Method and apparatus for the low-temperature fractionation of a fluid mixture

Patent metadata

Field	Value
Publication number	US-9527002-B2
Application number	US-201214240565-A
Country	US
Kind code	B2
Filing date	Aug 2, 2012
Priority date	Aug 25, 2011
Publication date	Dec 27, 2016
Grant date	Dec 27, 2016

Abstract

The method and the apparatus are used for the low-temperature fractionation of a fluid mixture. The fluid mixture is introduced into a separation column. At least a portion of the sump liquid from the separation column is introduced into a sump evaporator and at least partly evaporated there. At least a portion of the vapor produced in the sump evaporator is led back into a lower section of the separation column. A top product is removed at the top of the separation column, and a sump product is removed from the sump of the separation column or from the sump evaporator. The sump evaporator is operated by means of inductive heating.

First claim

The invention claimed is:

1. A method for low-temperature fractionation of a fluid mixture comprising:
introducing said fluid mixture into a separation column to produce a top gaseous product and a bottom liquid,
introducing at least part of said bottom liquid into a bottom evaporator wherein said bottom liquid is at least partially evaporated in said bottom evaporator to form a vapor,
returning at least part of said vapor generated in the bottom evaporator to a lower portion of said separation column,
removing said top gaseous product from the top of said separation column, and
removing a bottom product from the bottom of said separation column or from said bottom evaporator,
wherein said bottom evaporator is heated by inductive heating.

2. The method as claimed in claim 1 , wherein said bottom evaporator comprises a vessel having a wall, and said wall of said vessel is heated directly by induction.

3. The method as claimed in claim 1 , wherein said bottom evaporator comprises a vessel having a wall, and a heating body is arranged on the outer side of said wall of said vessel, said heating body is heated directly by induction and the inductively generated heat is transferred to said wall of said vessel by conduction.

4. The method as claimed in claim 1 , wherein said bottom evaporator comprises a vessel having a wall, and a heating body is arranged on the inner side of said wall of said vessel, and said heating body is heated directly by induction.

5. The method as claimed in claim 1 , wherein said bottom evaporator comprises a vessel having a wall, and a heating body is arranged inside said vessel of said bottom evaporator, at a distance from said wall of said vessel, said heating body is heated directly by induction.

6. The method as claimed in claim 1 , wherein said fluid mixture is a mixture of air gases enriched with krypton and xenon.

7. An apparatus for the low-temperature fractionation of a fluid mixture, comprising:
a separation column and a bottom evaporator for evaporating bottom liquid of the separation column, means for introducing a fluid mixture into the separation column, means for introducing vapor generated in the bottom evaporator into a lower portion of the separation column, means for drawing off a top product at the top of the separation column, means for removing a bottom product at the bottom of the separation column or from the bottom evaporator and an induction heating unit for heating the bottom evaporator.

8. The method as claimed in claim 4 , wherein said heating body comprises multiple concentric cylinders with different diameters.

9. The method as claimed in claim 5 , wherein said heating body comprises multiple concentric cylinders with different diameters.

10. The method as claimed in claim 2 , wherein the inner side of the vessel wall is provided with ribs.

11. The method as claimed in claim 3 , wherein the inner side of the vessel wall is provided with ribs.

12. The method as claimed in claim 5 , wherein said heating body is provided with ribs.

13. The method as claimed in claim 4 , wherein said heating body is perforated.

14. The method as claimed in claim 5 , wherein said heating body is perforated.

15. The method as claimed in claim 2 , wherein said bottom evaporator further comprises a heating body which is heated directly by induction and which is arranged on the outer side of said wall of said vessel or the inner side of said wall of said vessel, and said is heating body is in the form of a hollow cylinder.

16. The method as claimed in claim 3 , wherein said heating body is in the form of a hollow cylinder.

17. The method as claimed in claim 4 , wherein said heating body is in the form of a hollow cylinder.

18. The method as claimed in claim 5 , wherein said heating body is in the form of a hollow cylinder.

19. The method as claimed in claim 4 , wherein said heating body is provided with ribs.

Assignees

• Rudiger Horst
• Eckl Robert
• Windmeier Christoph
• Beimler Alexander
• Yu Yonggui
• Linde Ag

Inventors

• Rudiger Horst
• Eckl Robert
• Windmeier Christoph
• Beimler Alexander
• Yu Yonggui

Classifications

• F25J2200/40

  Features relating to the provision of boil-up in the bottom of a column · CPC title

• F25J2290/44

  Particular materials used, e.g. copper, steel or alloys thereof or surface treatments used, e.g. enhanced surface · CPC title

• F25J3/04751

  Producing pure krypton and/or xenon recovered from a crude krypton/xenon mixture · CPC title

• B01D3/322

  Reboiler specifications · CPC title

• F25J3/04745

  Krypton and/or Xenon · CPC title