Treatment methods for silicon nanosheet surfaces
US-2024055265-A1 · Feb 15, 2024 · US
US10134602B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-10134602-B2 |
| Application number | US-201715403505-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jan 11, 2017 |
| Priority date | Jan 14, 2016 |
| Publication date | Nov 20, 2018 |
| Grant date | Nov 20, 2018 |
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A process for smoothing a silicon-on-insulator structure comprising the exposure of a surface of the structure to an inert or reducing gas flow and to a high temperature during a heat treatment includes performing a first heat treatment step at a first temperature and under a first gas flow defined by a first flow rate, and performing a second heat treatment step at a second temperature lower than the first temperature and under a second gas flow defined by a second flow rate lower than the first flow rate.
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What is claimed is: 1. A method for smoothing a silicon-on-insulator structure comprising the exposure of a surface of the structure to an inert or reducing gas flow and to a high temperature during a heat treatment, the method comprising: a first heat treatment step at a first temperature greater than a threshold temperature which is between 1150° C. and 1170° C., and under a first gas flow defined by a first flow rate greater than 20 slm; and a second heat treatment step at a second temperature lower than the first temperature and the threshold temperature and greater than 1130° C., and under a second gas flow defined by a second flow rate lower than the first flow rate and less than 15 slm. 2. The method of claim 1 , further comprising a preliminary step of supplying the SOI structure comprising a thin surface layer positioned on a dielectric layer, the dielectric layer positioned on a carrier substrate, the surface layer having a thickness of less than 500 nm. 3. The method of claim 1 , wherein the first temperature is between 1160° C. and 1200° C. 4. The method of claim 3 , wherein the first temperature is between 1170° C. and 1200° C. 5. The method of claim 1 , wherein the second temperature is between 1130° C. and 1160° C. 6. The method of claim 1 , wherein the second heat treatment step comprises a hold at the second temperature of a given duration. 7. The method of claim 6 , wherein the duration of the hold is between 5 minutes and 2 hours. 8. The method of claim 1 , wherein the second heat treatment step comprises a temperature decrease ramp, starting from the second temperature, at a decrease ramp rate of between 0.1°/minute and 20°/minute. 9. The method of claim 1 , wherein the second flow rate is about 5 slm. 10. The method of claim 9 , wherein the inert gas is selected from argon or a mixture of argon and hydrogen. 11. The method of claim 1 , wherein the first heat treatment step and second heat treatment step are linked together during the same heat treatment. 12. The method of claim 1 , wherein the first temperature is greater than a threshold temperature and the second temperature is lower than the threshold temperature, the threshold temperature being between 1150° C. and 1170° C. 13. The method of claim 1 , wherein the second temperature is between 1130° C. and 1170° C. 14. The method of claim 1 , wherein the second heat treatment step comprises a hold at the second temperature of a given duration. 15. The method of claim 1 , wherein the first flow rate is greater than 20 slm, and wherein the second flow rate is less than 15 slm. 16. The method of claim 1 , wherein the inert gas is selected from argon or a mixture of argon and hydrogen. 17. The method of claim 1 , wherein the first heat treatment step and second heat treatment step are linked together during the same heat treatment. 18. The method of claim 1 , wherein the surface of the structure is smoothened and dissolution of an insulator layer occurs during the first heat treatment.
Thermal treatments, e.g. annealing or sintering · CPC title
with separation or delamination along an ion implanted layer, e.g. Smart-cut · CPC title
Semiconductor-on-insulator [SOI] isolation regions, e.g. buried oxide regions of SOI wafers · CPC title
for altering the shape of semiconductors, e.g. smoothing the surface · CPC title
Preparing SOI wafers · CPC title
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