Flexible-to-rigid tubing

Patent metadata

Field	Value
Publication number	US-9894754-B2
Application number	US-201715423709-A
Country	US
Kind code	B2
Filing date	Feb 3, 2017
Priority date	Aug 27, 2010
Publication date	Feb 13, 2018
Grant date	Feb 13, 2018

Abstract

A flexible-to-rigid tube is flexible when routed and is then rigidized to increase burst strength. According to the preferred embodiments of the present invention, the flexible-to-rigid tube is included in a cooling plate assembly for transferring heat from electronic components mounted on a circuit board. In one embodiment, the flexible-to-rigid tube (while in a flexible state) includes a polydimethylsiloxane (PDMS) or other silicone containing pendant or terminal epoxy, vinyl and/or acrylate functional groups and an initiator (e.g., a sulfonium salt photoinitiator, a free radical photoinitiator, or a thermal initiator). In another embodiment, triallyl isocyanurate (TAIC) and an initiator are incorporated into a conventional PVC-based tubing material. The flexible-to-rigid tube changes from the flexible state to a rigid state via formation of a cross-linked network upon exposure to actinic radiation or heat.

First claim

What is claimed is:

1. A method of utilizing a multi-layer flexible-to-rigid tube to interconnect an outlet port of a first component and an inlet port of a second component, comprising the steps of:
routing the multi-layer flexible-to-rigid tube in a flexible state, wherein the multi-layer flexible-to-rigid tube comprises a first end configured to be slid over and clamped to a tubular fitting that defines the outlet port of the first component, a second end configured to be slid over and clamped to a tubular fitting that defines the inlet port of the second component, an inner liner having a composition comprising polyvinyl chloride, and a crosslinkable jacket extruded over the inner liner and having a composition comprising polyvinyl chloride and triallyl isocyanurate (TAIC), wherein the jacket changes from a flexible state to a rigid state via formation of a cross-linked network upon exposure of the jacket to actinic radiation or heat to increase the flexural modulus and burst strength of the multi-layer flexible-to-rigid tube, and wherein the routing step includes routing the multi-layer flexible-to-rigid tube, while the jacket is in the flexible state, between the outlet port of the first component and the inlet port of the second component so that the first end of the multi-layer flexible-to-rigid tube can be slid over and clamped to the tubular fitting of the first component and the second end of the multi-layer flexible-to-rigid tube can be slid over and clamped to the tubular fitting of the second component; and
rigidizing the multi-layer flexible-to-rigid tube after the routing step, wherein the rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to actinic radiation or heat to change the jacket to the rigid state via formation of the cross-linked network.

2. The method as recited in claim 1 , wherein the cross-linked network is a polymerization reaction product of:
triallyl isocyanurate (TAIC); and
an initiator selected from a group of initiators consisting of free radical photoinitiators and thermal initiators.

3. The method as recited in claim 2 , wherein the initiator comprises a free radical photoinitiator including benzoin, and wherein the rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to actinic radiation.

4. The method as recited in claim 2 , wherein the initiator comprises a thermal initiator including a benzoyl peroxide or azobisisobutyronitrile, and wherein rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to heat.

5. A method of utilizing a multi-layer flexible-to-rigid tube to interconnect an outlet port of a first component and an inlet port of a second component, comprising the steps of:
routing the multi-layer flexible-to-rigid tube in a flexible state, wherein the multi-layer flexible-to-rigid tube comprises a first end configured to be slid over and clamped to a tubular fitting that defines the outlet port of the first component, a second end configured to be slid over and clamped to a tubular fitting that defines the inlet port of the second component, an inner liner having a composition comprising polyvinyl chloride, and a crosslinkable jacket extruded over the inner liner and having a composition comprising polyvinyl chloride and triallyl isocyanurate (TAIC), wherein the jacket changes from a flexible state to a rigid state via formation of a cross-linked network upon exposure of the jacket to actinic radiation or heat to increase the flexural modulus and burst strength of the multi-layer flexible-to-rigid tube, and wherein the routing step includes routing the multi-layer flexible-to-rigid tube while the jacket is in the flexible state, between the outlet port of the first component and the inlet port of the second component, sliding and clamping the first end of the flexible-to-rigid tube over and to the tubular fitting of the first component, and sliding and clamping the second end of the flexible-to-rigid tube over and to the tubular fitting of the second component; and
rigidizing the multi-layer flexible-to-rigid tube after the routing step, wherein the rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to actinic radiation or heat to change the jacket to the rigid state via formation of the cross-linked network.

6. The method as recited in claim 5 , wherein the cross-linked network is a polymerization reaction product of:
triallyl isocyanurate (TAIC); and
an initiator selected from a group of initiators consisting of free radical photoinitiators and thermal initiators.

7. The method as recited in claim 6 , wherein the initiator comprises a free radical photoinitiator including benzoin, and wherein the rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to actinic radiation.

8. The method as recited in claim 6 , wherein the initiator comprises a thermal initiator including a benzoyl peroxide or azobisisobutyronitrile, and wherein rigidizing step includes the step of exposing the multi-layer flexible-to-rigid tube to heat.

Assignees

• IBM

Inventors

• Boday Dylan J
• Kuczynski Joseph
• Meyer Iii Robert E

Classifications

• H10W40/251

  Organics · CPC title

• H10W40/47 Primary

  by flowing liquids, e.g. forced water cooling · CPC title

• H10W40/40

  involving heat exchange by flowing fluids · CPC title

• H10W40/25

  characterised by their materials · CPC title

• H10W40/22

  characterised by their shape, e.g. having conical or cylindrical projections · CPC title