Quality control process to assess the aluminized coating characteristics of hot stamped parts

Patent metadata

Field	Value
Publication number	US-10481052-B2
Application number	US-201815937917-A
Country	US
Kind code	B2
Filing date	Mar 28, 2018
Priority date	Mar 28, 2018
Publication date	Nov 19, 2019
Grant date	Nov 19, 2019

Abstract

A method of inspecting and determining characteristics of an aluminized coating of a hot stamped part is provided. The method includes removing a sample from the hot stamped part for Glow Discharge Optical Emission Spectrometry (GDOES), analyzing the sample using GDOES, and plotting constituent element weight percentages versus depth on a graph. The method further includes determining points on the graph where constituent elements intersect and where the points of intersection indicate the characteristics of the aluminized coating. The characteristics of the method include, by way of example, a total thickness of the aluminized coating, a thickness of an inter-diffusion layer (IDL), constituents of the aluminized coating, constituents of the hot stamped part, phase composition of the aluminized coating, surface oxidation, and weldability.

First claim

What is claimed is:

1. A method of inspecting and determining characteristics of an aluminized coating of a hot stamped part comprising:
removing a sample from the hot stamped part for Glow Discharge Optical Emission Spectrometry (GDOES);
analyzing the sample using GDOES and plotting constituent element weight percentages versus depth on a graph; and
determining points on the graph where constituent elements intersect,
wherein the points of intersection indicate the characteristics of the aluminized coating.

2. The method according to claim 1 , wherein the characteristics are selected from the group consisting of a total thickness of the aluminized coating, a thickness of an inter-diffusion layer (IDL), constituents of the aluminized coating, constituents of the hot stamped part, phase composition of the aluminized coating, surface oxidation, and weldability.

3. The method according to claim 2 , wherein the hot stamped part is coated with a eutectic AlSi 10 Fe 3 alloy, and an intersection between Aluminum and Carbon indicates the total thickness of the aluminized coating.

4. The method according to claim 2 , wherein the hot stamped part is coated with a eutectic AlSi 10 Fe 3 alloy, and a difference between an intersection of Aluminum and Carbon and a second maximum Silicon wt. % indicates the thickness of the IDL.

5. The method according to claim 1 , wherein the sample size is approximately 5 mm in diameter.

6. The method according to claim 1 , wherein the sample does not undergo any preparation prior to being analyzed by GDOES.

7. The method according to claim 6 , wherein the preparation includes mounting, grinding, and polishing.

8. The method according to claim 1 further comprising determining whether contamination is present by a comparison of constituent elements to a composition of the hot stamped part.

9. The method according to claim 1 further comprising the step of providing the characteristics to a subsequent manufacturing operation.

10. The method according to claim 9 , wherein the subsequent manufacturing operation is selected from the group consisting of an annealing operation, a shot-blasting operation, and a welding operation.

11. The method according to claim 10 , wherein the characteristics are provided to a controller of the annealing furnace, wherein the controller adjusts a temperature and processing time of the hot stamped part in the annealing furnace based on at least one characteristic.

12. A method of inspecting and determining a total thickness of an aluminized coating and a thickness of an inter-diffusion layer (IDL) of a hot stamped boron steel part comprising:
preparing a sample from the hot stamped part for Glow Discharge Optical Emission Spectrometry (GDOES);
analyzing the sample using GDOES and plotting constituent element weight percentages versus depth on a graph; and
determining points on the graph where constituent elements intersect,
wherein an intersection between Aluminum and Carbon indicates the total thickness of the aluminized coating, and a difference between an intersection of Aluminum and Carbon and a second maximum Silicon wt. % indicates the thickness of the IDL.

13. The method according to claim 12 further comprising determining whether contamination is present by a comparison of constituent elements to a composition of the hot stamped part.

14. The method according to claim 12 further comprising the step of providing the total thickness of the aluminized coating and the thickness of the IDL to a controller of an annealing furnace, wherein the controller adjusts a temperature and processing time of the hot stamped part in the annealing furnace based on at least one of the total thickness of the aluminized coating and the thickness of the IDL.

15. The method according to claim 12 further comprising the step of providing the total thickness of the aluminized coating and the thickness of the IDL to a subsequent welding operation, wherein welding parameters are adjusted based on at least one of the total thickness of the aluminized coating and the thickness of the IDL.

16. A method of controlling a manufacturing operation for hot stamped parts comprising:
removing a sample from a hot stamped part for Glow Discharge Optical Emission Spectrometry (GDOES);
analyzing the sample using GDOES and plotting constituent element weight percentages versus depth on a graph;
determining points on the graph where constituent elements intersect,
wherein the points indicate the characteristics of the aluminized coating; and
providing the characteristics to a controller of the manufacturing operation, wherein the controller parameters of the manufacturing operation are based on at least one characteristic.

17. The method according to claim 16 , wherein the characteristics are selected from the group consisting of a total thickness of the aluminized coating, a thickness of an inter-diffusion layer (IDL), constituents of the aluminized coating, constituents of the hot stamped part, phase composition of the aluminized coating, surface oxidation, and weldability.

18. The method according to claim 16 , wherein the manufacturing operation is selected from the group consisting of an annealing operation, a shot-blasting operation, and a welding operation.

19. The method according to claim 16 , wherein the hot stamped part is coated with a eutectic AlSi 10 Fe 3 alloy, and an intersection between Aluminum and Carbon indicates the total thickness of the aluminized coating.

20. The method according to claim 16 , wherein the hot stamped part is coated with a eutectic AlSi10Fe3 alloy, and a difference between an intersection of Aluminum and Carbon and a second maximum Silicon wt. % indicates the thickness of the IDL.

Assignees

• Ford Global Tech Llc

Inventors

• Chiriac Constantin
• Sohmshetty Raj
• Bullard Elizabeth
• Engle James

Classifications

• G01N21/67 Primary

  using electric arcs or discharges · CPC title

• G01B11/0616

  of coating · CPC title

• G01N2021/8427

  Coatings · CPC title

• G01N21/8422

  Investigating thin films, e.g. matrix isolation method · CPC title

• G01N2203/0076

  Hardness, compressibility or resistance to crushing · CPC title