Horizontal heat treatment device

Patent metadata

Field	Value
Publication number	US-10132008-B2
Application number	US-201314376979-A
Country	US
Kind code	B2
Filing date	Feb 7, 2013
Priority date	Feb 7, 2012
Publication date	Nov 20, 2018
Grant date	Nov 20, 2018

Abstract

A horizontal heat treatment device continuously subjects an untreated continuous flat object to heat treatment while horizontally transferring the untreated object within a heat treatment chamber. Seal chambers are interconnected to the untreated-object loading opening and treated-object unloading opening of the heat treatment chamber. A passage is connected to an opening of each of the seal chambers, the opening located on the side opposite the heat treatment chamber. The untreated-object passage loading opening interconnected to the untreated-object seal chamber loading opening and the treated-object passage unloading opening interconnected to the treated-object seal chamber unloading opening are the untreated-object loading opening and treated-object unloading opening of the heat treatment device. A pair of gas ejection nozzles are provided at upper and lower positions of the passages. The nozzles eject gas in specific directions, and the nozzle openings have a specific shape, a direction, and a length.

First claim

The invention claimed is:

1. A horizontal heat treatment device configured to continuously heat-treats a continuous flat object, while transporting the object within a heat treatment chamber in a horizontal direction,
wherein a seal chamber connected to an exhaust fan is connected to each of object loading opening and unloading opening of the heat treatment chamber, and the seal chamber is configured so that the object can pass through the seal chamber in the horizontal direction,
a passage having a rectangular cross-section is connected to an opening of the object loading opening and unloading opening of each seal chamber located on a side opposite to the heat treatment chamber, and the passage is configured so that the object can pass through the passage in the horizontal direction,
the seal chamber is located between the heat treatment chamber and the passage,
the object loading opening of the passage connected to the seal chamber object loading opening is an object loading opening of the heat treatment device, and the object unloading opening of the passage connected to the seal chamber object unloading opening is an object unloading opening of the heat treatment device,
a pair of nozzles configured to eject gas is provided at upper and lower positions of each passage,
a gas ejection opening of each nozzle has a rectangular shape,
in each passage, the pair of nozzles provided in the passage ejects the gas toward a center in the vertical direction of the passage, and toward the object loading opening or the object unloading opening of the heat treatment device included in the passage,
in each passage, the gas ejection opening of each nozzle provided in the passage is parallel to a long-side direction of the loading opening and the unloading opening of the object of the passage, and has a length equal to a length of the long side, and
in each passage, a distance d, which is greater than 0, between the gas ejection opening of the pair of nozzles provided in the passage and the object loading opening or the object unloading opening of the heat treatment device included in the passage, and a height Dn of the passage satisfy a relation of 2 mm≤d<0.75 Dn.

2. The horizontal heat treatment device according to claim 1 , wherein in each passage, the distance d is 15 mm or more.

3. The horizontal heat treatment device according to claim 1 , wherein in each passage, an opening width Wn of the nozzle is 0.5 mm or more and 3 mm or less, and the height Dn of the passage is 20 mm or more and 78 mm or less.

4. The horizontal heat treatment device according to claim 1 , wherein the passages are each provided at multiple positions in the vertical direction so that the object can be transported in the horizontal direction at the multiple positions in the vertical direction, respectively, and
the seal chamber is partitioned so as to correspond to each of the passages.

5. The horizontal heat treatment device according to claim 1 , further comprising:
a gas flow rate control mechanism capable of adjusting an amount of ejection of gas for each nozzle.

6. The horizontal heat treatment device according to claim 1 ,
wherein the passage is formed by an upper passage member, a lower passage member, and a lateral surface member,
each of the upper and lower passage members has two members with the nozzle interposed therebetween, and
the two members are integrated with a spacer member configured to determine a nozzle gap while interposing the spacer member therebetween.

7. The horizontal heat treatment device according to claim 1 , wherein the two members and the spacer member are freely attachable and detachable.

