Minimally invasive microsampler for intact removal of surface deposits and substrates

Patent metadata

Field	Value
Publication number	US-11573156-B2
Application number	US-201916248132-A
Country	US
Kind code	B2
Filing date	Jan 15, 2019
Priority date	Jan 15, 2019
Publication date	Feb 7, 2023
Grant date	Feb 7, 2023

Abstract

A method of sampling a multi-layered material and a micro-sampling tool are described. The sampling method includes penetrating a top surface of a material in a component of interest with a micro-cutting tool to a predetermined depth sufficient to include each layer of the multi-layered material and a portion of the base, without cutting through the full depth of the base, under-cutting from the depth of penetration through the base to define a micro-sample of the multi-layered material, and removing the micro-sample with each layer of the multi-layered material intact. The micro-sampler includes a cutting tool calibrated to cut to a depth no greater than 2 mm, and in some aspects, no greater than 200 microns into a multi-layered material, the material having a top surface and a metallic or ceramic base and a container for removing and storing a micro-sample cut from the material with each layer of the multi-layered material and a portion of the base intact.

First claim

What is claimed is:

1. A method of sampling a multi-layered material having a top surface and a metallic or ceramic base comprising:
penetrating a top surface of the material with a micro-cutting tool to a predetermined depth sufficient to include each layer of the multi-layered material and a portion of the base, without cutting through the full depth of the base;
under-cutting from the depth of penetration through the base to define a micro-sample of the multi-layered material; and
removing the micro-sample with each layer of the multi-layered material intact,
wherein the top surface is curved and the penetrating and under-cutting are performed simultaneously through an arc of the curve,
wherein the micro-cutting tool comprises an end mill,
wherein the end mill comprises a major shank having a top end and a bottom end, a minor shank having a top end and a bottom end, the top end of the minor shank extending from the bottom end of the major shank, the major shank having a diameter larger than the diameter of the minor shank and together defining a central bore, and at least one cutter positioned at the bottom end of the minor shank, and wherein the step of penetrating the end mill comprises:
rotating the end mill while penetrating the material to cut into the material to the predetermined depth;
flowing a coolant downwardly through the central bore toward the material;
undercutting through the material by moving the at least one cutter in a perpendicular direction relative to the bore sufficient to free the sample from the material, and simultaneously changing the direction of flow of the coolant upwardly through the bore towards the top of the major shank; and
drawing the sample with the coolant flow through the bore upwardly through a filter for capturing the sample.

2. The method recited in claim 1 wherein the depth of penetration is no greater than 2 mm.

3. The method recited in claim 1 wherein the depth of penetration is no greater than 200 microns.

4. The method recited in claim 1 wherein penetrating the top surface comprises making a first cut at a first angle relative to the plane of the top surface and making a second cut at a second angle relative to the plane of the top surface.

5. The method recited in claim 4 wherein the end mill is a coring end mill and the first and second cuts are performed simultaneously.

6. The method recited in claim 4 wherein the first and second angles are right angles.

7. The method recited in claim 4 wherein the surface is flat and the first and second angles are supplemental angles relative to the surface.

8. The method recited in claim 1 wherein the step of removing the micro-sample comprises drawing the micro-sample into a container and sealing the container.

9. The method recited in claim 8 wherein the micro-sample is drawn into the container by suction.

10. The method recited in claim 1 further comprising applying a protective layer to the top surface of the material prior to penetration with the end mill.

11. The method recited in claim 1 wherein the material comprises an iron-containing material and the filter has magnetic properties to secure the sample.

12. The method recited in claim 1 wherein the end mill comprises a plurality of cutters, each cutter having an internal blade section that extends laterally into the bore and an external blade section that extends outwardly from the minor shank, wherein the length of the internal blades is less than the radius of the central bore, thereby defining a central area within the bore that determines the width of the micro-sample.

13. The method recited in claim 1 wherein the top surface is convex.

14. The method recited in claim 1 wherein the top surface is concave.

15. A micro-sampler comprising:
a cutting tool calibrated to cut to a depth less than half the thickness of a multi-layered material, the material having a top surface and a base made of a metallic or ceramic material; and
a container for removing and storing a micro-sample cut from the material with each layer of the multi-layered material and a portion of the base intact,
wherein the cutting tool is selected from the group consisting of a micro-diamond wire saw, a micro-focus laser, a fluted core drill, an end mill, a wire electrical discharge machine, and combinations thereof,
wherein the cutting tool is the end mill comprising:
a major shank having a top end and a bottom end;
a minor shank having a top end and a bottom end, the top end of the minor shank extending from the bottom end of the major shank, the major shank having a diameter larger than the diameter of the minor shank;
the major and minor shanks together defining a central bore; and
at least one cutter positioned at the bottom end of the minor shank.

16. The micro-sampler recited in claim 15 wherein the container comprises:
a chamber;
a filter separating the chamber into first and second sections;
an inlet channel having one end opening into the first section of the chamber and a second open end for operative connection to a site of interest to be removed by the cutting tool; and,
a vacuum port fluidly connected on one end to the second section of the chamber and another end fluidly connected to a vacuum source.

17. The micro-sampler recited in claim 15 wherein the end mill comprises a plurality of cutters, each cutter having an internal blade section that extends laterally into the bore and an external blade section that extends outwardly from the minor shank, wherein the length of the internal blades is less than the radius of the central bore, thereby defining a central area within the bore that determines the width of the micro-sample.

18. The micro-sampler recited in claim 15 wherein the cutting tool is calibrated to cut to a depth up to 2 mm.

19. The micro-sampler recited in claim 15 wherein the cutting tool is calibrated to cut to a depth less than or equal to 200 microns.

Assignees

• Westinghouse Electric Co Llc

Inventors

• Parsi Arash
• Byers William A

Classifications

• G01N1/06 Primary

  providing a thin slice, e.g. microtome · CPC title

• G01N2001/063

  with sawing action · CPC title

• G01N2001/066

  electric · CPC title

• G01N1/08 Primary

  involving an extracting tool, e.g. core bit · CPC title

• G21C17/06

  Devices or arrangements for monitoring or testing fuel or fuel elements outside the reactor core, e.g. for burn-up, for contamination (G21C17/08, G21C17/10 take precedence; detecting leaking fuel elements during reactor operation G21C17/04) · CPC title