Method for preparing aluminum nitride

Patent metadata

Field	Value
Publication number	US-10112833-B2
Application number	US-201715429340-A
Country	US
Kind code	B2
Filing date	Feb 10, 2017
Priority date	Nov 28, 2016
Publication date	Oct 30, 2018
Grant date	Oct 30, 2018

Abstract

A method for producing aluminum nitride is to disclose, which includes injecting a nitrogen-containing gas and a pure aluminum material into a high-temperature jet mill. In the high-temperature jet mill, the injected pure aluminum material reacts with the nitrogen and forms aluminum nitride on the surface. The aluminum nitride is continuously to pulverize in the high-temperature jet mill to form fine aluminum nitride powder. According to the present disclosure, unnecessary cost and complicated processes in elevated-temperature agglomeration is to avoid.

First claim

What is claimed is:

1. A method for preparing aluminum nitride, consisting of steps of:
(a) injecting a nitrogen-containing gas and a pure aluminum material into a pulverizing chamber operating in vacuum in a high-temperature jet mill by a high-pressure air to form a high-speed airflow;
(b) melting the pure aluminum material into a liquid status of the pure aluminum in the pulverizing chamber in the high-temperature jet mill;
(c) allowing the liquid status of the pure aluminum material to react with the nitrogen and form aluminum nitride on the surface of the pure aluminum material in the pulverizing chamber in the high-temperature jet mill;
(d) pulverizing the formed aluminum nitride into aluminum nitride powder and removing the aluminum nitride powder from the surface of the pure aluminum material by the high-speed airflow in the pulverizing chamber in the high-temperature jet mill;
(e) exposing the remaining liquid status of the pure aluminum material to the nitrogen-containing gas in the pulverizing chamber in the high-temperature jet mill; and
(f) repeating steps (c) to (e) in the pulverizing chamber in the high-temperature jet mill until all the liquid status of the pure aluminum material is completely consumed.

2. The method for producing aluminum nitride according to claim 1 , wherein the nitrogen-containing gas further contains argon or other noble gases.

Assignees

• Univ Nat Tsing Hua

Inventors

• Chen Swe-Kai

Classifications

• C01B21/0722 Primary

  Preparation by direct nitridation of aluminium · CPC title