Process for manufacturing recycled pulp from used sanitary goods

Patent metadata

Field	Value
Publication number	US-10280560-B2
Application number	US-201415024713-A
Country	US
Kind code	B2
Filing date	Sep 4, 2014
Priority date	Oct 30, 2013
Publication date	May 7, 2019
Grant date	May 7, 2019

Abstract

Provided is a process for recovering pulp fiber from used sanitary goods which contain both pulp fiber and a superabsorbent polymer and producing a recycled pulp which contains little ash and which is reusable for sanitary goods. This process comprises: a calcium treatment step for treating used sanitary goods with a water-soluble calcium compound and thereby conducting the dehydration of a superabsorbent polymer contained in the used sanitary goods; a disintegration step for applying a physical force to the used sanitary goods to disintegrate the used sanitary goods into pulp fiber and other materials; a separation step for separating the pulp fiber from a pulp fiber/other materials mixture which has been formed in the disintegration step; a disinfecting step using a disinfectant; and a citric acid treatment step for subjecting the separated pulp fiber to treatment with an aqueous citric acid solution at an acidic pH.

First claim

The invention claimed is:

1. A process for manufacturing recycled pulp that is reusable for sanitary goods, by recovering pulp fiber from used sanitary goods containing pulp fiber and a superabsorbent polymer, the process comprising:
a calcium treatment step in which used sanitary goods are treated with a water-soluble calcium compound to dehydrate the superabsorbent polymer in the used sanitary goods,
a disintegration step in which the used sanitary goods are subjected to physical force to disintegrate the used sanitary goods into pulp fiber and other materials,
a separation step in which pulp fiber is separated from a mixture of pulp fiber and other materials generated in the disintegration step,
a disinfection step using a disinfectant, and
a citric acid treatment step in which the separated pulp fiber is treated with an aqueous citric acid solution at an acidic pH.

2. The process according to claim 1 , wherein the pH in the citric acid treatment step is in a range of 2 to 6.

3. The process according to claim 1 , further comprising a rinsing step carried out after the citric acid treatment step.

4. The process according to claim 1 , wherein the citric acid treatment step removes calcium compounds and other metal compounds residing in the pulp fiber by forming chelates of citric acid with calcium and other metals.

5. A process of manufacturing recycled pulp that is reusable for sanitary goods, by recovering pulp fiber from used sanitary goods containing pulp fiber and a superabsorbent polymer, the process comprising:
treating used sanitary goods with a water-soluble calcium compound to dehydrate the superabsorbent polymer in the used sanitary goods,
disintegrating the used sanitary goods by physical force into pulp fiber and other materials,
separating the pulp fiber from a mixture of the pulp fiber and the other materials generated in the disintegrating,
disinfecting with a disinfectant, and
treating the separated pulp fiber with an aqueous citric acid solution at an acidic pH, wherein
the disintegrating is carried out after, before or simultaneously with the treating with the water-soluble calcium compound,
the separating is carried out after the disintegrating,
the disinfecting is carried out immediately after the calcium treatment step, or immediately after the disintegration step, or immediately after the separation step, or immediately after the citric acid treatment step, or simultaneously with the calcium treatment step, or simultaneously with the disintegration step, or simultaneously with the separation step, or simultaneously with the citric acid treatment step, and
the treating with the aqueous citric acid solution is carried out after the separating.

6. The process according to claim 5 , wherein the pH in the citric acid treatment step is in a range of 2 to 6.

7. The process according to claim 5 , further comprising a rinsing step carried out after the citric acid treatment step.

8. The process according to claim 5 , wherein the citric acid treatment step removes calcium compounds and other metal compounds residing in the pulp fiber by forming chelates of citric acid with calcium and other metals.

Assignees

• Unicharm Corp

Inventors

• Yamaguchi Masashi
• Konishi Takayoshi

Classifications

• B29L2031/4878

  Diapers, napkins · CPC title

• D21C9/00

  After-treatment of cellulose pulp, e.g. of wood pulp, or cotton linters {; Treatment of dilute or dewatered pulp or process improvement taking place after obtaining the raw cellulosic material and not provided for elsewhere (polysaccharides, derivatives thereof C08B; paper-making D21B - D21H)} · CPC title

• D21C5/02 Primary

  Working-up waste paper (mechanical part D21B1/08, D21B1/32) · CPC title

• D21C3/04

  with acids, acid salts or acid anhydrides {(D21C3/003 and D21C3/222 take precedence)} · CPC title

• Y02W30/622

  Cross-Sectional Technologies · mapped topic