Method for purification of lecithin

Patent metadata

Field	Value
Publication number	US-10442827-B2
Application number	US-201715833299-A
Country	US
Kind code	B2
Filing date	Dec 6, 2017
Priority date	Oct 30, 2013
Publication date	Oct 15, 2019
Grant date	Oct 15, 2019

Abstract

The present invention relates to a method for the purification of lecithin, comprising the steps of (a) mixing lecithin with active carbon to form a dispersion; then (b) mixing an organic solvent into the dispersion; then (c) separating the active carbon and contaminants from the lecithin preferably through gravitational forces. The invention further relates to a lecithin substantially free of contaminants, and a food or feed product comprising said lecithin.

First claim

The invention claimed is:

1. A method for the purification of lecithin, the method comprising:
(a) mixing lecithin with active carbon to form a dispersion;
(b) mixing an organic solvent into the dispersion; and
(c) separating the active carbon and contaminants from the lecithin to achieve a purified lecithin;
wherein the purified lecithin contains less than 10 μg/kg wet weight of benzo(a)pyrene, benzo(a)anthracene, benzo(b)fluoranthene and chrysene.

2. The method of claim 1 , wherein the purified lecithin contains ethanol at a level of less than 5000 ppm or contains hexane at a level of less than 10 ppm.

3. The method of claim 1 , wherein the purified lecithin has a turbidity of less than 100 nephelometric turbidity units.

4. The method of claim 1 , wherein the purified lecithin contains at most 0.1% hexane insoluble.

5. The method of claim 1 wherein, in step (a), lecithin is at a temperature of from 10° C. to 90° C.

6. The method of claim 1 , wherein the active carbon is mixed with the lecithin for a period of from 1 hour to 120 hours.

7. The method of claim 1 , wherein the active carbon is powder active carbon.

8. The method of claim 1 , wherein the active carbon is mixed with lecithin at a level of from 0.01% to 3% by weight of the lecithin.

9. The method of claim 1 , wherein the organic solvent is mixed into the dispersion at a ratio of lecithin to organic solvent of from 3:1 to 1:20.

10. The method of claim 1 , wherein the active carbon and contaminants are separated by means of a disk stack centrifuge or a decanter.

11. The method of claim 1 , wherein the organic solvent is at a temperature of from 1° C. above its melting point to 1° C. below its boiling point.

12. The method of claim 1 , wherein the organic solvent is separated from the lecithin.

13. The method of claim 1 , further comprising the step of filtrating the lecithin.

14. A sunflower lecithin in liquid form showing a turbidity of less than 100 nephelometric turbidity units (NTU) when measured at 1 wt % lecithin in hexane, said lecithin having an amount of hexane insoluble (HI) in solution of at most 0.005% when measured at a concentration of 20% lecithin in hexane and having a poly-aromatic hydrocarbons (PAH4) content of less than 10 μg/kg wet weight of PAH4, wherein PAH4is a combination of benzo(a)pyrene, 5 benzo(a)anthracene, benzo(b)fluoranthene and chrysene.

15. The lecithin of claim 14 comprising ethanol or hexane, wherein the ethanol level is less than 5000 ppm and the hexane level is less than 10 ppm.

16. A food or feed product comprising the lecithin of claim 14 .

17. The food or feed product of claim 16 , wherein the food product is an infant food product.

Assignees

• Cargill Inc

Inventors

• Stevens Robert
• Van Denderen Jos

Classifications

• C07F9/103 Primary

  Extraction or purification by physical or chemical treatment of natural phosphatides; Preparation of compositions containing phosphatides of unknown structure · CPC title

• C07F9/10

  Phosphatides, e.g. lecithin · CPC title

• C11B3/10

  by adsorption · CPC title

• A23J7/00

  Phosphatide compositions for foodstuffs, e.g. lecithin · CPC title

• A23L33/40

  Complete food formulations for specific consumer groups or specific purposes, e.g. infant formula · CPC title