatty acid. 6. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 100 to 15000 cP. 7. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 2000 to 12000 cP. 8. The method of claim 1 , wherein the lecithin fatty acid blend has a Brookfield Viscosity at 25° C. of about 5000 to 9000 cP. 9. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 1 to 100 mg KOH/g. 10. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 50 to 90 mg KOH/g. 11. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 10 to 70 mg KOH/g. 12. The method of claim 1 , wherein the lecithin fatty acid blend has an acid value of 15 to 40 mg KOH/g. 13. The method of claim 1 , wherein the lecithin-containing material is derived from a crude refining stream. 14. The method of claim 13 , wherein the crude refining stream is a plant-based gum. 15. The method of claim 14 , wherein the plant-based gum is selected from the group consisting of corn gum, soybean gum, and canola gum. 16. The method of claim 13 , wherein the crude refining stream is soapstock. 17. The method of claim 13 , wherein the crude refining stream is derived from animal sources. 18. The method of claim 1 , wherein the fatty acid source is selected from the group consisting of deodorized distillate streams, vegetable oils, and recovered corn oil streams and derivatives thereof. 19. The method of claim 1 , wherein the asphalt is polyphosphoric acid modified asphalt. 20. The method of claim 1 , wherein the asphalt application is an anti-strip or a compaction aid additive.
Extraction or purification by physical or chemical treatment of natural phosphatides; Preparation of compositions containing phosphatides of unknown structure · CPC title
containing phosphorus · CPC title
Compositions of oils, fats or waxes; Compositions of derivatives thereof · CPC title
containing surfactants · CPC title
from soap stock · CPC title
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