Sample container, sampling system, nuclear power plant and corresponding operating method

Patent metadata

Field	Value
Publication number	US-10670746-B2
Application number	US-201815966774-A
Country	US
Kind code	B2
Filing date	Apr 30, 2018
Priority date	Oct 29, 2015
Publication date	Jun 2, 2020
Grant date	Jun 2, 2020

Abstract

A sample container, sampling system and operating methods permit representative sampling from a liquid phase or boiling liquid, a gaseous phase, a containment sump, containment atmosphere, or condensation chamber of a nuclear power plant following a severe accident. A sample container obtaining an environmental sample includes an outer chamber surrounded by an outer container wall, being directly fluidically connected to the environment through a passage opening in the outer container wall and being fillable with a liquid at least in a base region. An inner chamber surrounded by an inner container wall is fluidically connected to the base region through a passage opening in the inner container wall, has connections for sampling and conveyor medium lines and is otherwise pressure and media tightly sealed from the environment. A pneumatically or hydraulically actuatable closure device for the passage opening between the outer and inner chambers has an actuation medium line connection.

First claim

The invention claimed is:

1. A sample container for obtaining an environmental sample, the sample container comprising:
an outer chamber having a base region;
an outer container wall surrounding said outer chamber, said outer container wall having at least one passage opening formed therein, said at least one passage opening directly fluidically connecting said outer chamber to the environment for filling said outer chamber with a liquid at least in said base region;
an inner chamber having a connection for a sampling line and a connection for a conveyor medium line and said inner chamber otherwise being sealed from the environment in a pressure-tight and media-tight manner;
an inner container wall surrounding said inner chamber, said inner container wall having a closable passage opening disposed therein forming a fluidic connection between said inner chamber and said base region of said outer chamber, said closable passage opening between said outer chamber and said inner chamber being constructed as a Venturi nozzle; and
a pneumatically or hydraulically actuatable closure device for said closable passage opening between said outer chamber and said inner chamber, said closure device having a connection for an actuation medium line.

2. The sample container according to claim 1 , wherein said closure device includes a hollow cylinder and a closing piston being moveable in said hollow cylinder between an opening position and a closing position.

3. The sample container according to claim 2 , which further comprises a spring element having a spring force and having a resting state setting said closing piston to said opening position, said closing piston moving against said force of said spring element into said closing position in an event of a sufficient pressure in an actuation medium in said actuation medium line.

4. The sample container according to claim 1 , wherein said outer container wall has a base plate, and said closure device is disposed in said base plate.

5. The sample container according to claim 1 , which further comprises a riser projecting into said inner chamber, said connection for said sampling line being connected to said riser.

6. The sample container according to claim 1 , which further comprises at least one heat transfer pipe projecting into said inner chamber for transferring heat from the environment to said inner chamber.

7. A sampling system, comprising:
a sample container according to claim 1 ;
a vacuum pump;
said sampling line connecting said vacuum pump to said inner chamber of said sample container;
a compressed gas source;
said conveyor medium line connecting said compressed gas source to said inner chamber of said sample container; and
said actuation medium line disposed on said closure device of said sample container and connected to said compressed gas source.

8. The sampling system according to claim 7 , wherein said actuation medium line branches off from said conveyor medium line permitting a conveyor medium to simultaneously function as an actuation medium for said closure device.

9. The sampling system according to claim 8 , wherein the conveyor medium is nitrogen gas.

10. The sampling system according to claim 7 , which further comprises a supercritical flow-through choke disposed in said sampling line for maintaining a constant volumetric flow through said sampling line.

11. The sampling system according to claim 7 , wherein said vacuum pump is a jet pump.

12. A nuclear power plant, comprising:
a safety containment having an interior;
a process and analysis module disposed outside said safety containment; and
a sampling system including:
at least one sample container according to claim 1 disposed in said interior of said safety containment;
a vacuum pump;
said sampling line connecting said vacuum pump to said inner chamber of said sample container;
a compressed gas source;
said conveyor medium line connecting said compressed gas source to said inner chamber of said sample container; and
said actuation medium line disposed on said closure device of said sample container and connected to said compressed gas source.

13. A method for operating a sampling system, the method comprising the following steps:
providing a sample container according to claim 1 ;
providing a vacuum pump;
using said sampling line to connect said vacuum pump to said inner chamber of said sample container;
providing a compressed gas source;
using said conveyor medium line to connect said compressed gas source to said inner chamber of said sample container;
providing said actuation medium line on said closure device of said sample container and connected to said compressed gas source; and
extracting a gas sample by applying a negative pressure to said sampling line upon said closable passage opening between said outer chamber and said inner chamber being open.

14. The method according to claim 13 , which further comprises using a scrubbing liquid to convey the gas sample upon a transition of the gas sample from said outer chamber to said inner chamber.

15. The method according to claim 14 , which further comprises using said sampling line to feed the scrubbing liquid into said sample container prior to sampling.

16. The method according to claim 13 , which further comprises extracting an aerosol sample by firstly conveying a gas sample into the sample container by using a scrubbing liquid and then extracting a liquid sample from the scrubbing liquid.

17. The method according to claim 13 , which further comprises applying pressure to said actuation medium line to close said closure device.

18. A method for operating a sampling system, the method comprising the following steps:
providing a sample container according to claim 1 ;
providing a vacuum pump;
using said sampling line to connect said vacuum pump to said inner chamber of said sample container;
providing a compressed gas source;
using said conveyor medium line to connect said compressed gas source to said inner chamber of said sample container;
providing said actuation medium line on said closure device of said sample container and connected to said compressed gas source; and
compressing a fluid sample through said sampling line by applying an overpressure to said conveyor medium line upon said closable passage opening between said outer chamber and said inner chamber being closed.

19. The method according to claim 18 , which further comprises extracting an aerosol sample by firstly conveying a gas sample into the sample container by using a scrubbing liquid and then extracting a liquid sample from the scrubbing liquid.

20. The method according to claim 18 , which further comprises applying pressure to said actuation medium line to close said closure device.

Assignees

• Framatome Gmbh

Inventors

• Hill Axel

Classifications

• G01N1/10 Primary

  in the liquid or fluent state {(burettes, pipettes B01L3/02; sampling of ground water E02D1/06; metering by volume of fluids or fluent solid material G01F11/00, G01F13/00)} · CPC title

• G01N2001/2223

  aerosol sampling devices · CPC title

• G01N2001/2238

  the gas being compressed or pressurized · CPC title

• G01N2001/2229

  Headspace sampling, i.e. vapour over liquid · CPC title

• G01N1/2202

  involving separation of sample components during sampling · CPC title