Gallium nitride self-supported substrate, light-emitting device and manufacturing method therefor
US-2015144956-A1 · May 28, 2015 · US
US10774002B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10774002-B2 |
| Application number | US-201815956898-A |
| Country | US |
| Kind code | B2 |
| Filing date | Apr 19, 2018 |
| Priority date | Nov 16, 2015 |
| Publication date | Sep 15, 2020 |
| Grant date | Sep 15, 2020 |
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A method for producing an oriented sintered body according to the present invention includes the steps of: (a) preparing a multilayer body, the multilayer body including a layer including a fine raw-material powder and a layer including a plate-like raw-material powder which are alternately stacked each other, particles of the plate-like raw-material powder being arranged such that surfaces of the particles of the plate-like raw-material powder extend along a surface of the layer including a fine raw-material powder; and (b) sintering the multilayer body.
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What is claimed is: 1. A method for producing an oriented sintered body comprising the steps of: (a) preparing a multilayer body, the multilayer body including a layer including a fine raw-material powder and a layer including a plate-like raw-material powder which are alternately stacked on each other, particles of the plate-like raw-material powder being arranged such that surfaces of the particles of the plate-like raw-material powder extend along a surface of the layer including the fine raw-material powder; and (b) sintering the multilayer body, wherein the particles of the fine raw-material powder have a smaller average diameter than the particles of the plate-like raw-material powder, and wherein a coverage at which the surface of the layer including the fine raw-material powder is covered with the plate-like raw-material powder is 1% to 60%. 2. The method for producing an oriented sintered body according to claim 1 , wherein the layer including the fine raw-material powder has a thickness of 5 to 100 μm. 3. The method for producing an oriented sintered body according to claim 1 , wherein, in the step (a), a single-side processed body including a compact of the fine raw-material powder having two opposed major surfaces and the layer including the plate-like raw-material powder, the layer covering one major surface of the compact, is prepared, and the multilayer body is prepared using the single-side processed body. 4. The method for producing an oriented sintered body according to claim 3 , wherein the single-side processed body is prepared by stacking a compact of the plate-like raw-material powder on one of the major surfaces of the compact of the fine raw-material powder, the compact of the plate-like raw-material powder having a smaller thickness than the compact of the fine raw-material powder, or by applying a dispersion liquid containing the plate-like raw-material powder on one of the major surfaces of the compact of the fine raw-material powder by printing method, spray coating method, spin coating method, or dip coating method. 5. The method for producing an oriented sintered body according to claim 1 , wherein, in the step (a), a double-side processed body including a compact of the fine raw-material powder and the particles of the plate-like raw-material powder having two opposed major surfaces, the particles being arranged on both of the major surfaces of the compact such that the surfaces of the particles extend along a corresponding major surface of the compact, is prepared, and the multilayer body is prepared using the double-side processed body and a compact that has not been processed. 6. The method for producing an oriented sintered body according to claim 5 , wherein the double-side processed body is prepared by stacking a compact of the plate-like raw-material powder on both of the major surfaces of the compact of the fine raw-material powder, the compact of the plate-like raw-material powder having a smaller thickness than the compact of the fine raw-material powder, or by applying a dispersion liquid containing the plate-like raw-material powder on both of the major surfaces of the compact of the fine raw-material powder by printing method, spray coating method, spin coating method, or dip coating method. 7. The method for producing an oriented sintered body according to claim 1 , wherein, in the step (b), the multilayer body is sintered under pressure. 8. The method for producing an oriented sintered body according to claim 1 , wherein a principal component of the fine raw-material powder and a principal component of the plate-like raw-material powder are both alumina.
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directly from the solid state · CPC title
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