Large area format sapphire windows via transient liquid phase bonding
US-9915756-B2 · Mar 13, 2018 · US
US10793970B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10793970-B2 |
| Application number | US-201716310238-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 14, 2017 |
| Priority date | Jun 15, 2016 |
| Publication date | Oct 6, 2020 |
| Grant date | Oct 6, 2020 |
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A method of fabricating a turbine engine part, the method including fabricating an ingot out of ceramic material of eutectic composition by performing the Czochralski process including putting a seed of the ingot that is to be obtained into contact with a molten bath of a mixture of eutectic composition in order to initiate the formation of the ingot on the seed, the mixture including at least two ceramic compounds; drawing the ingot from the molten bath while imposing on the ingot that is being formed a drawing speed less than or equal to 10 mm/h together with rotation at a speed of rotation less than or equal to 50 rpm; and machining the ingot as fabricated in this way in order to obtain the turbine engine part.
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The invention claimed is: 1. A method of fabricating a turbine engine part, the method comprising: fabricating an ingot out of ceramic material of eutectic composition by performing the Czochralski process comprising the following steps: putting a seed of the ingot that is to be obtained into contact with a molten bath of a mixture of eutectic composition in order to initiate the formation of the ingot on the seed, said mixture comprising at least two ceramic compounds; drawing the ingot from the molten bath while imposing on the ingot that is being formed a drawing speed less than or equal to 10 mm/h together with rotation at a speed of rotation less than or equal to 50 rpm; and machining the ingot as fabricated in this way in order to obtain the turbine engine part, wherein the ingot is drawn from the molten bath along a drawing axis, and wherein a temperature gradient less than or equal to 50° C./mm is maintained in the ingot along the drawing axis, at least in the vicinity of a surface of the molten bath. 2. A method according to claim 1 , wherein the eutectic mixture includes alumina. 3. A method according to claim 1 , wherein the eutectic mixture includes zirconia. 4. A method according to claim 1 , wherein the eutectic mixture includes at least: a rare earth oxide, an aluminum and rare earth garnet RE 3 Al 5 O 12 , or a perovskite REAlO 3 , where RE designates a rare earth element. 5. A method according to claim 1 , wherein the eutectic mixture is selected from the following mixtures: Al 2 O 3 —ZrO 2 , Al 2 O 3 -YAG, RE 3 Al 5 O 12 —Al 2 O 3 where RE is a rare element, Al 2 O 3 —RE 3 Al 5 O 12 —ZrO 2 , and Al 2 O 3 -YAG-ZrO 2 . 6. A method according to claim 1 , wherein the ingot being formed is subjected to a drawing speed lying in the range 1 mm/h to 5 mm/h. 7. A method according to claim 1 , wherein the ingot being formed is subjected to a speed of rotation lying in the range 1 rpm to 30 rpm. 8. A method according to claim 1 , wherein the fabricated part is a turbine engine blade or vane. 9. A method according to claim 1 , wherein the fabricated part is a ring sector. 10. A method according to claim 1 , wherein the fabricated part is a nozzle.
by pulling from a melt · CPC title
containing zirconium oxide or zircon (ZrSiO4) · CPC title
with formula A3Me5O12 wherein A is a rare earth metal and Me is Fe, Ga, Sc, Cr, Co or Al, e.g. garnets · CPC title
Refractories by fusion casting · CPC title
with formula AMeO3, wherein A is a rare earth metal and Me is Fe, Ga, Sc, Cr, Co or Al, e.g. ortho ferrites · CPC title
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