Large area format sapphire windows via transient liquid phase bonding

Patent metadata

Field	Value
Publication number	US-9915756-B2
Application number	US-201514811305-A
Country	US
Kind code	B2
Filing date	Jul 28, 2015
Priority date	Jul 28, 2015
Publication date	Mar 13, 2018
Grant date	Mar 13, 2018

Abstract

A method for forming an optical window. In one example, the method includes depositing a layer of eutectic bonding material onto a first surface of a first section of window material, positioning a second surface of a second section of window material onto the layer of eutectic bonding material such that the first surface is disposed opposite the second surface, and heating the eutectic bonding material to a temperature above a eutectic temperature of the eutectic bonding material and below a melting temperature of the window material for a predetermined length of time to form an optical window. The window material of the first section and the second section may be transparent to infrared radiation and comprise aluminum.

First claim

What is claimed is:

1. A method of forming an optical window comprising:
depositing a layer of eutectic bonding material onto a first surface of a first section of a window material, wherein the eutectic bonding material is an aluminosilicate;
positioning a second surface of a second section of the window material onto the layer of eutectic bonding material such that the first surface is disposed opposite the second surface, the window material being transparent to infrared radiation and including aluminum; and
heating the eutectic bonding material to a temperature above a eutectic temperature of the eutectic bonding material and below a melting temperature of the window material for a predetermined length of time to bond the first and second sections together such that at least a portion of the aluminum in the window material diffuses in the form of crystalline needles into an interface between the first section of window material and the eutectic bonding material and the second section of window material and the eutectic bonding material to form an optical window.

2. The method of claim 1 , wherein the eutectic bonding material is calcium aluminosilicate (CAS).

3. The method of claim 1 , wherein the window material is at least one of Spinel, AlON, sapphire, YAG, Nd:YAG, and SiAlON.

4. The method of claim 3 , wherein the window material is sapphire.

5. The method of claim 4 , wherein the window material is c-plane sapphire.

6. The method of claim 4 , further comprising aligning the crystal orientation of the window material of the first section to the crystal orientation of the window material of the second section.

7. The method of claim 6 , wherein the window material is a-plane sapphire.

8. The method of claim 1 , wherein the first surface and the second surface are as-ground surfaces.

9. The method of claim 1 , wherein the temperature is in a range of 1275-1350° C. and the predetermined length of time is about 18 hours.

10. The method of claim 1 , further comprising positioning and heating at least two sections to form a large area format optical window having a size of at least 14 inches×28 inches.

11. The method of claim 1 , wherein the second section of the window material is positioned orthogonally relative to the first section of the window material.

12. The method of claim 1 , wherein the formed optical window can withstand a tensile load of at least 8 psi.

13. The method of claim 1 , wherein the first surface and the second surface are edge surfaces of the first section of the window material and the second section of the window material, respectively.

14. An optical window, comprising:
a first section of a window material having a first surface;
a second section of the window material having a second surface, the window material being transparent to infrared radiation and comprising aluminum; and
at least one layer of eutectic bonding material disposed between the first surface and the second surface, wherein the eutectic bonding material is an aluminosilicate and the first surface is bonded to the second surface using a transient liquid phase bonding process and at least a portion of the aluminum in the window material is integrated as crystalline needles into the an interface between the first section of the window material and the eutectic bonding material and the second section of the second section of the window material and the eutectic bonding material.

15. The optical window of claim 14 , wherein the eutectic bonding material is calcium aluminosilicate (CAS).

16. The optical window of claim 14 , wherein the window material is at least one of Spinel, AlON, sapphire, YAG, Nd:YAG, and SiAlON.

17. The optical window of claim 16 , wherein the window material is sapphire.

18. The optical window of claim 17 , wherein the window material is c-plane sapphire or a-plane sapphire.

19. The optical window of claim 14 , wherein two or more sections of the window material form a large area format optical window having a size of at least 14×28 inches.

20. The optical window of claim 14 , wherein the optical window can withstand a tensile load of at least 8 psi.

Assignees

• Raytheon Co

Inventors

• Nordahl Christopher S

Classifications

• G02B1/02 Primary

  made of crystals, e.g. rock-salt, semi-conductors (G02B1/08 takes precedence) · CPC title

• C30B33/06

  Joining of crystals · CPC title

• C04B2237/064

  based on alumina or aluminates · CPC title

• C04B2237/60

  Forming at the joining interface or in the joining layer specific reaction phases or zones, e.g. diffusion of reactive species from the interlayer to the substrate or from a substrate to the joining interface, carbide forming at the joining interface · CPC title

• C04B2237/343

  Alumina or aluminates · CPC title