Method and device for producing and coding metal powder

Patent metadata

Field	Value
Publication number	US-11020801-B2
Application number	US-201716300089-A
Country	US
Kind code	B2
Filing date	May 12, 2017
Priority date	May 13, 2016
Publication date	Jun 1, 2021
Grant date	Jun 1, 2021

Abstract

The invention relates to a method for coding metal powder. Said method comprises the following steps: providing a melt, forming a melt stream, spraying the melt stream by means of a spraying fluid, and forming metal powder particles from the melt stream. The method is characterized in that, during the spraying of the melt and/or the spraying fluid, a coding component or a coding gas is added in such a way that the use of the coding component in the metal powder can be detected, wherein the gaseous coding component comprises one or more isotopes of at least one gas and the fraction of the at least one isotope is changed in comparison with the naturally occurring fraction of said isotope in the gas and/or wherein the gaseous coding component contains gaseous alloying elements.

First claim

The invention claimed is:

1. A method for producing and coding metal powder, comprising:
providing a melt;
forming a melt stream;
spraying the melt stream by means of a spraying fluid; and
forming metal powder particles from the melt stream;
wherein, during the spraying of the melt and/or the spraying fluid, a coding component is added in such a way that the use of the coding component in the metal powder can be detected, and
wherein the coding component comprises one or more isotopes of at least one gas and the fraction of the at least one isotope is changed in comparison with the naturally occurring fraction of said isotope in the gas.

2. The method of claim 1 , wherein information about the coding component and the composition thereof is stored in a database.

3. The method of claim 2 , wherein the metal powder is detected by means of a chemical analysis method or by means of a mass spectrometer.

4. The method of claim 2 , wherein the metal powder is detected by means of a chemical analysis method or by means of a mass spectrometer and the coding component of the metal powder is verified by comparison with the stored information about the coding component.

5. The method of claim 1 , wherein the spraying fluid comprises an inert gas selected from:
argon, helium, neon, krypton, xenon and radon; or
an active gas selected from the group consisting of O 2 , CO 2 , H 2 , N 2 , and mixtures thereof; and
the coding component comprises a component selected from oxygen 18 carbon dioxide (C 18 O 2 ), carbon 13 carbon dioxide ( 13 CO 2 ), carbon 13 carbon monoxide ( 13 CO), deuterium (D 2 ), nitrogen 15 ( 15 N 2 ) and oxygen 18 ( 18 O 2 ), and mixtures thereof.

6. The method of claim 1 , wherein the frequency of the isotopes in comparison with the naturally occurring frequency is increased or reduced by more than 0.5%.

7. The method of claim 1 , wherein the coding component contains at least one isotope of an active gas, which reacts with the powder particles of the metal powder in such a way that the at least one isotope of the active gas it remains in the powder particles of the metal powder.

8. The method of claim 1 , wherein the coding component comprises one or more isotopes of the spraying fluid, wherein the fraction of one or more isotopes of the spraying fluid in the coding component is changed in comparison with the natural fraction of the one or more isotopes in the spraying fluid, wherein the different isotopes form the coding in the coding component.

9. The method of claim 1 , wherein the isotopes are isotopes of the gas, which forms the main component of the spraying fluid.

10. The method of claim 1 , wherein the coding component comprises a gaseous alloying element.

11. The method of claim 1 , wherein the frequency of the isotopes in comparison with the naturally occurring frequency is increased or reduced by more than 0 1.0%.

12. The method of claim 1 , wherein the frequency of the isotopes in comparison with the naturally occurring frequency is increased or reduced by more than 5%.

13. The method of claim 1 , wherein the coding component comprises at least one isotope of an inert gas, wherein the isotope becomes included in the metal powder.

14. The method of claim 1 , wherein the isotopes are different from the isotopes of the spraying fluid.

Assignees

• Linde Ag

Inventors

• SCHOLZ Jürgen
• Miklos Ernst
• Fieret Jim

Classifications

• B22F2009/0848

  Melting process before atomisation · CPC title

• B22F2998/10

  Processes characterised by the sequence of their steps · CPC title

• B22F9/082 Primary

  atomising using a fluid (using centrifugal force B22F9/10) · CPC title

• B22F2009/0844

  in controlled atmosphere · CPC title

• B22F2201/013

  Hydrogen · CPC title