Dissolvable films impregnated with encapsulated tobacco, tea, coffee, botanicals, and flavors for oral products

Patent metadata

Field	Value
Publication number	US-10568338-B2
Application number	US-201514923899-A
Country	US
Kind code	B2
Filing date	Oct 27, 2015
Priority date	Dec 30, 2008
Publication date	Feb 25, 2020
Grant date	Feb 25, 2020

Abstract

A process for preparing an orally-enjoyable film of encapsulated plant material includes combining particles of finely divided plant material, a first coating material, and a second coating material, then inducing gelation to form a gel matrix of the particles coated with the first coating material embedded in the second coating material, followed by forming a film from the gel matrix. Also disclosed is a film of coated particles of finely-divided plant material, made of a gel matrix of plant material at least partially surrounded by a first coating material and embedded in a second coating material.

First claim

What is claimed is:

1. A process for preparing an orally-enjoyable film of coated particles of finely divided plant material, comprising:
combining particles of finely divided plant material and a first coating material in a liquid medium, wherein the first coating material adsorbs onto at least a portion of a surface of the particles to form a layer of the first coating material;
mixing a second coating material with the liquid medium, wherein the second coating material adsorbs onto at least a portion of the layer;
inducing gelation to form a gel matrix including the particles at least partially surrounded by the layer of the first coating material and embedded in the second coating material; and
forming a film from the gel matrix,
wherein:
(i) the plant material and the first coating material are electrostatically attracted,
(ii) the first coating material and the second coating material are electrostatically attracted, or
(iii) both (i) and (ii).

2. The process of claim 1 , wherein the forming the film comprises:
(i) cutting the gel matrix into a desired geometry,
(ii) flattening the gel matrix, or
(iii) both (i) and (ii).

3. The process of claim 1 wherein the forming comprises flattening using one or more rollers, and at least one of the rollers is heated, textured, or both heated and textured.

4. The process of claim 1 , wherein the plant material consists of:
a micronized powder obtained by finely dividing a plant or a fragment of a plant.

5. The process of claim 1 , wherein the plant material and the first coating material are electrostatically attracted and the first coating material and the second coating material are electrostatically attracted.

6. The process of claim 1 , wherein:
(i) the first coating material comprises a protein including milk protein, whey protein, soy protein, wheat protein, rice protein, egg white protein, protein obtained from tobacco, gelatin, protein hydrolyzates, or any combination thereof;
(ii) the first coating material comprises a zwitterionic or positively charged protein;
(iii) the second coating material comprises at least one pectin obtained from tobacco, apples, citrus peel, plums, gooseberries, or any combination thereof;
(iv) the second coating material comprises an anionic polysaccharide;
(v) the second coating material comprises a material including carrageenan, gum Arabic, carboxymethyl cellulose, sodium alginate, gum tragacanth, locust bean gum, gellan gum, xanthan gum, or any combination thereof;
(vi) the plant material comprises a tobacco, a tobacco substitute, coffee, tea, or any combination thereof;
(vii) the film is self-supporting;
(viii) further comprising adding a flavorant;
(ix) the film comprises a smooth surface, a textured surface, perforations, or any combination thereof;
(x) the film is formed from two or more gel matrices of different compositions;
(xi) two or more of (i) through (x).

7. The process of claim 1 :
(i) wherein the process is performed without addition of a salt as a crosslinking agent;
(ii) further comprising forming a colloidal dispersion of the plant material;
(iii) further comprising lowering a pH of the liquid medium using a material including citric acid, acetic acid, adipic acid, fumaric acid, malic acid, lactic acid, tartaric acid, gluconic acid, glucono delta lactone, hydrochloric acid, or any combination thereof;
(iv) further comprising increasing the pH of the liquid medium using a material including sodium carbonate, sodium bicarbonate, sodium hydroxide, or any combination thereof;
(v) further comprising a drying step;
(vi) further comprising an extrusion step;
(vii) further comprising using at least a third coating material to form one or more additional layers around the plant material; or
(viii) two or more of (i) through (vii).

8. The process of claim 1 , further comprising:
inducing gelation by
(i) adjusting a pH of the liquid medium;
(ii) adding monovalent, divalent, or trivalent cations to the liquid medium;
(iii) heating to a temperature of between about 60° C. and about 90° C. for about 1 to about 3 hours;
(iv) cooling to a temperature of between about 20° C. and about 0° C. for about 1 to about 48 hours; or
(v) two or more of (i) to (iv).

9. The process of claim 1 , wherein,
(i) the first coating material includes proteins, cationic polysaccharides or oligosaccharides, non-ionic polysaccharides, oligosaccharides, or any combination thereof;
(ii) the second coating material includes anionic, zwitterionic, or neutral polysaccharides; a protein; or any combination thereof; or
(iii) both (i) and (ii).

10. The process of claim 9 , wherein the first coating material is a protein and the second coating material is a polysaccharide.

11. The process of claim 1 , wherein:
(i) the particles have an average largest dimension of less than about 3000 microns;
(ii) the film includes,
(a) the plant material in an amount of about 10 to about 90% by dry weight,
(b) first coating material in an amount of about 1% to about 20% by dry weight,
(c) second coating material in an amount of about 5% to about 50% by dry weight, or
(d) any combination thereof;

(iii) the coated particles have a moisture content of less than about 15% by weight;
(iv) the coated particles have a net negative or neutral charge;
(v) the process further includes forming one or more additional layers around the plant material; or
(vi) two or more of (i) to (v).

12. The process of claim 1 , wherein the plant material comprises tobacco, a tobacco substitute, or both tobacco and a tobacco substitute.

13. The process of claim 10 , wherein the protein has a molecular weight of between about 2 kDa and about 1000 kDa and the polysaccharide has a molecular weight of between about 5 kDa and about 1000 kDa.

Assignees

• Philip Morris Usa Inc

Inventors

• Sengupta Tapashi
• Mishra Munmaya K
• Sweeney William R

Classifications

• A24B15/302

  by natural substances obtained from animals or plants · CPC title

• A23F3/14 Primary

  Tea preparations, e.g. using additives (flavouring A23F3/40) · CPC title

• A23V2002/00

  Food compositions, function of food ingredients or processes for food or foodstuffs · CPC title

• A24B15/285

  characterised by structural features, e.g. particle shape or size · CPC title

• A23F5/14

  using additives, e.g. milk or sugar; Coating (flavouring A23F5/46) · CPC title