Methods for the desolventization of bagasse

Patent metadata

Field	Value
Publication number	US-10132563-B2
Application number	US-201715424224-A
Country	US
Kind code	B2
Filing date	Feb 3, 2017
Priority date	Jun 18, 2012
Publication date	Nov 20, 2018
Grant date	Nov 20, 2018

Abstract

Provided herein are methods for the removal of organic solvents from wet bagasse. The use of the methods result in dried bagasse that contains no more than 1 weight percent organic solvents.

First claim

What is claimed is:

1. A method for removing organic solvents from wet guayule guayule bagasse comprising:
utilizing a quantity of wet guayule bagasse that contains up to 45 weight % combined organic solvents and water (based upon the total weight of the wet guayule bagasse) and no more than 0.1 weight % rubber;
heating the wet guayule bagasse to a temperature of at least 100° C. utilizing a dryer apparatus containing multiple layers, circulating heated air through the layers, and passing the wet guayule bagasse from one layer to another whereby the organic solvents are evaporated;
producing dried guayule bagasse that contains no more than 1 weight % organic solvents.

2. The method of claim 1 , wherein the heating occurs for no more than 10 minutes at a temperature of at least 110° C.

3. The method of claim 1 , wherein the heating occurs for no more than 8 minutes at a temperature of 125° C.

4. The method of claim 1 , wherein the heating occurs for no more than 7 minutes at a temperature of at least 125° C.

5. The method of claim 1 , wherein the dried guayule bagasse contains no more than 0.5 weight % organic solvents.

6. The method of claim 1 , wherein the wet guayule bagasse remains in the apparatus for 5-90 minutes.

7. The method of claim 1 , wherein the heating is achieved by heated steam.

8. The method of claim 1 , further comprising condensing the evaporated organic solvents and collecting them separately from the dried guayule bagasse.

9. The method of claim 1 , further comprising compressing the dried guayule bagasse into a briquette having a density that is at least 40% greater than the density of the non-compressed dried guayule bagasse.

10. The method of claim 1 , wherein the combined solvents are acetone and hexane.

11. The method of claim 9 , wherein the combined solvents are acetone and hexane.

12. The method of claim 1 , wherein the wet guayule bagasse is heated to a temperature of between 100 and 200° C.

13. A method for removing organic solvents from wet guayule bagasse comprising:
utilizing a quantity of wet guayule bagasse that contains up to 45 weight % combined organic solvents and water (based upon the total weight of the wet guayule bagasse) and no more than 0.1 weight % rubber;
heating the wet guayule bagasse to a temperature of at least 100° C. utilizing a dryer apparatus containing multiple paddles for mixing the wet guayule bagasse with heated air to evaporate the organic solvents;
producing dried guayule bagasse that contains no more than 1 weight % organic solvents.

14. The method of claim 13 , wherein the heating occurs for no more than 10 minutes at a temperature of at least 110° C.

15. The method of claim 13 , wherein the wet guayule bagasse remains in the apparatus for 5-90 minutes.

16. The method of claim 13 , further comprising condensing the evaporated organic solvents and collecting them separately from the dried guayule bagasse.

17. The method of claim 13 , further comprising compressing the dried guayule bagasse into a briquette having a density that is at least 40% greater than the density of the non-compressed dried guayule bagasse.

18. The method of claim 13 , wherein the combined solvents are acetone and hexane.

19. The method of claim 17 , wherein the combined solvents are acetone and hexane.

20. A method for removing organic solvents from wet guayule bagasse comprising:
utilizing a quantity of wet guayule bagasse that contains up to 45 weight % combined organic solvents and water (based upon the total weight of the wet guayule bagasse) and no more than 0.1 weight % rubber;
heating the wet guayule bagasse to a temperature of at least 100° C. utilizing a desolventization screw extruder apparatus;
producing dried guayule bagasse that contains no more than 1 weight % organic solvents.

21. The method of claim 20 , wherein the heating occurs for no more than 10 minutes at a temperature of at least 110° C.

22. The method of claim 20 , wherein the wet guayule bagasse remains in the apparatus for 5-90 minutes.

23. The method of claim 20 , further comprising condensing the evaporated organic solvents and collecting them separately from the dried guayule bagasse.

24. The method of claim 20 , further comprising compressing the dried guayule bagasse into a briquette having a density that is at least 40% greater than the density of the non-compressed dried guayule bagasse.

25. The method of claim 20 , wherein the combined solvents are acetone and hexane.

26. The method of claim 24 , wherein the combined solvents are acetone and hexane.

Assignees

• Bridgestone Corp

Inventors

• Huang Yingyi
• Smale Mark W
• Cole William M

Classifications

• F26B21/471

  condensing vapours onto the surface of the materials to be dried · CPC title

• F26B3/04 Primary

  the gas or vapour circulating over or surrounding the materials or objects to be dried (F26B3/14 takes precedence) · CPC title

• C08H99/00

  Subject matter not provided for in other groups of this subclass {, e.g. flours, kernels} · CPC title

• C08C4/00 Primary

  Treatment of rubber before vulcanisation, not provided for in groups C08C1/00 - C08C3/02 · CPC title

• C09K3/00

  Materials not provided for elsewhere · CPC title