Classification method of particulate water absorbent resin

Patent metadata

Field	Value
Publication number	US-10099254-B2
Application number	US-53290908-A
Country	US
Kind code	B2
Filing date	Mar 24, 2008
Priority date	Mar 26, 2007
Publication date	Oct 16, 2018
Grant date	Oct 16, 2018

Abstract

A particulate water absorbent resin is obtained by polymerizing an unsaturated monomer so as to form a cross-linked polymer hydrogel and drying and pulverizing the cross-linked polymer hydrogel, and plural classification steps different from each other are carried out so as to remove fine powder. In this manner, the present invention provides the method for classification of particulate water absorbent resin which method allows particulate water absorbent resin having a desired particle diameter range to be efficiently obtained at low cost while securing the high productivity even in case where a larger production equipment is used.

First claim

The invention claimed is:

1. A method for classification of particulate water absorbent resin obtained by polymerizing an unsaturated monomer so as to form a cross-linked polymer hydrogel and drying and pulverizing the cross-linked polymer hydrogel,
said method comprising:
a first classification step in which a first screen and a gravity are used; and
a second classification step in which a second screen device and an aerial current are used,
the first classification step and the second classification step being carried out continuously,
the first and the second classification steps being different from each other so as to remove fine powder,
the first classification step being carried out by using a sieving device at a temperature ranging from 30° C. to 100° C., and
the particulate water absorbent resin, having been classified by the first classification step and having passed through the first screen, being further classified by the second classification step and passing through the second screen so as to remove fine powder,
whereby an amount of particulate water absorbent resin classified in second classification step is smaller than that in the first classification step; and
wherein the sieving device used in the first classification step and the second screen device used in the second classification step differ from each other
wherein a mesh size of the first screen is 150 μm or more and 300 μm or less, and
wherein a mesh size of the second screen is 106 μm or more and 180 μm or less
the sieving device is used at a temperature which is lower than a temperature of the particulate water absorbent resin so that the temperature difference therebetween is within 20° C. and
wherein, in the first classification step, a differential pressure equal to or more than 10 mm H 2 O is provided between an area where the particulate water absorbent resin has not passed through the screen and an area where the particulate water absorbent resin has passed through the screen so as to remove fine powder.

2. The method as set forth in claim 1 , wherein the plural classification steps are applied to a line for continuously producing particulate water absorbent resin so that a production amount is 500 kg/hr or more for each line.

3. The method as set forth in claim 1 , wherein a pneumatic classifier having the second screen is used in the second classification step.

4. The method as set forth in claim 1 , wherein a difference between the mesh size of the first screen and the mesh size of the second screen is 30 μm or more and 200 μm or less.

5. The method as set forth in claim 1 , wherein particles whose particle diameter is less than 180 μm are classified from the particulate water absorbent resin in the first classification step, and particles whose particle diameter is 106 μm or more are classified from the particles whose particle diameter is less than 180 μm in the second classification step.

6. The method as set forth in claim 1 , wherein particles whose particle diameter is less than 180 μm are classified from the particulate water absorbent resin in the first classification step, and particles whose particle diameter is 150 μm or more are classified from the particles whose particle diameter is less than 180 μm in the second classification step.

Assignees

• Konishi Kazumasa
• Kadonaga Kenji
• Dairoku Yorimichi
• Fujino Shinichi
• Nippon Catalytic Chem Ind

Inventors

• Konishi Kazumasa
• Kadonaga Kenji
• Dairoku Yorimichi
• Fujino Shinichi

Classifications

• C08J3/122

  Pulverisation by spraying · CPC title

• B07B9/00 Primary

  Combinations of apparatus for screening or sifting or for separating solids from solids using gas currents; General arrangement of plant, e.g. flow sheets · CPC title

• C08J2300/00

  Characterised by the use of unspecified polymers · CPC title

• C08J3/12

  Powdering or granulating · CPC title