Process and apparatus for preparing pigment and wax dual dispersions

Patent metadata

Field	Value
Publication number	US-9890284-B2
Application number	US-201414254499-A
Country	US
Kind code	B2
Filing date	Apr 16, 2014
Priority date	Apr 16, 2014
Publication date	Feb 13, 2018
Grant date	Feb 13, 2018

Abstract

Disclosed herein are formulations and processes for the preparation of pigment and wax dual dispersions by (1) providing a solution comprising a water and at least one surfactant in a dispersion apparatus comprising a container, a rotor-stator homogenizer, and a piston homogenizer coupled via a recirculation device; (2) adding at least one pigment to the solution; (3) forming a pigment dispersion by flowing the at least one pigment and the solution to the rotor-stator homogenizer via the recirculation device; (4) adding at least one wax to the pigment dispersion; and (5) flowing the at least one wax and pigment dispersion to the piston homogenizer via the recirculation device until a pigment and wax dual dispersion is formed. Also disclosed herein are pigment and wax dual dispersions, as well as a dispersion apparatus for preparing pigment and wax dual dispersions. In certain embodiments, a dispersion apparatus for preparing a pigment and wax dual dispersion may comprise a container, a rotor-stator homogenizer, a piston homogenizer, and a recirculation device coupled to the container and the homogenizers that allows a dispersion to flow between the container and the homogenizers.

First claim

What is claimed is:

1. A process for preparing a pigment and wax dual dispersion comprising:
providing a solution comprising water and at least one surfactant in a dispersion apparatus comprising a container, a rotor-stator homogenizer, and a piston homogenizer coupled via a recirculation device;
adding at least one pigment to the solution in the container;
flowing the at least one pigment and solution from the container, through a first loop, and back to the container via the recirculation device to produce a pigment dispersion, wherein the first loop comprises a strainer, the rotor-stator homogenizer downstream from the strainer, and a heat exchanger downstream from the rotor-stator homogenizer, wherein the rotor-stator homogenizer reduces a particle size of the pigment dispersion to less than 125 nm, and wherein the heat exchanger reduces a temperature of the pigment dispersion;
stirring the pigment dispersion in the container;
adding at least one wax to the pigment dispersion in the container; and
flowing the wax and the pigment dispersion from the container, through a second loop, and back to the container via the recirculation device to produce the pigment and wax dual dispersion, wherein the second loop comprises the piston homogenizer, wherein the recirculation device in the second loop comprises a steam jacket, wherein the pigment and wax dual dispersion is exposed to a pressure in the piston homogenizer between 700 psi and 900 psi for a first period of time, and subsequently the pressure to which the pigment and wax dual dispersion is exposed in the piston homogenizer is between 5500 psi and 6500 psi for a second period of time.

2. The process according to claim 1 , wherein the at least one pigment is chosen from cyan pigments, and wherein the at least one pigment comprises solids in an amount less than 17%.

3. The process according to claim 1 , further comprising mixing the water and the at least one surfactant together with an agitator to provide the solution prior to adding the at least one wax.

4. The process according to claim 1 , wherein the at least one wax is chosen from polymethylene wax.

5. The process according to claim 1 , wherein the at least one surfactant is chosen from 60% sodium dodecyl benzene sulfonate.

6. The process according to claim 1 , wherein the pigment and wax dual dispersion is prepared at a temperature ranging from 120° C. to 130° C. and then subsequently cooled to ambient temperature.

7. The process according to claim 1 , wherein the at least one pigment is added in an amount of at least 20% by weight of the pigment dispersion.

8. The process according to claim 1 , wherein the pigment dispersion is recirculated through the rotor-stator homogenizer via the recirculation device at least 3 passes.

9. The process according to claim 1 , wherein the pigment dispersion is diluted with the water to an amount of less than 25% pigment solids by weight.

10. The process according to claim 1 , wherein the pigment dispersion is diluted with the water to an amount of less than 20% pigment solids by weight.

11. The process according to claim 1 , wherein the pigment and wax dual dispersion comprises the at least one pigment and the at least one wax in a combined amount greater than 20%, the at least one surfactant in an amount greater than 1%.

Assignees

• Xerox Corp

Inventors

• Qiu Shigang
• Damato Michael
• Lee Frank Ping Hay

Classifications

• B01F13/103

  Operations & Transport · mapped topic

• B01F3/0807

  Operations & Transport · mapped topic

• B01F7/0075

  Operations & Transport · mapped topic

• B01F15/065

  Operations & Transport · mapped topic

• B01F15/06

  Operations & Transport · mapped topic