Swept membrane emulsification

Patent metadata

Field	Value
Publication number	US-9393532-B2
Application number	US-201414761327-A
Country	US
Kind code	B2
Filing date	Jan 27, 2014
Priority date	Feb 27, 2013
Publication date	Jul 19, 2016
Grant date	Jul 19, 2016

Abstract

A method for making an emulsion using a rotating membrane device ( 10 ) including:
i) a membrane assembly ( 12 ) including a cylindrical porous surface ( 14 ) enclosing an inner chamber ( 16 ) concentrically positioned about an axis (X), ii) a vane assembly ( 18 ) including a plurality of vanes ( 20 ) extending along the axial length (L) of the porous surface ( 14 ) of the membrane assembly ( 12 ), wherein the vanes ( 24 ) comprise a shear surface ( 24 ) located within 1 mm of the porous surface ( 14 ), and iii) a vessel ( 22 ) enclosing the membrane and vane assemblies ( 12, 18 ); wherein the method includes the step of moving a dispersible liquid phase ( 26 ) through the porous surface ( 14 ) into a continuous liquid phase ( 28 ) while rotating at least one of the vane assembly ( 18 ) or membrane assembly ( 12 ) relative to the other about the axis (X) such that the shear surfaces ( 24 ) exert shear forces upon the dispersible liquid phase ( 26 ) passing through the porous surface ( 14 ) to form droplets ( 30 ) of a dispersed liquid phase having a size of 1 to 500 μm within the continuous liquid phase ( 28 ).

First claim

The invention claimed is:

1. A method for making an emulsion wherein the method comprises providing:
i) a membrane assembly ( 12 ) comprising a cylindrical porous surface ( 14 ) enclosing an inner chamber ( 16 ) concentrically positioned about an axis (X),
ii) a vane assembly ( 18 ) comprising a plurality of vanes ( 20 ) extending along the axial length of the porous surface ( 14 ) of the membrane assembly ( 12 ), wherein the vanes ( 20 ) comprise a shear surface ( 24 ) located within 1 mm of, and without making physical contact with the porous surface, and
iii) a vessel ( 22 ) enclosing the membrane and vane assemblies;
and wherein the method further comprises the step of moving a dispersible liquid phase through the porous surface ( 14 ) into a continuous liquid phase while rotating at least one of the vane assembly ( 18 ) or membrane assembly ( 12 ) relative to the other about the axis (X) such that the shear surfaces ( 24 , 24 ′) exert shear forces upon the dispersible liquid phase passing through the porous surface ( 14 ) to form droplets of a dispersed liquid phase having a size of 1 to 500 μm within the continuous liquid phase.

2. The method of claim 1 wherein the step of forcing the dispersible liquid phase through the porous surface ( 14 ) includes the step of applying pressure to a source of the dispersible liquid phase located within the inner chamber ( 16 ) of the membrane assembly ( 12 ) to force the dispersible liquid phase radially outward through pores of the porous surface ( 14 ) and into a surrounding continuous liquid phase.

3. The method of claim 1 wherein the vane assembly is positioned concentrically about the membrane assembly ( 12 ) and the step of rotating involves spinning the vanes ( 20 ) of the vane assembly ( 18 ) about the circumference of the cylindrical porous surface ( 14 ) of the membrane assembly ( 12 ).

4. The method of claim 1 wherein the porous surface ( 14 ) and shear surfaces ( 24 ) both have surface areas, and wherein the collective surface area of the shear surfaces ( 24 ) is less than one half of the surface area of the porous surface ( 14 ).

Assignees

• Rohm & Haas
• Dow Global Technologies Llc

Inventors

• Ramalingam Santhosh K
• Sarafinas Aaron

Classifications

• B29B9/10

  by moulding the material, i.e. treating it in the molten state · CPC title

• B01F3/0807

  Operations & Transport · mapped topic

• B01F5/0465

  Operations & Transport · mapped topic

• B01F3/0865

  Operations & Transport · mapped topic

• B01F5/0665 Primary

  Operations & Transport · mapped topic