Dry milk formula and method and system for preparing same

Patent metadata

Field	Value
Publication number	US-9993009-B2
Application number	US-201414782130-A
Country	US
Kind code	B2
Filing date	Apr 3, 2014
Priority date	Apr 3, 2013
Publication date	Jun 12, 2018
Grant date	Jun 12, 2018

Abstract

A process and system is shown for obtaining a dry milk formula, having (a-i) ultrafiltration of an animal skim milk composition having 70-90 wt % casein and 10-30 wt % whey proteins, based on total protein, and (a-ii) ultrafiltration of an animal whey composition having 0-25 wt % casein and 75-100 wt % whey proteins, based on total protein; or (a-iii) ultrafiltration of a mixture of the compositions of (a-i) and (a-ii), (b) removing polyvalent ions from the UF permeate originating from step (a-i) and/or (a-ii) or (a-iii) to obtain at least one softened UF permeate; (c) combining the at least one softened UF permeate with a UF retentate to obtain a combined product; and (d) drying the combined product to obtain a dry milk formula.

First claim

The invention claimed is:

1. A process for obtaining a dry milk formula, comprising:
(a) ultrafiltering (UF)
(a-i) an animal skim milk composition comprising 70-90 wt % casein and 10-30 wt % whey proteins, based on total protein, and
(a-ii) an animal whey composition comprising 0-25 wt % casein and 75-100 wt % whey proteins, based on total protein; and
(b) optionally, combining of the UF retentate originating from step (a-i) with the UF retentate originating from step (a-ii);
or
(a-iii) a mixture of the compositions of (i) animal skim milk composition comprising 70-90 wt % casein and 10-30 wt % whey proteins, based on total protein, and (ii) animal whey composition comprising 0-25 wt % casein and 75-100 wt % whey proteins, based on total protein,

(c) removing polyvalent ions
(c-i) from the UF permeate originating from step (a-i) and/or the UF permeate originating from step (a-ii); or
(c-ii) from the UF permeate originating from step (a-iii)
to obtain at least one softened UF permeate;

(d) combining
(d-i) the at least one softened UF permeate originating from step (c-i) with a UF retentate originating from step (a-i) and/or (a-ii); or
(d-ii) the softened UF permeate originating from step (c-ii) with a UF retentate originating from (a-iii); or
(d-iii) the at least one softened UF permeate originating from step (c-i) with the UF retentate originating from step (b)
to obtain a combined product; and

(e) drying
(e-i) the combined product originating from step (d); or
(e-ii) drying any of (i)-(iii):
(i) the UF retentate originating from step (a-i) and the UF retentate originating from step (a-ii); or
(ii) the UF retentate originating from step (a-iii); or
(iii) the UF retentate originating from step (b),
prior to the combining in step (d);
and drying any of the softened UF permeates originating from step (c) prior to the combining in step (d), followed by combining the dried UF retentate with the dried softened UF permeate in step (d); or

(e-iii) drying one of (i)-(iv)
the UF retentate originating from step (a-i) and/or the UF retentate originating from step (a-ii);
(ii) the UF retentate originating from step (a-iii);
(iii) the UF retentate originating from step (b),
(iv) the UF
followed by subjecting the dried composition to the combining in step (d) and then dry the combined product originating from step (d),

to obtain a dry milk formula.

2. The process according to claim 1 , wherein the animal skim milk comprises 75-85 wt % casein and 15-25 wt % whey proteins, based on total protein.

3. The process according to claim 1 , wherein the animal whey composition comprises 0-20 wt % casein and 80-100 wt % whey proteins, based on total protein.

4. The process according to claim 1 , wherein a UF permeate originating from step (a-i) and a UF permeate originating from step (a-ii) are combined prior to said removal of polyvalent ions of step (c).

5. The process according to claim 1 , wherein a UF retentate originating from step (a-i) and/or (a-ii) is/are concentrated prior to the combining of step (b), prior to the combining of step (d) or prior to the drying of step (e).

6. The process according to claim 1 , wherein the UF permeate originating from step (a-i) is combined with a permeate originating from (a-ii) prior to polyvalent ion removal of step (c).

7. The process according to claim 1 , wherein the softened UF permeate originating from step (c) is concentrated prior to the combining of step (d) or the drying of step (e-i), and/or the combined product of step (d) is concentrated, prior to the drying of step (e).

8. The process according to claim 5 , wherein concentration occurs by reverse osmosis and/or nanofiltration.

9. The process according to claim 1 , wherein polyvalent ion removal of step (c) occurs by electrodialysis, ion exchange, lactose crystallization and/or salt precipitation.