8. The horizontal heat treatment device according to claim 1 , wherein the device is a heat treatment furnace that heat-treats the carbon fiber precursor fiber bundle.

9. A method of manufacturing a flame-resistant fiber bundle that heat-treats a carbon fiber precursor fiber bundle by a horizontal heat treatment device to manufacture a flame-resistant fiber bundle,
wherein the horizontal heat treatment device is a horizontal heat treatment device that continuously heat-treats a continuous flat object, while transporting the object within a heat treatment chamber in a horizontal direction,
a seal chamber connected to an exhaust fan is connected to each of object loading opening and unloading opening of the heat treatment chamber, and the seal chamber is configured so that the object can pass through the seal chamber in the horizontal direction,
a passage having a rectangular cross-section is connected to an opening of the object loading opening and unloading opening of each seal chamber located on a side opposite to the heat treatment chamber, and the passage is configured so that the object can pass through the passage in the horizontal direction,
the seal chamber is located between the heat treatment chamber and the passage,
the object loading opening of the passage connected to the seal chamber object loading opening is an object loading opening of the heat treatment device, and the object unloading opening of the passage connected to the seal chamber object unloading opening is an object unloading opening of the heat treatment device,
a pair of nozzles configured to eject the gas is provided at upper and lower positions of each passage,
a gas ejection opening of each nozzle has a rectangular shape,
in each passage, the pair of nozzles provided in the passage ejects gas toward a center in the vertical direction of the passage, and toward the object loading opening or the object unloading opening of the heat treatment device included in the passage,
in each passage, the gas ejection opening of each nozzle provided in the passage is parallel to a long side direction of the loading opening and the unloading opening of the object of the passage, and has a length equal to a length of the long side, and
in each passage, a distance d, which is greater than 0, between the gas ejection opening of the pair of nozzles provided in the passage and the object loading opening or the object unloading opening of the heat treatment device included in the passage, and a height Dn of the passage satisfy a relation of 2 mm≤d<0.75 Dn,
the method comprising:
setting a negative pressure in the seal chamber using the exhaust fan; and
ejecting the gas from each nozzle so that a relation of V≤−30×P+21 is satisfied, when an amount of gas ejection of each nozzle provided in the passage per long side 1 m of the loading opening and the unloading opening of the object of the passage is expressed as V (m 3 /h), and a gauge pressure in the seal chamber connected to the passage is expressed as P (Pa) in each passage.

10. The method of manufacturing a flame-resistant fiber bundle according to claim 9 , wherein a flow velocity Vo of the gas flowing into the seal chamber from each passage is set to 0.1 m/s or more and 0.5 m/s or less.

11. The method of manufacturing a flame-resistant fiber bundle according to claim 9 , wherein an ejection velocity Vs of the gas ejected from each nozzle is set to 3 m/s or more and 30 m/s or less.

12. A method of manufacturing a carbon fiber bundle comprising:
a step of manufacturing a flame-resistant fiber bundle by the method of manufacturing the flame-resistant fiber bundle according to claim 9 ; and
a step of carbonizing the flame-resistant fiber bundle.

13. A heat treatment method of continuously heat-treating a continuous flat object using the horizontal heat treatment device according to claim 1 .

14. The method according to claim 9 , further comprising:
dividing the seal chamber into a plurality of separate partitions

Assignees

• Mitsubishi Rayon Co
• Mitsubishi Chem Corp

Inventors

• Mizuno Keishi
• Yasunami Tetsu
• Kawamura Atsushi
• Hatanaka Youji
• Yamamoto Nobuyuki
• Inada Hiromasa

Classifications

• D02J13/001

  in a tube or vessel · CPC title

• F27B2009/382

  Charging · CPC title

• D01F9/32 Primary

  Apparatus therefor · CPC title

• F27D99/0075

  Gas curtain seals · CPC title

• F27B2009/384

  Discharging · CPC title