Measuring total organic carbon of shales using thermal expansion
US-2017336528-A1 · Nov 23, 2017 · US
US9518944B2 · US · B2
| Field | Value |
|---|---|
| Publication number | US-9518944-B2 |
| Application number | US-201414295781-A |
| Country | US |
| Kind code | B2 |
| Filing date | Jun 4, 2014 |
| Priority date | Jun 27, 2013 |
| Publication date | Dec 13, 2016 |
| Grant date | Dec 13, 2016 |
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A temperature-controlled bath capable of swiftly changing the temperature of a sample to a target temperature and maintaining the temperature of the sample at a fixed temperature after the temperature change is provided. A temperature-controlled bath includes a temperature changing means, a temperature-controlled chamber, a sample holding chamber, and connection cut-off means. The temperature changing means is disposed in the temperature-controlled chamber, and the temperature of the temperature-controlled chamber is adjusted by the temperature changing means. The sample holding chamber is separated from the temperature-controlled chamber by a thermally conducive wall, and contains a sample therein. The connection cut-off means change a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state.
Opening claim text (preview).
What is claimed is: 1. A temperature-controlled bath comprising: temperature changing means for heating or cooling a gas so that the temperature of the gas is adjusted to a set temperature; a temperature-controlled chamber whose temperature is adjusted by the temperature changing means, the temperature changing means being disposed in the temperature-controlled chamber; a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall; and connection cut-off means for changing a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state. 2. The temperature-controlled bath according to claim 1 , further comprising first blower means for sending a gas whose temperature is adjusted by the temperature changing means mainly into the temperature-controlled chamber. 3. The temperature-controlled bath according to claim 1 , further comprising an air hole that serves as an inlet/outlet of the gas between the temperature-controlled chamber and the sample holding chamber; second blower means for sending the gas in the temperature-controlled chamber into the sample holding chamber through the air hole; and third blower means for sending out the gas in the sample holding chamber toward the temperature-controlled chamber through the air hole. 4. The temperature-controlled bath according to claim 1 , wherein the thermally conductive wall comprises at least one of a radiator plate protruding toward the temperature-controlled chamber and a radiator plate protruding toward the sample holding chamber. 5. The temperature-controlled bath according to claim 1 , wherein the sample holding chamber comprises a probe inserting hole for inserting a probe into the sample holding chamber, the probe inserting hole being able to be opened and closed. 6. The temperature-controlled bath according to claim 1 , wherein the sample holding chamber comprises an optically transparent window for enabling optical measurement of the sample. 7. The temperature-controlled bath according to claim 1 , wherein the connection cut-off means is an open/close shutter that opens/closes by rotating a plate member, and the plate member is an air-permeable plate member capable of letting a gas pass through the plate member. 8. A linear expansion coefficient measuring device comprising: a temperature-controlled bath; measurement means for measuring a length of the sample at different temperatures; and calculation means for calculating a coefficient of linear expansion of the sample based on the length of the sample at each temperature, wherein the temperature-controlled bath comprises: temperature changing means for heating or cooling a gas so that the temperature of the gas is adjusted to a set temperature; a temperature-controlled chamber whose temperature is adjusted by the temperature changing means, the temperature changing means being disposed in the temperature-controlled chamber; a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall; and connection cut-off means for changing a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state. 9. A temperature-controlled bath comprising: a temperature changing unit that heats or cools a gas so that the temperature of the gas is adjusted to a set temperature; a temperature-controlled chamber whose temperature is adjusted by the temperature changing unit, the temperature changing unit being disposed in the temperature-controlled chamber; a sample holding chamber containing a sample therein, the sample holding chamber being separated from the temperature-controlled chamber by a thermally conductive wall; and a connection cut-off unit that changes a connection between the temperature-controlled chamber and the sample holding chamber to a connected state or a cut-off state. 10. The temperature-controlled bath according to claim 9 , further comprising a first blower unit that sends a gas whose temperature is adjusted by the temperature changing unit mainly into the temperature-controlled chamber. 11. The temperature-controlled bath according to claim 9 , further comprising an air hole that serves as an inlet/outlet of the gas between the temperature-controlled chamber and the sample holding chamber; a second blower unit that sends the gas in the temperature-controlled chamber into the sample holding chamber through the air hole; and a third blower unit that sends out the gas in the sample holding chamber toward the temperature-controlled chamber through the air hole. 12. The temperature-controlled bath according to claim 9 , wherein the connection cut-off unit is an open/close shutter that opens/closes by rotating a plate member, and the plate member is an air-permeable plate member capable of letting a gas pass through the plate member.
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