Dissolvable films impregnated with encapsulated tobacco, tea, coffee, botanicals, and flavors for oral products

Patent metadata

Field	Value
Publication number	US-10952452-B2
Application number	US-201514923995-A
Country	US
Kind code	B2
Filing date	Oct 27, 2015
Priority date	Dec 30, 2008
Publication date	Mar 23, 2021
Grant date	Mar 23, 2021

Abstract

A process for preparing an orally-enjoyable film of encapsulated plant material includes combining particles of finely divided plant material, a first coating material, and a second coating material, then inducing gelation to form a gel matrix of the particles coated with the first coating material embedded in the second coating material, followed by forming a film from the gel matrix. Also disclosed is a film of coated particles of finely-divided plant material, made of a gel matrix of plant material at least partially surrounded by a first coating material and embedded in a second coating material.

First claim

What is claimed is:

1. An orally-enjoyable film of coated particles of finely-divided plant material, the film comprising:
a gel matrix including,
a plurality of particles of finely-divided plant material at least partially surrounded by a first coating material and embedded in a second coating material, the plant material including tobacco,

wherein:
(i) the plant material and the first coating material are electrostatically attracted,
(ii) the first coating material and the second coating material are electrostatically attracted, or
(iii) both (i) and (ii),

wherein the film has a smooth surface, the film is flexible, and the film is mouth-stable for about 1 minute to about 20 minutes,
wherein the film includes the first coating material in an amount of about 1% to about 20% by dry weight and the second coating material in an amount of about 5% to about 50% by dry weight, and
wherein the film provides controlled release of the plant material.

2. The film of claim 1 , wherein the plant material consists of:
a micronized powder obtained by finely dividing a plant or a fragment of a plant and the film is an extruded film.

3. The film of claim 1 , wherein:
(i) the particles have an average largest dimension of less than about 3000 microns;
(ii) the film comprises:
the plant material in an amount of about 10 to about 90% by dry weight;

(iii) the coated particles have a moisture content of less than about 15% by weight;
(iv) the coated particles has a net negative or neutral charge;
(v) or two or more of (i) to (iv).

4. The film of claim 1 , wherein:
(i) the first coating material comprises at least one protein, the at least one protein including milk protein, whey protein, soy protein, wheat protein, rice protein, egg white protein, protein obtained from tobacco, gelatin, protein hydrolyzates, or any combination thereof;
(ii) the first coating material comprises a zwitterionic or positively charged protein;
(iii) the second coating comprises at least one pectin obtained from tobacco, apples, citrus peel, plums, gooseberries, or any combination thereof;
(iv) the second coating comprises an anionic polysaccharide;
(v) the second coating comprises at least one material including carrageenans, gum Arabic, carboxymethyl cellulose, sodium alginates, gum tragacanth, locust bean gum, gellan gum, xanthan gum, or any combination thereof;
(vi) the plant material further comprises a tobacco substitute, coffee, or tea;
(vii) the film is self-supporting;
(viii) the film comprises two or more matrices of different compositions;
(ix) the film comprises a flavorant; or
(x) two or more of (i) through (ix).

5. The film of claim 1 , wherein the plant material further comprises a tobacco substitute.

6. The film of claim 1 , wherein,
(i) the first coating material includes proteins, cationic polysaccharides or oligosaccharides, non-ionic polysaccharides, oligosaccharides, or any combination thereof;
(ii) the second coating material includes anionic, zwitterionic, or neutral polysaccharides; a protein; or any combination thereof; or
(iii) (i) and (ii).

7. The film of claim 6 , wherein the first coating material is a protein and the second coating material is a polysaccharide.

8. The film of claim 7 , wherein the protein has a molecular weight of between about 2 kDa and about 1000 kDa and the polysaccharide has a molecular weight of between about 5 kDa and about 1000 kDa.

9. The film of claim 1 , wherein the film includes areas having differing compositions so as to provide different release profiles.

10. A palatable or comestible product comprising at least one film according to claim 1 .

11. An orally-enjoyable film of coated particles of finely-divided plant material, the film comprising:
a gel matrix including,
a plurality of particles of finely-divided plant material at least partially surrounded by a first coating material and embedded in a second coating material, which has been gelled, the plant material including tobacco,

wherein:
(i) the plant material and the first coating material are electrostatically attracted,
(ii) the first coating material and the second coating material are electrostatically attracted, or
(iii) both (i) and (ii),

wherein the film has a textured surface, the film is flexible, and the film is mouth-stable for about 1 minute to about 20 minutes,
wherein the film includes the first coating material in an amount of about 1% to about 20% by dry weight and the second coating material in an amount of about 5% to about 50% by dry weight, and
wherein the film provides controlled release of the plant material.

12. The film of claim 11 , wherein the plant material consists of:
a micronized powder obtained by finely dividing a plant or a fragment of a plant and the film is an extruded film.

13. The film of claim 11 , wherein:
(i) the particles have an average largest dimension of less than about 3000 microns;
(ii) the film comprises:
the plant material in an amount of about 10 to about 90% by dry weight;

(iii) the coated particles have a moisture content of less than about 15% by weight;
(iv) the coated particles have a net negative or neutral charge;
(v) or two or more of (i) to (iv).

14. The film of claim 11 , wherein:
(i) the first coating material comprises at least one protein including milk protein, whey protein, soy protein, wheat protein, rice protein, egg white protein, protein obtained from tobacco, gelatin, protein hydrolyzates, or any combination thereof;
(ii) the first coating material comprises a zwitterionic or positively charged protein;
(iii) the second coating comprises at least one pectin obtained from tobacco, apples, citrus peel, plums, gooseberries, or any combination thereof;
(iv) the second coating comprises an anionic polysaccharide;
(v) the second coating comprises at least one material including carrageenans, gum Arabic, carboxymethyl cellulose, sodium alginates, gum tragacanth, locust bean gum, gellan gum, xanthan gum, or any combination thereof;
(vi) the plant material further comprises a tobacco substitute, coffee, or tea;
(vii) the film is self-supporting;
(viii) the film comprises two or more matrices of different compositions; or
(ix) the film comprises a flavorant; or
(x) two or more of (i) through (ix).

15. The film of claim 11 , wherein the plant material further comprises a tobacco substitute.

16. The film of claim 11 , wherein,
(i) the first coating material includes proteins, cationic polysaccharides or oligosaccharides, non-ionic polysaccharides, oligosaccharides, or any combination thereof;
(ii) the second coating material includes anionic, zwitterionic, or neutral polysaccharides; a protein; or any combination thereof; or
(iii) (i) and (ii).

17. The film of claim 16 , wherein the first coating material is a protein and the second coating material is a polysaccharide.

18. The film of claim 17 , wherein the protein has a molecular weight of between about 2 kDa and about 1000 kDa and the polysaccharide has a molecular weight of between about 5 kDa and about 1000 kDa.

19. The film of claim 11 , wherein the film includes areas having differing compositions so as to provide different release profiles.

20. A palatable or comestible product comprising at least one film according to claim 11 .

Assignees

• Philip Morris Usa Inc

Inventors

• Sengupta Tapashi
• Mishra Munmaya K
• Sweeney William R

Classifications

• A23P10/30

  Encapsulation of particles, e.g. foodstuff additives · CPC title

• A23F5/14

  using additives, e.g. milk or sugar; Coating (flavouring A23F5/46) · CPC title

• A24B15/285

  characterised by structural features, e.g. particle shape or size · CPC title

• A23L27/79

  in the form of films · CPC title

• A24B15/186

  by coating with a coating composition, encapsulation of tobacco particles (encapsulation of additives other than tobacco : A24B15/283) · CPC title