Method of producing phosphoric acid crosslinked starch
US-12110346-B2 · Oct 8, 2024 · US
US11225529B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-11225529-B2 |
| Application number | US-202016910494-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 24, 2020 |
| Priority date | Jul 16, 2019 |
| Publication date | Jan 18, 2022 |
| Grant date | Jan 18, 2022 |
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Disclosed is method for preparation of a starch phosphate using phytate. The method enables the preparation of a starch phosphate with improved physical properties such as high transparency, solubility, swelling power, and storage stability by the phosphorylation of a starch using naturally occurring phytate rather than using a synthetic chemical. Due to these advantages, the starch phosphate is expected to replace conventional chemically modified starches. In addition, the method enables the preparation of a starch phosphate based on a simple modification. The use of the starch phosphate greatly contributes to improvements in the quality and storage stability of various starchy foods. Therefore, the starch phosphate is expected to find application in the food industry, including starchy foods.
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What is claimed is: 1. A method for preparing a starch phosphate comprising: dispersing a mixture of phytate and starch in a solution to prepare a phytate-starch dispersion having a pH of 7-10; drying the phytate-starch dispersion to obtain a phytate-starch powder; and heating the phytate-starch powder to induce a reaction between the phytate and the starch to obtain the starch phosphate. 2. The method according to claim 1 , further comprising neutralizing and washing the obtained starch phosphate. 3. The method according to claim 2 , further comprising drying and pulverizing the neutralized and washed starch phosphate. 4. The method according to claim 1 , wherein the starch is selected from the group consisting of native starches, comprising normal corn starch, waxy corn starch, high amylose starch, rice starch, waxy rice starch, high amylose rice starch, potato starch, sweet potato starch, tapioca starch, sorghum starch, wheat starch, sago starch, chestnut starch, bean starch, and mixtures, and modified starches thereof. 5. The method according to claim 1 , wherein the phytate is used in an amount of 1 to 5% (w/w), based on the weight of the starch. 6. The method according to claim 1 , wherein the drying is performed at a temperature of 30 to 50° C. 7. The method according to claim 1 , wherein the heating is performed at 110 to 130° C. for 2 to 24 hours. 8. The method according to claim 1 , wherein the solution comprises NaHCO 3 , NaOH, or a mixture thereof. 9. The method according to claim 1 , wherein the solution comprises a gelatinization inhibitor. 10. The method according to claim 9 , wherein the gelatinization inhibitor is Na 2 SO 4 . 11. The method according to claim 9 , wherein an amount of the gelatinization inhibitor is 1 to 10 wt % based on a weight of the starch. 12. The method according to claim 1 , a concentration of the phytate-starch dispersion is 50 to 70 wt % based on a weight of the solution.
Chemically modified starch; Reaction or complexation products of starch with other chemicals · CPC title
Drying, dehydrating · CPC title
Starch phosphates, e.g. phosphorylated starch · CPC title
Heat, thermal treatment · CPC title
Phosphoric acid · CPC title
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