System for incondensable component separation in a liquefied natural gas facility

Patent metadata

Field	Value
Publication number	US-9644889-B2
Application number	US-55453909-A
Country	US
Kind code	B2
Filing date	Sep 4, 2009
Priority date	Sep 8, 2008
Publication date	May 9, 2017
Grant date	May 9, 2017

Abstract

A liquefied natural gas (LNG) facility that employs a system to remove incondensable material from one or more refrigeration cycles within the facility. One or more embodiments of the present invention can be advantageously employed in an open-loop refrigeration cycle to remove at least a portion of one or more high vapor pressure components that have accumulated in the refrigerant cycle over time. In addition, several embodiments can be advantageously employed to stabilize facility operation in the event of drastic changes to the concentration of the natural gas feed stream introduced into the facility.

First claim

What is claimed is:

1. A process for liquefying a natural gas stream, the process comprising:
(a) cooling said natural gas stream via indirect heat exchange with a first refrigerant in a first closed-loop refrigeration cycle to provide a cooled natural gas stream;
(b) further cooling at least a portion of the cooled natural gas stream via indirect heat exchange with a predominantly methane refrigerant in an open-loop refrigeration cycle to provide a further cooled natural gas stream, wherein the open-loop refrigeration cycle comprises a refrigerant compressor;
(c) separating an incondensable material from at least a portion of the further cooled natural gas stream in a first separation vessel to provide an incondensables-depleted predominantly liquid bottoms fraction and an incondensables-rich predominantly vapor overhead fraction, wherein at least a portion of said further cooled natural gas stream introduced into said first separation vessel has passed through said refrigerant compressor;
(d) routing the incondensables-rich predominantly vapor overhead fraction to a fuel gas system for use as a fuel gas; and
(e) recovering the incondensables-depleted predominantly liquid bottoms fraction back into the predominantly methane refrigerant of the open-loop refrigeration cycle, wherein the incondensables-depleted predominantly liquid bottoms fraction is controllably routed from the first separation vessel routed directly to an inlet of a main heat exchanger of the open-loop refrigeration cycle along a first path and from the first separation vessel to an outlet of the main heat exchanger of the open-loop refrigeration cycle along a bypass path.

2. The process of claim 1 , further comprising, prior to step (b), separating at least a portion of said cooled natural gas stream into a heavies-depleted stream and a heavies-rich stream in a heavies removal column, wherein said at least a portion of said cooled natural gas stream introduced into said open-loop refrigeration cycle comprises at least a portion of said heavies-depleted stream.

3. The process of claim 2 , wherein the overhead pressure of said first separation vessel is at least about 170 kPa greater than the overhead pressure of said heavies removal column.

4. The process of claim 2 , further comprising, prior to step (b), cooling at least a portion of said heavies-depleted stream in a second refrigeration cycle via indirect heat exchange with a second refrigerant to thereby provide a cooled heavies-depleted stream, wherein said at least a portion of cooled natural gas stream introduced into said open-loop refrigeration cycle comprises at least a portion of said cooled heavies-depleted stream.

5. The process of claim 1 , wherein the further cooled natural gas stream introduced into said first separation vessel has a temperature in the range of from about −80° C. to about −105° C. and a pressure in the range of from about 3,790 kPa to about 4,485 kPa.

6. The process of claim 1 , further comprising, subsequent to step (b), flashing at least a portion of said further cooled natural gas stream to thereby provide a two-phase natural gas stream and separating at least a portion of said two-phase natural gas stream into a cooled vapor fraction and a cooled liquid fraction, wherein the further cooled natural gas stream introduced into said first separation vessel comprises at least a portion of said cooled vapor fraction.

7. The process of claim 6 , wherein said predominantly methane refrigerant comprises at least a portion of said cooled vapor fraction.

8. The process of claim 6 , further comprising compressing at least a portion of said cooled vapor fraction in said refrigerant compressor, wherein substantially all of the further cooled natural gas stream introduced into said first separation vessel has passed through said compressor.

9. The process of claim 1 , wherein said first refrigerant is a pure component refrigerant.

10. The process of claim 1 , wherein said first refrigerant predominantly comprises propane, propylene, ethane, or ethylene.

11. The process of claim 1 , further comprising measuring the pressure of said predominantly vapor stream and/or said predominantly liquid stream withdrawn from said first separation vessel to provide a measured pressure value and, based on said measured pressure value, adjusting the flow rate of said predominantly vapor stream and/or said predominantly liquid stream.

12. The process of claim 1 , wherein said first separation vessel defines an operating liquid level; further comprising, measuring said operating liquid level of said first separation vessel to provide a measured level value and, based on said measured level value, adjusting the flow rate of said predominantly vapor stream and/or said predominantly liquid stream withdrawn from said first separation vessel.

13. The process of claim 1 , wherein said first separation vessel is horizontally elongated.

Assignees

• Ransbarger Weldon L
• Evans Megan V
• Praderio Attilio J
• Messersmith David B
• Conocophillips Co

Inventors

• Ransbarger Weldon L
• Evans Megan V
• Praderio Attilio J
• Messersmith David B

Classifications

• F25J1/021 Primary

  using a deep flash recycle loop · CPC title

• F25J1/0052

  by vaporising a liquid refrigerant stream · CPC title

• F25J1/0022

  Hydrocarbons, e.g. natural gas · CPC title

• F25J1/004

  by flash gas recovery (F25J1/0267 takes precedence) · CPC title

• F25J2220/62

  Separating low boiling components, e.g. He, H2, N2, Air · CPC title