Method for evaluating degree of cleanliness of recycled material, method for manufacturing recycled material, and method for manufacturing recycled pulp fiber

Patent metadata

Field	Value
Publication number	US-11802373-B2
Application number	US-201816771736-A
Country	US
Kind code	B2
Filing date	Dec 20, 2018
Priority date	Dec 20, 2017
Publication date	Oct 31, 2023
Grant date	Oct 31, 2023

Abstract

The objective of the present disclosure is to provide a method for easily evaluating the degree of cleanliness of recycled material derived from used sanitary products. The evaluation method according to the present disclosure has the following configuration. This method for evaluating a degree of cleanliness of recycled material derived from used sanitary products includes: a preparation step of preparing a dispersed aqueous solution in which the recycled material is dispersed in water; a separation step of subjecting the dispersed aqueous solution to centrifugal separation to separate the dispersed aqueous solution into a liquid component and a solid component; and a measuring step of measuring the concentration of protein in the liquid component using a protein measuring means.

First claim

The invention claimed is:

1. A method of manufacturing a recycled material from an used sanitary product, wherein the method includes:
a recycling step of forming the recycled material from the used sanitary product and
an evaluation step of evaluating the cleanliness of the recycled material by the following method

a provision step of providing a dispersed aqueous solution having the recycled material dispersed in water,
a separation step of separating the dispersed aqueous solution into a liquid component and a solid component by centrifugal separation, and

a measurement step of measuring a concentration of protein in the liquid component by protein measurement means.

2. A method of manufacturing recycled pulp fibers from a pulp fiber-containing used sanitary product, wherein the method includes:
a supply step of supplying an aqueous solution containing the pulp fibers to a driving fluid supply port of a treatment tank provided with an ejector, the ejector comprising the driving fluid supply port, a mixed fluid discharge port connected to the treatment tank, and a suction fluid supply port between them, while supplying ozone to the suction fluid supply port, and
a recycled pulp fiber-forming step of forming recycled pulp fibers by discharging a liquid mixture formed by mixing of the aqueous solution and the ozone in the ejector into the treatment solution in the treatment tank from the mixed fluid discharge port, and decomposing the protein-containing components in the pulp fibers such that an aqueous dispersion comprising the recycled pulp fibers dispersed at a solid concentration of 5.0 mass % contains protein at a concentration of 60 μg/mL or lower, as measured by a Modified Lowry method.

3. The method according to claim 2 , wherein the used sanitary product further includes a superabsorbent polymer, the aqueous solution further includes the superabsorbent polymer in the supply step, and the superabsorbent polymer is further decomposed in the recycled pulp fiber-forming step.

4. The method according to claim 3 , wherein the manufacturing method includes, before the supply step, an inactivating step of inactivating the superabsorbent polymer by an acidic aqueous solution.

5. The method according to claim 2 , wherein an ozone concentration in the solution is 1 to 50 ppm by mass.

6. The method according to claim 2 , wherein an ozone concentration in the solution is 40 to 200 g/m 3 .

Assignees

• Unicharm Corp

Inventors

• Imai Shigeo
• Wada Mitsuhiro

Classifications

• B09B3/70

  Chemical treatment, e.g. pH adjustment or oxidation (involving an extraction step B09B3/80) · CPC title

• B09B3/35

  Shredding, crushing or cutting · CPC title

• D21C5/022 Primary

  Chemicals therefor · CPC title

• G01N33/343 Primary

  Paper pulp · CPC title

• C08J11/16

  by treatment with inorganic material (C08J11/14 takes precedence) · CPC title