Method and apparatus for separation of mixture

Patent metadata

Field	Value
Publication number	US-9370782-B2
Application number	US-201214364154-A
Country	US
Kind code	B2
Filing date	Dec 11, 2012
Priority date	Dec 12, 2011
Publication date	Jun 21, 2016
Grant date	Jun 21, 2016

Abstract

The present invention provides a method and an apparatus for separating a mixture that are capable of separating a mixture containing a plurality types of particles, using a countercurrent classification technique, even when there is little difference in density and particle diameter depending on the types of particles. In the present invention, a mixture containing first particles and second particles is separated using a separation tube 13 having the inverted-conical or pyramidal shape or a substantially inverted-conical or pyramidal shape. The first particles and the second particles are made of substances having different magnetic susceptibilities. A fluid is caused to flow upward through the separation tube 13 , and the flow of the fluid is used to introduce the mixture into the separation tube 13 . The first particles and the second particles are held in the separation tube 13 in a mixed state. A gradient magnetic field is applied to a region inside the separation tube 13 using magnetic field generation means 23 , in the state where the first particles and the second particles are held in the separation tube 13 . The magnetic field gradient of the gradient magnetic field has a vertical component.

First claim

The invention claimed is:

1. A mixture separation method for separating, by type, a mixture containing first particles and second particles which are different in type, or separating a specific type of particles from the mixture, using a separation tube having an inverted-conical or pyramidal shape or a substantially inverted-conical or pyramidal shape, the first particles and the second particles being respectively made of substances having different magnetic susceptibilities, the method comprising:
causing a fluid to flow upward through the separation tube;
introducing the mixture into the separation tube and holding the first particles and the second particles in the separation tube through which the fluid is flowing;
applying a gradient magnetic field to the first particles and the second particles that are held in the separation tube; and
moving the second particles in the separation tube to outside the separation tube by changing the flow of the fluid in the separation tube in a state where the gradient magnetic field is being applied,
wherein a magnetic field gradient of the gradient magnetic field has a vertical component, and
wherein the first particles are brought together at substantially the same height in the separation tube when the gradient magnetic field is applied.

2. A mixture separation method for separating, by type, a mixture containing first particles and second particles which are different in type, or separating a specific type of particles from the mixture, using a separation tube that has an inverted-conical or pyramidal shape or a substantially inverted-conical or pyramidal shape, the method comprising:
causing a fluid to flow upward through the separation tube to which a gradient magnetic field is applied;
introducing the mixture into the separation tube;
holding, in the separation tube through which the fluid is flowing, the first particles and the second particles to which the gradient magnetic field is applied, with distributed regions of the first particles and the second particles separated from each other in the vertical direction; and
moving the second particles in the separation tube to outside the separation tube by changing the flow of the fluid in the separation tube,
wherein the first particles and the second particles are respectively made of substances having different magnetic susceptibilities,
a magnetic field gradient of the gradient magnetic field has a vertical component,
the fluid flows through the separation tube such that the first particles and the second particles are held in the separation tube, even when the gradient magnetic field is not applied to the separation tube, and
the first particles are brought together at substantially the same height in the separation tube.

3. The mixture separation method according to claim 1 , further comprising causing the fluid in which the mixture is suspended to flow upward through the separation tube.

4. The mixture separation method according to claim 1 , wherein the fluid is water, and the first particles are made of a paramagnetic substance and the second particles are made of a diamagnetic substance.

5. A mixture separation apparatus for separating a mixture containing first particles and second particles which are different in type and made of substances having different magnetic susceptibilities, or separating a specific type of particle from the mixture, the apparatus comprising:
a separation tube that has an inverted-conical or pyramidal shape or a substantially inverted-conical or pyramidal shape, and through which a fluid is caused to flow upward;
flow rate adjusting means for adjusting a flow rate of the fluid that is supplied to the separation tube; and
magnetic field generation means for applying a gradient magnetic field whose magnetic field gradient has a vertical component to the separation tube,
wherein the flow rate of the fluid that is supplied to the separation tube is adjusted so that the first particles and the second particles are held in the separation tube when the mixture is introduced into the separation tube,
the gradient magnetic field is applied to the first particles and the second particles in a state where the first particles and the second particles are held in the separation tube,
the first particles are brought together at substantially the same height in the separation tube when the gradient magnetic field is applied, and
the second particles in the separation tube move to outside the separation tube by the flow rate adjusting means changing the flow of the fluid in the separation tube in a state where the gradient magnetic field is being applied.

6. A mixture separation apparatus for separating a mixture containing first particles and second particles which are different in type and made of substances having different magnetic susceptibilities, or separating a specific type of particle from the mixture, the apparatus comprising:
a separation tube that has an inverted-conical or pyramidal shape or a substantially inverted-conical or pyramidal shape;
flow rate adjusting means for adjusting a flow rate of a fluid that is supplied to the separation tube; and
magnetic field generation means for applying a gradient magnetic field whose magnetic field gradient has a vertical component to the separation tube,
wherein the fluid is caused to flow upward through the separation tube to which the gradient magnetic field is being applied, the mixture is introduced into the separation tube, and the first particles and the second particles to which the gradient magnetic field is being applied are held in the separation tube through which the fluid is flowing, with distributed regions of the first particles and the second particles separated from each other in the vertical direction,
the flow rate of the fluid that is supplied to the separation tube is adjusted such that the first particles and the second particles are held in the separation tube, even when the gradient magnetic field is not applied to the separation tube,
the first particles are brought together at substantially the same height in the separation tube, and
the second particles in the separation tube move to outside the separation tube by the flow rate adjusting means changing the flow of the fluid in the separation tube.

7. The mixture separation apparatus according to claim 5 , wherein the fluid in which the mixture is suspended is caused to flow upward through the separation tube.

8. The mixture separation apparatus according to claim 5 , wherein the fluid is water, and the first particles are made of a paramagnetic substance and the second particles are made of a diamagnetic substance.

9. The mixture separation method according to claim 2 , further comprising causing the fluid in which the mixture is suspended to flow upward through the separation tube.

10. The mixture separation method according to claim 2 , wherein the fluid is water, and the first particles are made of a paramagnetic substance and the second particles are made of a diamagnetic substance.

11. The mixture separation apparatus according to claim 6 , wherein the fluid in which the mixture is suspended is caused to flow upward through the separation tube.

12. The mixture separation apparatus according to claim 6 , wherein the fluid is water, and the first particles are made of a paramagnetic substance and the second particles are made of a diamagnetic substance.

Assignees

• Univ Osaka
• Ube Industries

Inventors

• Nishijima Shigehiro
• MISHIMA Fumihito
• Kaiso Koji
• Shimakawa Toshihiro

Classifications

• B03B5/66

  of the hindered settling type · CPC title

• B03C1/32 Primary

  acting on the medium containing the substance being separated, e.g. magneto-gravimetric-, magnetohydrostatic-, or magnetohydrodynamic separation · CPC title

• B03C2201/20

  Magnetic separation of bulk or dry particles in mixtures · CPC title

• B03B13/04

  using electrical or electromagnetic effects · CPC title

• B03B5/623

  Upward current classifiers · CPC title