Methods for desolventization of bagasse

Patent metadata

Field	Value
Publication number	US-9562720-B2
Application number	US-201314409132-A
Country	US
Kind code	B2
Filing date	Jun 18, 2013
Priority date	Jun 18, 2012
Publication date	Feb 7, 2017
Grant date	Feb 7, 2017

Abstract

Provided herein are methods for the removal of organic solvents from wet bagasse. The use of the methods result in dried bagasse that contains no more than 1 weight percent organic solvents.

First claim

What is claimed is:

1. A method for removing organic solvents from wet bagasse comprising:
utilizing a quantity of wet bagasse that contains up to 45 weight % combined organic solvents and water (based upon the total weight of the wet bagasse) and no more than 0.1 weight % rubber;
heating the wet bagasse to a temperature of at least 100° C. whereby the organic solvents are evaporated;
producing dried bagasse that contains no more than 1 weight % organic solvents.

2. The method according to claim 1 where the bagasse is from guayule shrub.

3. The method according to claim 1 , wherein the heating takes place in an apparatus selected from the following:
i. a dryer containing multiple layers, circulating heated air through the layers of the apparatus and passing the wet guayule bagasse from one layer to another whereby the organic solvents are evaporated;
ii. a dryer containing multiple paddles for mixing the wet bagasse with heated air to evaporate the organic solvent; or
iii. a desolventization screw extruder, producing dried guayule bagasse that contains no more than 1 weight % organic solvents.

4. The method according to claim 1 , wherein the heating occurs for no more than 10 minutes at a temperature of at least 110° C.

5. The method according to claim 1 , wherein the dried bagasse contains no more than 0.5 weight % organic solvent.

6. The method according to claim 3 , wherein the heating utilizes apparatus (i).

7. The method according to claim 6 , wherein the heated air has a temperature of 100-150° C.

8. The method according to claim 1 , wherein the wet bagasse remains in the apparatus for 5-90 minutes.

9. The method according to claim 1 , wherein the heating is achieved by heated steam.

10. The method according to claim 1 , further comprising condensing the evaporated organic solvents and collecting them separately from the dried bagasse.

11. The method according to claim 1 , further comprising compressing the dried bagasse into a briquette having a density that is at least 40% greater than the density of the non-compressed dried bagasse.

12. The method according to claim 1 , wherein the combined solvents are acetone and hexane.

13. The method according to claim 7 , wherein the dried bagasse contains no more than 0.2 weight % organic solvent.

14. A method for removing organic solvents from wet guayule bagasse comprising:
utilizing a quantity of wet guayule bagasse that contains up to 45 weight % combined organic solvents and water (based upon the total weight of the wet bagasse) and no more than 0.1 weight % rubber;
heating the wet guayule bagasse to a temperature of at least 100° C. whereby the organic solvents are evaporated;
producing dried guayule bagasse that contains no more than 1 weight % organic solvents,
wherein the heating takes place in an apparatus selected from the following:
i. a dryer containing multiple layers, circulating heated air through the layers of the apparatus and passing the wet guayule bagasse from one layer to another whereby the organic solvents are evaporated;
ii. a dryer containing multiple paddles for mixing the wet guayule bagasse with heated air to evaporate the organic solvent; or
iii. a desolventization screw extruder, producing dried guayule bagasse that contains no more than 1 weight % organic solvents.

15. The method according to claim 14 , wherein the heating occurs for no more than 10 minutes at a temperature of at least 110° C.

16. The method according to claim 14 , wherein the dried guayule bagasse contains no more than 0.5 weight % organic solvent.

17. The method according to claim 14 , further comprising condensing the evaporated organic solvents and collecting them separately from the dried guayule bagasse.

18. The method according to claim 14 , further comprising compressing the dried guayule bagasse into a briquette having a density that is at least 40% greater than the density of the non-compressed dried guayule bagasse.

19. The method according to claim 14 , wherein the combined solvents are acetone and hexane.

20. The method according to claim 16 , wherein the combined solvents are acetone and hexane.

Assignees

• Bridgestone Corp

Inventors

• Huang Yingyi
• Smale Mark W
• Cole William M

Classifications

• F26B21/471

  condensing vapours onto the surface of the materials to be dried · CPC title

• F26B3/04 Primary

  the gas or vapour circulating over or surrounding the materials or objects to be dried (F26B3/14 takes precedence) · CPC title

• C08C4/00 Primary

  Treatment of rubber before vulcanisation, not provided for in groups C08C1/00 - C08C3/02 · CPC title

• C08H99/00

  Subject matter not provided for in other groups of this subclass {, e.g. flours, kernels} · CPC title

• C08C1/04

  Purifying; Deproteinising · CPC title