Method for producing fine particles and apparatus for producing fine particles

Patent metadata

Field	Value
Publication number	US-9522370-B2
Application number	US-201314382471-A
Country	US
Kind code	B2
Filing date	Feb 28, 2013
Priority date	Mar 5, 2012
Publication date	Dec 20, 2016
Grant date	Dec 20, 2016

Abstract

A method for producing fine particles, including: discharging a fine particle material liquid, where solid materials to be formed into fine particles are dissolved or dispersed in a solvent or are melted, from two or more discharge holes in a downward vertical direction, to thereby form liquid droplets; and solidifying the liquid droplets discharged to form fine particles, wherein in the discharging a fine particle material liquid, gas flow is supplied at angle of greater than 0° but 90° or smaller to the downward vertical direction, and wherein an initial discharge velocity of the liquid droplets discharged from the discharge hole located at an upstream side of the gas flow in a flowing direction thereof is equal to or higher than an initial discharge velocity of the liquid droplets discharged from the discharge hole located at a downstream side of the gas flow in the flowing direction thereof.

First claim

The invention claimed is:

1. A method for producing fine particles, comprising:
discharging a fine particle material liquid, where solid materials to be formed into fine particles are dissolved or dispersed in a solvent or are melted, from two or more discharge holes in a downward vertical direction, to thereby form liquid droplets; and
solidifying the liquid droplets discharged to form fine particles,
wherein in the discharging the fine particle material liquid, a gas flow is supplied at an angle of greater than 0° but 90° or smaller with respect to the downward vertical direction, and
wherein an initial discharge velocity of the liquid droplets discharged from the discharge hole located at an upstream side of the gas flow in a flowing direction thereof is equal to or higher than an initial discharge velocity of the liquid droplets discharged from the discharge hole located at a downstream side of the gas flow in the flowing direction thereof;
wherein in at least one of adjacent pairs of the discharge holes in the two or more discharge holes, the liquid droplets discharged from the discharge hole located at the downstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 1 and the liquid droplets discharged from the discharge hole located at the upstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 2 , where the initial discharge velocity V 1 is equal to or smaller than 0.9×V 2 .

2. The method according to claim 1 ,
wherein the at least one of adjacent pairs of the discharge holes are a pair of the discharge hole located at the most upstream side of the gas flow in the flowing direction thereof and the discharge hole adjacent to the discharge hole located at the most upstream side of the gas flow in the flowing direction thereof.

3. The method according to claim 1 ,
wherein in each of the adjacent pairs of the discharge holes in the two or more discharge holes, the liquid droplets discharged from the discharge hole located at the downstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 1 and the liquid droplets discharged from the discharge hole located at the upstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 2 , where the initial discharge velocity V 1 is equal to or smaller than 0.9×V 2 .

4. The method according to claim 1 ,
wherein the discharge hole located at the downstream side of the gas flow in the flowing direction thereof has an opening diameter D 1 and the discharge hole located at the upstream side of the gas flow in the flowing direction thereof has an opening diameter D 2 , where the opening diameter D 1 is equal to or greater than 1.1×D 2 .

5. The method according to claim 1 ,
wherein the gas flow is supplied at an angle of 90° with respect to the downward vertical direction.

6. The method according to claim 1 ,
wherein the discharging the fine particle material liquid comprises applying vibration to the fine particle material liquid in a liquid column resonance-generating liquid chamber comprising the two or more discharge holes to thereby form a standing wave through liquid column resonance, and discharging the fine particle material liquid from the discharge holes located in a region corresponding to an antinode of the standing wave to thereby form liquid droplets.

7. The method according to claim 6 ,
wherein a frequency f of the vibration satisfies a relationship: N×c/(4L)≦f≦(N+1)×c/(4Le),
wherein L is a length of the liquid column resonance-generating liquid chamber in a longitudinal direction thereof, Le is a distance between an end portion of the liquid column resonance-generating liquid chamber at a side of a supply path for supplying the fine particle material liquid to the liquid column resonance-generating liquid chamber and the discharge hole closest to the end portion thereof, c is a velocity of a sound wave in the fine particle material liquid, and N is an integer.

8. The method according to claim 1 ,
wherein the initial discharge velocities of the liquid droplets are lower than a velocity of the gas flow.

9. The method according to claim 1 ,
wherein the initial discharge velocities of the liquid droplets discharged from the two or more discharge holes are adjusted by changing pitches between the discharge holes or opening diameters of the discharge holes.

10. An apparatus, comprising:
a gas flow generating unit configured to generate gas flow having an angle of greater than 0° but 90° or smaller with respect to a downward vertical direction;
a gas flow path through which the gas flow generated by the gas flow generating unit flows; and
a liquid droplet discharging unit comprising two or more discharge holes and configured to discharge, to the gas flow path, a fine particle material liquid where solid materials to be formed into fine particles are dissolved or dispersed in a solvent or are melted,
wherein an initial discharge velocity of the liquid droplets discharged from the discharge hole located at an upstream side of the gas flow in a flowing direction thereof is equal to or higher than an initial discharge velocity of the liquid droplets discharged from the discharge hole located at a downstream side of the gas flow in the flowing direction thereof;
wherein in at least one of adjacent pairs of the discharge holes in the two or more discharge holes, the liquid droplets discharged from the discharge hole located at the downstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 1 and the liquid droplets discharged from the discharge hole located at the upstream side of the gas flow in the flowing direction thereof have an initial discharge velocity V 2 , where the initial discharge velocity V 1 is equal to or smaller than 0.9×V 2 .

Assignees

• Norikane Yoshihiro
• Takahashi Satoshi
• Ohgaki Masaru
• Ricoh Co Ltd

Inventors

• Norikane Yoshihiro
• Takahashi Satoshi
• Ohgaki Masaru
• Mulwa Andrew Mwaniki

Classifications

• G03G9/0804

  whereby the components are brought together in a liquid dispersing medium · CPC title

• G03G9/0802

  Preparation methods · CPC title

• B01J2/04

  in a gaseous medium {(if combined with suspending the material in a gas, e.g. fluidised beds B01J2/16)} · CPC title

• B01J2/18

  using a vibrating apparatus · CPC title

• B01J2/06 Primary

  in a liquid medium · CPC title