10. The process according to claim 1 , wherein the softened UF permeate of step (c) is subjected to monovalent ion removal; and/or one of (i)-(iii) is subjected to monovalent ion removal:
(i) the UF retentate originating from step (a-i) and/or (a-ii); or
(ii) the UF retentate originating from step (a-iii); or
(iii) the UF retentate originating from step (b).

11. The process according to claim 1 , wherein a UF retentate and/or a UF permeate is heat treated by DSI prior to the drying of step (e), wherein the UF retentate is selected from:
(i) the UF retentate originating from step (a-i) and/or (a-ii);
(ii) the UF retentate originating from step (a-iii); and
(iii) the UF retentate originating from step (b),

and the UF permeate is selected from:
(iv) the UF permeate originating from step (a-i) and/or (a-ii); and
(v) the UF permeate originating from step (a-iii).

12. The process according to claim 1 , wherein drying of step (e) is by spray-drying.

13. The process according to claim 1 , wherein the combined product originating from step (d) or the dried combined product of (e) is further processed into a nutritional product for providing nutrition to infants.

14. The process according to claim 1 , wherein the animal skim milk composition and animal whey composition are combined in such a ratio that a product is obtained having a casein:whey protein weight ratio of between 75:25 to 30:70, wherein the combining occurs prior to step (a-iii), in step (b) or in step (d).

15. The process according to claim 1 , wherein
(i) the mixture of the animal skim milk composition and animal whey composition which is subjected to step (a-iii);
(ii) the combined UF retentate of step (b);
(iii) the combined product of step (d); or
(iv) the dry milk formula of (e) has a casein:whey protein weight ratio of between 75:25 to 30:70.

16. A composition, comprising: a protein content of between 40 and 52 wt %, wherein casein and whey are present in a weight ratio which lies between 70:30 and 30:70, lactose in an amount of between 35 and 50 wt %; and the following minerals: magnesium in an amount of between 0.01 and 0.30 wt %, calcium in an amount of between 0.80 and 1.70 wt %, phosphorus in an amount of between 0.60 and 1.50 wt %, sodium in an amount of between 0.10 and 0.60 wt %, chloride in an amount of between 0.05 and 0.60 wt % and potassium in an amount of between 0.60 and 1.50 wt %, all based on dry weight of the composition.

17. A composition, comprising: a protein content of between 16 and 24 wt %, wherein casein and whey are present in a weight ratio which lies between 70:30 and 30:70, lactose in an amount of between 65 and 80 wt %; and the following minerals: magnesium in an amount of between 0.01 and 0.25 wt %, calcium in an amount of between 0.20 and 0.80 wt %, phosphorus in an amount of between 0.40 and 0.80 wt %, sodium in an amount of between 0.20 and 0.80 wt %, chloride in an amount of between 0.30 and 0.90 wt % and potassium in an amount of between 0.30 and 0.90 wt % all based on dry weight of the composition.

18. A dry milk formula obtainable by the process according to claim 1 .

19. A modular system, comprising:
(1) an ultrafiltration module, comprising
(1a) an inlet for receiving a first liquid composition and/or a second liquid composition, or a mixture thereof, to a first side of an ultrafiltration membrane,
(1b) the ultrafiltration membrane,
(1c) a first outlet for discharging an ultrafiltration retentate (UFR) from the first side of the ultrafiltration membrane, and
(1d) a second outlet for discharging an ultrafiltration permeate (UFP) from the second side of the ultrafiltration membrane;

(

Assignees

• Nutricia Nv

Inventors

• Tobin John
• Chiaranaipanich Jitti
• Verdurmen Rudolph Eduardus Maria
• Janssen Antonius Hendricus
• Rabartin Olivier Bertrand
• Moonen Raoul Charles Johan
• Van Der Hoeven Martijn Johannes

Classifications

• A23L33/00

  Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof · CPC title

• A23C9/142

  by dialysis, reverse osmosis or ultrafiltration (A23C9/144 takes precedence) · CPC title

• A23L33/40

  Complete food formulations for specific consumer groups or specific purposes, e.g. infant formula · CPC title

• A23C9/1512 Primary

  containing isolated milk or whey proteins, caseinates or cheese; Enrichment of milk products with milk proteins in isolated or concentrated form, e.g. ultrafiltration retentate · CPC title

• A23C9/144

  by electrical means, e.g. electrodialysis · CPC title