Method of manufacturing fluorine-containing compound
US-12577199-B2 · Mar 17, 2026 · US
US10787406B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10787406-B2 |
| Application number | US-201816626642-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jul 3, 2018 |
| Priority date | Jul 3, 2017 |
| Publication date | Sep 29, 2020 |
| Grant date | Sep 29, 2020 |
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This invention provides a composition that contains PFOB with a PFOA content lower than that of known PFOB, and that is less likely to have an adverse effect on the environment; and provides a method for producing PFOB. The composition contains C8F17Brand further contains C7F15COOH, wherein C7F15COOH is present in a concentration of 25 ppb or less based on the total weight of C8F17Br. The method for producing C8F17Br comprises reacting C8F17I and a brominating agent to obtain C8F17Br, and alkali-washing the obtained C8F17Br to reduce the C7F15COOH content to 25 ppb or less based on the total weight of C8F17Br.
Opening claim text (preview).
The invention claimed is: 1. A composition containing C 8 F 17 Br, and further containing C 7 F 15 COOH, wherein C 7 F 15 COOH is present in a concentration of 25 ppb or less based on the total weight of C 8 F 17 Br. 2. A method for producing C 8 F 17 Br, comprising: reacting C 8 F 17 I and a brominating agent to obtain C 8 F 17 Br; and alkali-washing the obtained C 8 F 17 Br to reduce the C 7 F 15 COOH content to 25 ppb or less based on the total weight of C 8 F 17 Br. 3. The production method according to claim 2 , wherein the alkali-washing is performed using an alkali solution having a concentration of 0.01 to 98 wt %. 4. The production method according to claim 2 , wherein the alkali-washing is performed using an alkali solution having a concentration of 0.01 to 48 wt %. 5. The production method according to claim 2 , wherein the alkali-washing is performed using an alkali solution having a concentration of 0.01 to 25 wt %. 6. The production method according to claim 2 , wherein the alkali-washing is performed using an alkali solution having a concentration of 0.01 to 10 wt %.
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